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This work concerned on nanocrystalline NiAl2O4 and ZnAl2O4 having spinel structure prepared by Sol–gel
technique. The structural and characterization properties for the obtained samples were examined using
different measurements such as X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR),
finally, Field emission scanning electron microscope (FESEM).The Spinel-type for two prepared compound
(NiAl2O4) and (ZnAl2O4) at different calcination temperature examined by XRD. Williamson-Hall Methods
used to estimate crystallite size, Average distribution crystallite size of two compound were, 34.2 nm for
NiAl2O4 and32.6 for ZnAl2O4, the increase in crystallite size affecting by increasing in calcination
temperature for both comp
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