Preferred Language
Sort By
Filters
Filter
Publication
Publication Date
Indexed In
Publication Date
Mon Oct 01 2012
Journal Name
Iraqi Journal Of Physics
Nanostructural study of Ti-Ni binary alloy prepared by mechanical alloying
...Show More Authors

In the present study, a powder mixture of elements Ti and Ni was mechanically alloyed in a high energy ball mill. Microstructure of the nanosized amorphous milled product in different stages of milling has been characterized by X- ray diffraction, scanning electron microscopy and differential thermal analysis. We found that time of mechanical alloying is more significant to convert all crystalline structure to the amorphous phase. Nanocrystalline phase was achieved as a result of the mechanical alloying process. The results also indicates that the phase transformation and the grain size occurs in these alloys are controlled by ball milling time

View Publication Preview PDF
Publication Date
Sun Dec 01 2013
Journal Name
Journal Of Economics And Administrative Sciences
CALCULATION BIASES FOR COEFFICIENTS AND SCALE PARAMETER FOR LINEAR (TYPE 1) EXTREME VALUE REGRESSION MODEL FOR LARGEST VALUES
...Show More Authors

Abstract

Characterized by the Ordinary Least Squares (OLS) on Maximum Likelihood for the greatest possible way that the exact moments are known , which means that it can be found, while the other method they are unknown, but approximations to their biases correct to 0(n-1) can be obtained by standard methods. In our research expressions for approximations to the biases of the ML estimators (the regression coefficients and scale parameter) for linear (type 1) Extreme Value Regression Model for Largest Values are presented by using the advanced approach depends on finding the first derivative, second and third.

View Publication Preview PDF
Crossref
Publication Date
Wed Apr 04 2012
Journal Name
The Iraqi Journal Of Veterinary Medicine
The effect of using Ginger (Zingiber officinale) or parsley seeds (petroselinum sativum) on some of physiologically traits of black: Mudhaffar N.R.Al-Saigh and Mohammed M. Dakheel
...Show More Authors

The study was aimed to know the effect of adding 3% of grind zingiber officinale or 8% of
petroselinum sativum seeds in the concentrate diet (400g/head/ daily) of the Black Iraqi Does (19
does) in some physiological traits. Nineteen healthy weak-medium does were divided into three
groups, the first group of 6 does fed concentrate diet containing zingiber, while in the second
group (6) does were fed on a diet containing 8% grind petroselinum sativum seeds, however, the
other does kept as control group and fed the concentrate diet free of the herbal medical additives
during mid December 2009 up to end of May 2010. The results revealed that group, The first and
second groups were highly significant (p>0.05) in their

... Show More
View Publication Preview PDF
Crossref (1)
Crossref
Publication Date
Sun Sep 06 2015
Journal Name
Baghdad Science Journal
Methionine as a Spacer between Poly Acrylic acid and Ampicillin
...Show More Authors

In this work a novel drug delivery system through modification of poly acrylic acid with Methionine as a spacer between the poly acrylic acid which was converted to its acyl chloride and reacted with Methionine as spacer unit which has been reacted with Ampicillin drug. In vitro drug release study had been conducted successfully in basic medium in pH 7.4 and acidic medium in pH 1.1 at 37?. Due to many problems associated with drug release and, this modification could decrease the side effect of drug. The prepared prodrug polymer was characterized by spectra method [FTIR and 1H?NMR]. Physical properties and intrinsic viscosity of drug polymer were determined. The good results were obtained in the presence of spacer unit with compar

... Show More
View Publication Preview PDF
Crossref
Publication Date
Sun Nov 01 2020
Journal Name
Journal Of Physics: Conference Series
Synthesis, Characterization and Biological Activity of Mixed Ligand Metal Salts Complexes with Various Ligands
...Show More Authors

Metal (III) and (II) coordination compounds of o- phenylenediamine, oxalic acid dihydrate and 8-hydroxyquinoline were synthesized for mixed ligand complexes and characterized using FT-IR, UV-Vis and mass spectra, atomic absorption, elemental analysis, electric conductance and magnetic susceptibility measurements. In addition, thermal behavior (TGA) of the metal complexes (1-6) showed good agreement with the formula suggested from the analytical data. The stoichiometric reaction between the metal (III) and (II) ions with three various ligands in molar ratio at aqueous ethyl alchol for (1:1:1:1) (M: O-PDA: OA: 8-HQ) [where M = Cr+3, Mn+2, Co+2, Ni+2. Cu+2 and Zn+2; O-PDA = O-Phenylenediamine; OA = Oxalic acid and 8-HQ = 8-Hydroxyquinoline]. R

... Show More
Publication Date
Wed Mar 10 2021
Journal Name
Baghdad Science Journal
Takir some study of environmental factors on the weight of some phases of the screwworm fly the ancient world
...Show More Authors

The weight of larvae virgins and Alcamlat for males more than the weight of females of the roles themselves that the highest rate of loss in weight of larvae developed to virgins when field conditions were (21.5,22,21.3) mg during June and July and August respectively, recorded the highest degrees of heat and less attributed to moisture

View Publication Preview PDF
Publication Date
Thu Aug 01 2024
Journal Name
Mustansiriyah Journal Of Sports Science
تأثير أسلوب التدريب المتقطع المتناوب في مستوى تركيز الكيتونات و الحامض الرايبوزي( 206) لدى لاعبي كرة السلة
...Show More Authors

تركزت نفاط البحث وأهدافه في اعداد برنامج تدريبي باسلوب التدريب المتقطع المتناوب الذي هو مزيج مابين السرعة والقوة وتاثيره في مستوى تركيز الكيتونات و الحامض الرايبوزي (206) لدى لاعبي كرة السلة.مجتمع البحث تم اختيارهم من لاعبي النخبة (الدوري الممتاز) بكرة السلة للموسم( 2023_2022) من لاعبي الدفاع الجوي للمتقدمين  والبالغ عددهم (16 لاعبا)، استخدم الباحث الاسلوب التجريبي بتصميم المجموعتين (الضابطة والتجريبية)، فترة ا

... Show More
View Publication
Crossref
Publication Date
Sun Sep 06 2015
Journal Name
Baghdad Science Journal
Preparation and Characterization of Some Metal Complexes with Heterocyclic Azo Ligand (4-SuBAI)
...Show More Authors

The preparation and characterization of the Cu (II), Co(II), Ni(II), Zn(II), Cd(II), and Hg(II) metal complexes of heterocyclic azo ligand 2-[(4`-sulphamide phenyl) azo] -4,5-diphenyl imidazole (4-SuBAI) have been studied by elemental analysis, FT-IR and UV-Vis Spectroscopic, magnetic moment and molar conductance methods. The analytical data showed that all chelate complexes were prepared with (metal-ligand) ratio of (1:2). The general formula of these complexes was [ML2X2]. nH2O [were L=2-[(4`-sulphamide phenyl) azo]-4,5-diphenyl imidazole and X=Cl, and the octahedral geometry were suggested for these complexes .

View Publication Preview PDF
Crossref
Publication Date
Sun Sep 30 2018
Journal Name
College Of Islamic Sciences
الحداثة في الأدب بين الغرب و العرب مقاربة بين الاتباع والابتداع
...Show More Authors

 

            حاول البحثُ أن يقدم رؤية للإجابة عن بعض التساؤلات التي أحاطت بمصطلح الحداثة وجذورها ، وأصولها ، وعن جهة انتماء المصطلح  وجذوره، وهل يملك العربُ حداثةً ؟  أو أن ارتباط الحداثة  بهم لا يعدو عن كونه أسلوباً ما لاستقطاب الأنصار،  كما ناقش البحث الادّعاء القائل إنّ الحداثة عند العرب ليست سوى ( حداثة تلفيـقيّـة ) أخذت ما عند الغير ، ولم تجدّد فيه ؟

... Show More
View Publication Preview PDF
Publication Date
Tue Nov 13 2018
Journal Name
Arab Science Heritage Journal
الثروة الثروة المائية في المغرب العربي من القرن 4 – 7 هـ/ 10 م – 13 م دراسة تاريخية
...Show More Authors

Water resources would be differentiate in Morocco specially in Morocco  which appear as form of eyes ,rivers as dissolved water of mountain.

The human takes care of water either as rains to store and use in necessity trying to bring it to Maracas  by  helping from state

View Publication Preview PDF
Publication Date
Thu Jun 28 2018
Journal Name
The Iraqi Journal Of Veterinary Medicine
Selection of male goat embryos in vitro by using swim-up of epididymal spermatozoa: Sura Shakir Hammood Al-Dulaimi and Ihsan H. S. Al-Timimi
...Show More Authors

     The main objectives of this study is the separation of X from Y bearing epididymal spermatozoa of local buck by swim-up, and the use of this spermatozoa for in vitro fertilization to determine the percentage of produced male and female embryos. The sex of produced embryo was identified by polymerase chain reaction. Testis of the local buck were obtained from Al-Shu'alah abattoir and the epididymal spermatozoa were harvested from the cauda by and submitted to in vitro maturation prior to separation of X from Y bearing spermatozoa and prior to their use for in vitro fertilization. For the separation of epididymal spermatozoa, swim-up technique was used with centrifugation at 200×g or 300

... Show More
View Publication Preview PDF
Crossref
Publication Date
Sun Jun 01 2014
Journal Name
Baghdad Science Journal
Antiamoebic activity of extracted alkaloids of Capparis spinosa in Laboratory mice
...Show More Authors

The current study was concerned with the effect of alkaloid extract of the aerial parts of Capparis spinosa against Entamoeba histolytica and compared with drug Metronidazole in the laboratory mice .Stool samples were collected from people infected with maebiasis to infect laboratory mice . The alkaloid compounds were separated by thin chromatography technique (TLC) and identified by spectral methods represented by spectral infrared (IR) and altraviolate (UV) . the stady include determining mid-term lethal dose LD50 of the extract as the concentration was 21.65 g / kg . The effect dose of the extract was tested on the infected experimental mice with Entamoeba histolytica after 10 days of the infection compared with the mice infected

... Show More
View Publication Preview PDF
Crossref
Publication Date
Thu Dec 31 2020
Journal Name
College Of Islamic Sciences
القصدية في اللغة العربية بين الدراسات القديمة والحديثة: القصدية : قديما و حديثا
...Show More Authors

معيار القصديَّة في النص هو من الدراسات الحديثة المتطورة من لسانيات الجملة الى لسانيات النص ، وتحليل الخطاب . والذي يعنى بالطرق والأدوات التي يستغلها المؤلف لتحقيق الغايات المقصديَّة 

وهذا البحث ناقش مفهوم(القصديَّة) لغةً ،واصطلاحاً . فاللغة والكلام شكل من أشكال الوجود الإنساني و( الكلام) هو وسيلة التواصل بين الملقي القارئ ، والمتلقي  السامع ؛ وللتوصل الى الدلالة القصديَّة الدقيقة للغة المنطوقة وا

... Show More
View Publication Preview PDF
Publication Date
Sun Dec 05 2010
Journal Name
Baghdad Science Journal
Effect of parasites on the of digestive system in Iraqi bulbul Pycnonotus lecuotis mesoptamiae
...Show More Authors

This study included collecting of 150 specimens of the Iraqi Bird Bulbule Pycnonotus lecuotis mesoptamiae (Pycnotidae , Passeriformes), from the 1st of November 2004 to 30th of October 2005 in the city of Baghdad and its suburbs, in concern of identifying the internal parasite of the digestive tract of these birds and studying the diseases resulted from the infection. The study showed that the bird Bulbule is Parasitized by Four types of Cestodes ,two of them are recorded in this kind of bird in Iraq for the first time ,Paradicranotinae anormalis and Haploparaxis sp. , and the other two are Raillietina tetragona and Allohymenolepsis sp. ,and by two types of Pin Worm(Trematode) that are identified for the first time in the Bird Bulb

... Show More
View Publication Preview PDF
Crossref (1)
Crossref
Publication Date
Tue Dec 30 2008
Journal Name
Al-kindy College Medical Journal
Evaluation of Patients with Liver Injuries Treated by Perihepatic Gauze Packing
...Show More Authors

Background: The liver is one of the most common organs
injured after blunt abdominal trauma. The control of severe
hemorrhage remains a problem.
Methods: One-hundred thirty-eight patients diagnosed as
liver injury between 09/2003 and 08/2006 had been evaluated
prospectively in Al- Kindy Teaching Hospital.
A distinction was made between hemodynamically stable and
unstable patients. Different modalities of surgical procedures
were done concentrating on perihepatic gauze packing.
Results: (60 out of 138) patients included in the study were
clinically evaluated as hemodynamically stable. The average
abbreviated injury severity score (ISS) was 25. Twenty
patients underwent abdominal surgery. In 12 of them

... Show More
View Publication Preview PDF
Publication Date
Sat Sep 28 2019
Journal Name
Journal Of Physical Education
وضع مستويات معيارية لبعض القياسات الجسمية للاعبات الدوري العراقي الممتاز بالكرة الطائرة
...Show More Authors

تكمن أهمية البحث في وضع درجات ومستويات معيارية لبعض المتغيرات الجسمية للاعبات الدوري العراقي الممتاز بالكرة الطائرة , أما مشكلة البحث فتتلخص بعدم وجود درجات ومستويات معيارية يمكن الاعتماد عليها لتحديد القياسات الجسمية الخاصة بلاعبات الكرة الطائرة في العراق, ويهدف البحث الى التعرف على مستوى بعض القياسات الجسمية ووضع درجات ومستويات معيارية لها, وتم اختيار المنهج الوصفي بالاسلوب المسحي لملائمته وموضع الدر

... Show More
View Publication Preview PDF
Crossref
Publication Date
Mon Jun 01 2015
Journal Name
Journal Of Economics And Administrative Sciences
The phenomenon of negative behavior has studied as a social and psychological phenomenon that effect on the performance and life of workers inside and outside the organization. The adoption of this phenomenon is studied in terms of the role of the interna
...Show More Authors

The phenomenon of negative behavior has studied as a social and psychological phenomenon that effect on the performance and life of workers inside and outside the organization. The adoption of this phenomenon is studied in terms of the role of the internal environment of the organization in addressing this behavior, being the variables belong to the field of organizational behavior to see the results of those variables on the Iraqi organizations, since the specificities of it differ from the rest of the Arab and foreign environments. Therefore, this study focused on testing the relationship of the internal environment of the organization and its role in addressing the negative behavior of the workers.

thi

... Show More
View Publication Preview PDF
Crossref
Publication Date
Fri Apr 12 2019
Journal Name
Journal Of Economics And Administrative Sciences
The Impact of Six Thinking Hats Strategy on Improving Creative Thinking Skills" Field research in the Medical City "
...Show More Authors

Abstract  

   The research problem focuses on studying the interest of the Medical City Department of the Ministry of Health in improving the creative thinking skills of the administrative leadership through parallel & comprehensive thinking according to the of six thinking hats strategy. The research sample consisted of (170) administrative leaders in the upper & middle organizational levels, The questionnaire was used as a main tool for data collection, In addition to the observation & Interview, The research sought to answer the following questions: What is the extent to which the administrative leadership (Tpp & middle) in the organization investigated the concept of the six thinkin

... Show More
View Publication Preview PDF
Crossref
Publication Date
Sun Jan 01 2012
Journal Name
Journal Of The College Of Languages (jcl)
NEW PERSPECTIVES ON SHAKESPEAR'S "THE TEMPEST"
...Show More Authors

         This paper is mainly concerned with the study of the moral aspects that prompts William Shakespeare to attempt a romance in which he has embedded the epitome of his thought, experience, and philosophy concerning certain significant aspects of human life whose absence or negligence may threaten human existence, peace, and stability. From the beginning of history man realizes the importance of prosperity on the many and various levels that touch and address his needs and desires—natural, material,  and spiritual. The Tempest, due to the dramatist's awareness of the aforementioned values, reflects the dramatist's duty as to projecting and unfolding these important aspects, rec

... Show More
View Publication Preview PDF
Publication Date
Sat Dec 31 2022
Journal Name
Al-kindy College Medical Journal
Changing the Trends in Surgery during the COVID-19 Times: An Experience from the Eastern Uttar Pradesh State, India: CHANGING TRENDS IN SURGERY DURING COVID TIMES
...Show More Authors

Background: The COVID-19 pandemic has an immense effect not only on the social and economic lives of people but also on the surgical lives of surgeons, residents, nursing staff, and patients as well as ground level staff. Amidst this COVID pandemic, emergency surgeries were being done but at a decreased rate, whereas elective cases depended on the will of hospitals, surgeons, and patients. Study aims to promulgate a "Neo–Surgical Check Box" by amalgamating the WHO surgical checklist and the results obtained from the questionnaires.

Subjects and Methods: After receiving ethical clearance from the Institute Ethical Committee, an online questionnaire with 50 questions divided into

... Show More
View Publication Preview PDF
Crossref
Publication Date
Sat Oct 01 2016
Journal Name
Journal Of Economics And Administrative Sciences
The impact of leadership styles in the crisis management center the Strategic planning - Field research in the Headquarters Ministry of electricity
...Show More Authors

Abstract

The current research aims to testing the impact of leadership styles (autocratic, democratic) in crises management (Making decision response, communications and information flows, Mobilization of resources) through strategic planning (Mission, objectives, and environmental analysis, and strategic choice) among managers of the Iraqi Ministry of electricity. Questionnaire has been adopted as a tool in data and information relating to research, as it had prepared on the basis of number of scales and finished using the included Likert quintet, which  has been subjected to standards of validity and reliability and distributed to a sample consisting of (96) managers at the three departments of Min

... Show More
View Publication Preview PDF
Crossref
Publication Date
Sun Jun 15 2025
Journal Name
Iraqi Journal Of Laser
Highly Sensitive Refractive Index Sensor Based on Dual Peak Plasmonic Tapered D-shaped PM-PCF Coated with Gold Nano-Structures
...Show More Authors

his paper uses the finite element method (FEM) to study a Surface Plasmon Resonance (SPR) refractive index sensor based on D-shaped Polarization Maintain Photonic Crystal Fiber (PM-PCF). A chemically stable plasmonic material, gold (Au), with hemispherical structures having a radius of 50 nm, is applied to the surface of a D-shaped sensor to create the surface plasmon resonance (SPR) effect, enabling this SPR sensor to detect variation in the surrounding analyte refractive index (RI). The resonance condition will change when the refractive index of the targeted analyte changes, leading to a certain shift in the loss peak. Two resonant peaks are observed, one located in the visible part of the spectrum, and the second in the near-infrared

... Show More
View Publication Preview PDF
Publication Date
Tue Sep 08 2020
Journal Name
Baghdad Science Journal
Improved throughput of Elliptic Curve Digital Signature Algorithm (ECDSA) processor implementation over Koblitz curve k-163 on Field Programmable Gate Array (FPGA)
...Show More Authors

            The widespread use of the Internet of things (IoT) in different aspects of an individual’s life like banking, wireless intelligent devices and smartphones has led to new security and performance challenges under restricted resources. The Elliptic Curve Digital Signature Algorithm (ECDSA) is the most suitable choice for the environments due to the smaller size of the encryption key and changeable security related parameters. However, major performance metrics such as area, power, latency and throughput are still customisable and based on the design requirements of the device.

The present paper puts forward an enhancement for the throughput performance metric by p

... Show More
View Publication Preview PDF
Scopus (3)
Crossref (3)
Scopus Clarivate Crossref
Publication Date
Thu Apr 24 2025
Journal Name
Iraqi Journal Of Agricultural Sciences
CHARACTERIZATION OF NOVEL EDIBLE FILM FROM DEAMIDATED RICE (Oryza sativa) BRAN PROTEIN
...Show More Authors

This study aimed to investigate the characteristics of   new edible film prepared from deamidated rice bran protein (RBP). Deamidation was carried out at temperatures of 80, 100, and 120°C under varying pH conditions of 8, 10, and 12 for durations of 15 and 30 minutes to enhance protein solubility. The resulting film was then assessed for its physical, mechanical, and optical properties. The results revealed that protein solubility of deamidated RBP improved across all temperatures and pH levels compared to the control. A film made from deamidated protein under conditions of 120°C and pH levels of 8, 10, and 12 was evaluated using protein concentrations of 3, 4, and 5%. The solubility

... Show More
View Publication Preview PDF
Publication Date
Thu Dec 29 2011
Journal Name
The Iraqi Journal Of Veterinary Medicine
The rapid detection of E. coli 0157 Antigen in meat products by using ELISA Test Kit
...Show More Authors

This study was conducted for rapid detection of contamination of meat products with E. coli 0157 by usage of ELISA test kit as one of the most rapid and newest test. The study showed the efficiency of ELISA test kit used in this study in detection of bacteria antigen in meat products samples of raw beef meat , kabab and beef burger which subjected to improper storage conditions or undercooked and hence when some peoples uptake some of these products they suffered from clinical intoxication signs like diarrhea ,vomiting and hyperthermia. The kit showed the presence of (9) samples positive among (90) samples ; (2) positive out of (30) kabab samples,(3) positive out of (30) beef burger and (4) positive out of (30) raw beef meat after 16 hrs

... Show More
View Publication Preview PDF
Crossref
Publication Date
Sat Dec 30 2023
Journal Name
Iraqi National Journal Of Nursing Specialties
فاعلية البرنامج التعليمي في معارف الممرضين حول استخدام القيود الجسدية للمرضى في وحدة العناية الفائقة
...Show More Authors

الهدف: تقويم فاعلية البرنامج التعليمي في معارف الممرضين حول استخدام القيود الجسدية للمرضى في وحدة العناية الفائقة.

 المنهجية: أجريت دراسة شبه تجريبية على عينة هادفة (غير احتمالية) من ٤٠ ممرض وممرضة يعملون في وحدة العناية الفائقة في مستشفى الناصرية التعليمي من تاريخ اليوم السابع من شهر كانون الثاني لسنة ٢٠٢٣ الى اليوم الثامن من شهر شباط لسنة ٢٠٢٣. تم إعداد برنامج تعليمي وتقديمه إلى المم

... Show More
View Publication Preview PDF
Publication Date
Wed Mar 30 2011
Journal Name
Iraqi Journal Of Chemical And Petroleum Engineering
ESTIMATION OF MASS TRANSFER COEFFICIENTS IN A PACKED DISTILLATION COLUMN USING BATCH MODE
...Show More Authors

This research adopts the estimation of mass transfer coefficient in batch packed bed distillation column as function of physical properties, liquid to vapour molar rates ratio (L / V), relative volatility (α), ratio of vapour and liquid diffusivities (DV / DL), ratio of vapour and liquid densities (ρV / ρL), ratio of vapour and liquid viscosities (μV/ μL).
The experiments are done using binary systems, (Ethanol Water), (Methanol Water), (Methanol Ethanol), (Benzene Hexane), (Benzene Toluene). Statistical program (multiple regression analysis) is used for estimating the overall mass transfer coefficient of vapour and liquid phases (KOV and KOL) in a correlation which represented the data fairly well.

KOV = 3.3 * 10-10

... Show More
View Publication Preview PDF
Publication Date
Sat Jun 30 2018
Journal Name
College Of Islamic Sciences
Narrative narration in the poetry of Mohammed Abdul Muttalib   (Top poem as a model)
...Show More Authors

Poets of the age since ancient times to recount the events of their adventures in a fun story style in which the elements of the story of personalities, time and place, and we do not mean this modern art technique (poetic story) as it is now, but was aimed at the pleasures of the other receiving because it is the rule of the quality of literary output, Other times the narrative of events inspired by his broad imagination and this mixing indicates the story's involvement with Arabic poetry to be (poetic story) and this depends entirely on addressing the poet to the recipient, and requires in this narrative to be familiar with the elements of influence and suspense in the other or turned into a monotonous and dull narrative Influential, un

... Show More
View Publication Preview PDF
Publication Date
Sun Dec 02 2007
Journal Name
Political Sciences Journal
سياسات الاتحاد الاوروبي والولايات المتحدة الامريكية تجاه ازمة الشرق الاوسط بعد الحادي عشر من ايلول
...Show More Authors

سياسات الاتحاد الاوروبي والولايات المتحدة الامريكية تجاه ازمة الشرق الاوسط بعد الحادي عشر من ايلول

View Publication Preview PDF
Crossref
Publication Date
Tue Jan 20 2026
Journal Name
Ibn Al-haitham Journal For Pure And Applied Sciences
Functionalization of N-H Linkage at Benzimidazole for the Construction of 1,3,4-Oxadiazole Derivatives
...Show More Authors

Benzimidazole is a bicyclic heterocyclic aromatic compound that contains a combination of a six-membered ring and a five-membered ring with two nitrogen atoms. The current study aims to combine these two moieties to identify new benzimidazole-based 1,3,4-oxadiazole derivatives. In this work, the preparation of new benzimidazole-containing substituted 1,3,4-oxadiazoles 3-16 has been described using a five-step process. The SN2 displacement reaction between benzimidazole and bromoacetic acid afforded the corresponding acid 1 in an 87% yield. Product 1 was treated with thionyl chloride to furnish the desired acid chloride form of 1. The next step involved the nucleophilic addition of hydrazine hydrate (99%) to the acid chloride d

... Show More
View Publication Preview PDF