In this study, new heterocyclic compounds were synthesized through the cyclization reactions of o-phenylenediamine (1) with various organic reagents. Benzodiazepine derivatives (2-4) were obtained by reaction of (1) with ethylacetoacetate, malonic acid and acetyl acetone.Treatment of compound (1) with chloroacetamide, chloroacetic acid, p-bromophenacyl bromide and oxalic acid dihydrate afforded quinoxaline derivatives (5-8), respectively. Reaction of compound (1) with benzoic acid, piperonal, cyclohexanone and carbon disulfide resulted in the formation of compounds (9-12), respectively. Finally, reaction of compound (12) with chloroacetic acid in the presence of potassium hydroxide produced compound (13).
Low back pain a major causes of morbidity throughout the world and it is a most debilitating condition ,and can lead to decreased physical function ,compromised quality of life, and psychological distress. Obesity is nowadays a pandemic condition. Obese subjects are commonly characterized by musculoskeletal disorders and particularly by non-specific LBP. However, the relationship between obesity and LBP remain to date unsupported by objective measurements of mechanical behavior of spine and it is morphology in obese subjects. Key words: obesity, low back pain,
This paper aimed to investigate the effect of the height-to-length ratio of unreinforced masonry (URM) walls when loaded by a vertical load. The finite element (FE) method was implemented for modeling and analysis of URM wall. In this paper, ABAQUS, FE software with implicit solver was used to model and analysis URM walls subjected to a vertical load. In order to ensure the validity of Detailed Micro Model (DMM) in predicting the behavior of URM walls under vertical load, the results of the proposed model are compared with experimental results. Load-displacement relationship of the proposed numerical model is found of a good agreement with that of the published experimental results. Evidence shows that load-displacement curve obtained fro
... Show MorePlagiarism is becoming more of a problem in academics. It’s made worse by the ease with which a wide range of resources can be found on the internet, as well as the ease with which they can be copied and pasted. It is academic theft since the perpetrator has ”taken” and presented the work of others as his or her own. Manual detection of plagiarism by a human being is difficult, imprecise, and time-consuming because it is difficult for anyone to compare their work to current data. Plagiarism is a big problem in higher education, and it can happen on any topic. Plagiarism detection has been studied in many scientific articles, and methods for recognition have been created utilizing the Plagiarism analysis, Authorship identification, and
... Show Moreيختص البحث بدراسة مرحلة زمنية مهمة من تاريخ العراق الحديث، وهي المدة الخاصة بتأسيس العراق الحديث واستقلاله من خلال انتهاء الانتداب البريطاني وقبول انضمامه الى عصبة الامم تلك المنظمة الدولية التي تضم في عضويتها الدول الحرة المستقلة والتي اخذت على عاتقها اقامة الامن والسلم العالمي من خلال اقرار مبدأ تحريم استخدام القوة واقرار مبدأ حل الخلافات الدولية بالطرق السلمية، يهدف البحث الى تحقيق مجموعة من الاهد
... Show MoreThis research was distributed into two sections, the first section was concerned with the concept of value for De Saussair and its methodological impact on his linguistic structural conceptions with respect of the distinction between synchronism and diachronism, the value role of linking function between the sounds and the though, the basing of his theoretical conception on the language being a form and not a material according to this principle and the value impact on the demonstration that the linguistic element acquires its functional importance from the relations inside the language system. It also stopped at the methodological impact of value on defining the analytical linguistic unit and the value role in semantics through the prin
... Show MoreIn literary criticism, both the context and the content of a given text; speech, graph, image, or picture are essential. It is the totality of these two elements that pave the way for a better understanding of any given text. Hence, since the purpose of every communication or speech act is comprehension, this study examines the stylistic profile of Wole Soyinka and Jean Pliya in The Lion and the Jewel (1964) and La secrétaire particulière (2001) respectively. The study adopts the French ‘explication de texte’ technique as its methodology to carry out a textual analysis of the two selected plays. As a theoretical framework, the study uses Edward Said and Homi Bhabha’s Postcolonial theory which interrogat
... Show Moreهدف البحث إلى التعرف على الانكسار النفسي فضلاً عن التعرف على الفروق في الانكسار النفسي بين الطلبة على وفق متغير الجنس (ذكر – انثى) والمرحلة الدراسية (أول- رابع)، تألفت عينة البحث من (120) طالبا وطالبة من طلبة الجامعة، وتم تطبيق مقياس البحث - مقياس (الانكسار النفسي) وهو (من إعداد الباحثة)، وقد اسفرت نتائج البحث عن: - إن طلبة الجامعة ليس لديهم انكسار نفسي. - عدم وجود فروق في الانكسار النفسي على وفق متغير الجنس أو متغير
... Show Moreتهدف الدراسة إلى تتبع موقف أئمة الإباضية والعلماء من الخلاف المتعلق بقضية عزل الإمام الصلت بن مالك الخروصي سنة (272هـ/885م)، والوقوف على محاولات وقف الخوض في ذلك الخلاف، وبيان أبرز الاجتماعات التي دعى إليها الأئمة والعلماء وما أفضت إليه من نتائج. تتضمن الدراسة خمسة مباحث رئيسة، يتناول المبحث الأول: التعريف بقضية عزل الإمام الصلت بن مالك الخروصي وموقف موسى بن موسى الإزكوي وراشد بن النظر اليحمدي منها، وخُصص المب
... Show Moreتعد السهام احدى اسلحة المعارك في حضارة بلاد الرافدين، وكان لها دورا كبيرا في تحقيق الانتصارات في الحروب، وقد زودتنا النصوص المسمارية بمعلومات قيمة ومتنوعة ومهمة حول السهام وتسمياتها والتسميات المتعلقة بها وماهيتها فضلا عن الجوانب الاخرى التي تتعلق بالسهام والتي لا ترتبط بالبعد العسكري بل بالابعاد الدينية وارتباط السهام بفكر ومعتقد سكان بلاد الرافدين من خلال ارتباطها بالإلهة والمعابد والطقوس وغير
... Show MoreThe present study aimed to determine the serum sex hormone levels among Benign Prostatic Hyperplasia (BPH) patients before and after 3 months of oral administration of 5-α reductase inhibitor(finasteride). Forty BPH patients and 40 healthy men from Amara city were involved in this study, their ages were between 40-59 year. They were all subjected to direct estimation of hormones by MinVidas method including Testosterone (T), Estradiol (E2), Follicle Stimulating Hormone (FSH), Luteinizing Hormone (LH), Prolactin (PRL), and Dihydrotestosterone (DHT) before and after 3 months of treatment with 5α-reductase inhibitor (finasteride) (the healthy individuals didn’t take finasteride).The results showed that T level was significantly lo
... Show MoreThis paper identifies and describes the textual densities of ideational metaphors through the application of GM theory (Halliday, 1994) to the textual analysis of two twentieth century English short stories: one American (The Mansion (1910-11), by Henry Jackson van Dyke Jr.), and one British (Home (1951), by William Somerset Maugham). One aim is to get at textually verifiable statistical evidence that attests to the observed dominance of GM nominalization in academic and scientific texts, rather than to fiction (e.g. Halliday and Martin (1993). Another aim is to explore any significant differentiation in GM’s us by the two short- story writers. The research has been carried out by identifying, describing, and statisti
... Show MoreThis research aims to investigate parameters for magnesium (Mg) carbon (C), and carbon/magnesium plasma produced by the exploding electrical wire (EEW) technique. In this work, C and Mg nanoparticles were synthesized. The plasma spectra with three different current values (50, 75 and 100A) were recorded using optical emission spectroscopy (OES). The plasma electron temperature (Te), electron density (ne), plasma frequency (fp), Debye length (ℷD), and Debye number (ND) provided by arc discharge plasma were calculated. Boltzmann plots were used to calculate the electron temperature (Te); electron density (ne) was calculated by Stark broadening . The results showed that the electron temperature and electron density increa
... Show Moreيهدف البحث الى تحليل واقع التوزيع المكاني للأنشطة الصناعية المتوسطة ، وتعرف على اهميتها على صعيد المحافظات العراقية وتحليل الانماط المكانية للتباين الاقليمي وخصائصه في التوطن الصناعي والتنوع فضلاً عن قياس وتحليل اثر عوامل الإنتاج على إنتاجية العمل فيها. تتمثل مشكلة البحث في وجود خللٍ في بنيان القطاع الصناعي العراقي لعدم وجود قطاع صناعيًّ متوسط الحجم يتناسق مع حجوم المشروعات الصناعية الصغيرة و
... Show MoreIn this paper an eco-epidemiological system has been proposed and studied analytically as well as numerically. The boundedness, existence and uniqueness of the solution are discussed. The local and global stability of all possible equilibrium point are investigated. The global dynamics is studied numerically. It is obtained that system has rich in dynamics including Hopf bifurcation.
الدولة الفاطمية التي قامت في بلاد المغرب الأدنى وتوسعت إلى المشرق وحتى إلى جنوب أوربا في الأندلس إي إسبانيا والبرتغال وجزر البحر المتوسط وأصبحت دولة مترامية الأطراف بفضل الجهد الذي قام به الخلفاء الفاطميين من نشر مذهب أهل البيت العلوي . مما حدا بتلك الدولة أن تصبح في أقل من قرن واحد إمبراطورية كبيرة امتدت جذورها إلى أطراف من ممتلكات الخلافة العباسية القائمة في الشرق الإسلامي ، وكان ذلك الانتشار الكبير ناتج م
... Show MoreKey-frame selection plays an important role in facial expression recognition systems. It helps in selecting the most representative frames that capture the different poses of the face. The effect of the number of selected keyframes has been studied in this paper to find its impact on the final accuracy of the emotion recognition system. Dynamic and static information is employed to select the most effective key-frames of the facial video with a short response time. Firstly, the absolute difference between the successive frames is used to reduce the number of frames and select the candidate ones which then contribute to the clustering process. The static-based information of the reduced sets of frames is then given to the fuzzy C-Means algor
... Show MoreThe aim of this article is to study the solution of Elliptic Euler-Poisson-Darboux equation, by using the symmetry of Lie Algebra of orders two and three, as a contribution in partial differential equations and their solutions.
The provided research paper offers a thorough analysis of the semiotic analysis present in tobacco-free initiative advertisements from the year 2021. The study delves into the intricate process of decoding the diverse signs, symbols, and visual components integrated into these anti-smoking campaigns. The core aim of this investigation is to comprehend and explore the semiotic tactics that underlie these advertisements, with a particular emphasis on visual communication as a pivotal tool in shaping the public's attitudes and behaviors towards tobacco usage. The research introduces a significant theoretical framework, the "Taxonomy of Image-Text Relations and Functions" theory, as proposed by Emily E. Marsh and Marilyn Dom
... Show MoreThis paper discusses reliability of the stress-strength model. The reliability functions ð‘…1 and ð‘…2 were obtained for a component which has an independent strength and is exposed to two and three stresses, respectively. We used the generalized inverted Kumaraswamy distribution GIKD with unknown shape parameter as well as known shape and scale parameters. The parameters were estimated from the stress- strength models, while the reliabilities ð‘…1, ð‘…2 were estimated by three methods, namely the Maximum Likelihood, Least Square, and Regression.
A numerical simulation study a comparison between the three estimators by mean square error is performed. It is found that best estimator between
... Show MoreEmerge application was used in Hampsson-Russell programs and that uses a combination of multiple 3D or 2D seismic attributes to predict some reservoir parameter of interest. In this research used the seismic inversion technique was performed on post-stack three dimensions (3D) seismic data in Nasriya oilfield with five wells and then used this results in Emerge analysis (training and application) were used to estimate reservoir properties (effective porosity) with multiattribute analysis derive relations between them at well locations. The horizon time slice of reservoir units of (Yb1, Yb3 and Yc) of Yamama Formation was made for property (effective porosity) to confirm match results and enhancement trends within these
... Show MoreA colloidal indium oxide (In2O3) nanoparticles (NPs) were synthesized pulsed laser ablation (PLA) of indium plate placed on the bottom of the quartz vessel containing (3ml) of pure ethanol. The influence laser energy on the properties of the formed nano-particles were characterized by using atomic force microscopy (AFM), X-ray diffraction (XRD), Ultraviolet Visible (UV-Vis) technique, and electrical properties measurements. The XRD revealed the crystallization structure of In2O3 nanoparticles and all the films having preferential orientation along (222) plane and intensity increases with increasing laser energy, The UV–Visible spect
... Show MoreThin films of the blended solution of NiPc/C60 are fabricated using spin-coating method for three different ratios (100/1, 100/10 and 100/100) according to the weight. The films are deposited on to glass substrates and treated with several annealing temperatures (373, 423 and 473)K. The structure and surface morphology of the as-deposited and annealed films using x-ray diffraction and AFM was studied and exhibited a change and enhanced crystallization and surface morphology caused by changes in heat treatment temperatures. Investigation of X-ray diffraction patterns of NiPc/C60 indicated that it have polymorphism structure, i.e. mix between amorphous and polycrystalline structure. when heat treatment temperatures ch
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