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Synthesis, Spectroscopic and Adsorption Studies of Cobalt (II) Complex for a ligand β-enaminone Derived from Sulfamethoxazole

This paper concerns is the preparation and characterization of a bidentate ligand [4-(5,5- dimethyl-3-oxocyclohex-1-enylamino)-N-(5-methylisoxazol-3-yl) benzene sulfonamide]. The ligand was prepared from fusing of sulfamethoxazole and dimedone at (140) ºC for half hour. The complex was prepared by refluxing the ligand with a bivalent cobalt ion using ethanol as a solvent. The prepared ligand and complex were identified using Spectroscopic methods. The proposed tetrahedral geometry around the metal ions studied were concluded from these measurements. Both molar ratio and continuous variation method were studied to determine metal to ligand ratio (M:L). The M to L ratio was found to be (1:1). The adsorption of cobalt complex was carried out using bentonite as adsorbent. The optimization of the adsorption conditions were studied as a function of contact time , temperature , pH , adsorbent weight and particle size. The results revealed that the time needed to reach concentration equilibrium was 60 min for cobalt complex. While the trend of the adsorption isotherm was L1 type according to Giles classification . Thermodynamic functions (ΔH, ΔG, and ΔS) were calculated.

Publication Date
Sat Dec 30 2023
Journal Name
Iraqi Journal Of Science
New Generalizations for Ϻ-Hyponormal Operators

     This article contains a new generalizations of Ϻ-hyponormal operators which is namely (Ϻ,θ)-hyponormal operator define on Hilbert space H.  Furthermore, we investigate some properties of this concept such as the product and sum of two (Ϻ, θ)-hyponormal operators, At the end the operator equation  where  ,  has been used for getting several characterization of (Ϻ,θ)-hyponormal operators.  

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Publication Date
Sun Jan 01 2017
Journal Name
Australian Journal Of Basic And Applied Sciences
Proposed Algorithm for Gumbel Distribution Estimation

Gumbel distribution was dealt with great care by researchers and statisticians. There are traditional methods to estimate two parameters of Gumbel distribution known as Maximum Likelihood, the Method of Moments and recently the method of re-sampling called (Jackknife). However, these methods suffer from some mathematical difficulties in solving them analytically. Accordingly, there are other non-traditional methods, like the principle of the nearest neighbors, used in computer science especially, artificial intelligence algorithms, including the genetic algorithm, the artificial neural network algorithm, and others that may to be classified as meta-heuristic methods. Moreover, this principle of nearest neighbors has useful statistical featu

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Publication Date
Sun Jul 02 2023
Journal Name
Iraqi Journal Of Science
Performance Improvement for Wireless Sensor Networks

In this paper, we prove that our proposed localization algorithm named Improved
Accuracy Distribution localization for wireless sensor networks (IADLoc) [1] is the
best when it is compared with the other localization algorithms by introducing many
cases of studies. The IADLoc is used to minimize the error rate of localization
without any additional cost and minimum energy consumption and also
decentralized implementation. The IADLoc is a range free and also range based
localization algorithm that uses both type of antenna (directional and omnidirectional)
it allows sensors to determine their location based on the region of
intersection (ROI) when the beacon nodes send the information to the sink node and
the la

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Publication Date
Wed May 17 2017
Journal Name
Ibn Al-haitham Journal For Pure And Applied Sciences
Multiproduct Mathematical Model for Productive Company

This model is an extension to H.M.M.S and related developments models of a single product. These models will be converted to deal with Multiproduct for productive company. This model executed by computer programming technique to maximize profits

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Publication Date
Sat Dec 31 2011
Journal Name
Al-khwarizmi Engineering Journal
Path Planning Control for Mobile Robot

Autonomous motion planning is important area of robotics research. This type of planning relieves human operator from tedious job of motion planning. This reduces the possibility of human error and increase efficiency of whole process.

This research presents a new algorithm to plan path for autonomous mobile robot based on image processing techniques by using wireless camera that provides the desired image for the unknown environment . The proposed algorithm is applied on this image to obtain a optimal path for the robot. It is based on the observation and analysis of the obstacles that lying in the straight path between the start and the goal point by detecting these obstacles, analyzing and studying their shapes, positions and

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Publication Date
Fri Dec 29 2017
Journal Name
Ibn Al-haitham Journal For Pure And Applied Sciences
Risk Factors For Unintentional Childhood Poisoning

Objectives:   To   identify   child  or  family  related  risk  factors   for

unintentional childhood  poisoning in Sulaymaniyah, Iraq  and to suggest

possible causes and preventive measures.

Methods: This is an epidemiological description and a case-control study. The study was undertaken in Sulaymani ,in 2004-2005. Cases were 200 children who were admitted to the hospital for treatment of poisoning. For every case two controls  were selected. Al l   parents of the children were interviewed  by  using a  questionnaire  that  incl uded  demographic  and poisoning characteristic information.<

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Publication Date
Tue Dec 21 2021
Journal Name
Journal Of Legal Sciences
International protection for human rights activists

Despite the primary role of governments in assuming the primary responsibility in protecting human rights in accordance with international human rights standards and instruments, they are not the only party responsible for ensuring the implementation of those rights. Individuals themselves have a duty towards their society to observe, respect and promote those rights and freedoms and work to protect them by means. All, and this is confirmed by Paragraph (1) of Article (29) of the Universal Declaration of Human Rights of 1948, which states: “Every individual has duties towards the society in which it is only possible for his personality to grow freely and fully.            &nbs

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Publication Date
Sun Apr 30 2023
Journal Name
Iraqi Journal Of Science
Semigroup Theory for Dual Dynamic Programming

In this paper, the nonclassical approach to dynamic programming for the optimal control problem via strongly continuous semigroup has been presented. The dual value function VD ( .,. ) of the problem is defined and characterized. We find that it satisfied the dual dynamic programming principle and dual Hamilton Jacobi –Bellman equation. Also, some properties of VD (. , .) have been studied, such as, various kinds of continuities and boundedness, these properties used to give a sufficient condition for optimality. A suitable verification theorem to find a dual optimal feedback control has been proved. Finally gives an example which illustrates the value of the theorem which deals with the sufficient condition for optimality.

<

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Publication Date
Mon Apr 01 2019
Journal Name
Journal Of Legal Sciences
International criminal Responsibility for terrorist crimes

   This research is entitled "International criminal Responsibility for terrorist crimes". Individuals bear the international criminal responsibility for supporting terrorist crimes, whatever their status, whether they are ordinary persons, heads of state or state officials. They could be prosecuting through national or international courts. Although terrorist crimes are not mentioned in the Statute of the International Criminal Court, terrorist groups may be prosecuting before the International Criminal Court when they commit international crimes within the jurisdiction under the Statute of this court, i.e., genocide, crimes against humanity or war crimes. Leaders and officials of States that support terr

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Publication Date
Mon Apr 20 2020
Journal Name
Ibn Al-haitham Journal For Pure And Applied Sciences