This research includes the synthesis of new series of heterocyclic compounds. Reaction of 2-nitro benzylidene)thiosemicarbazide(1) with ethyl chloro acetate gave (2-nitro benzylidene amino)-2-thioxomidazolidine-4-one(2) ,treatment(2) with methyl iodide to give(3)which was reacted with hydrazine to give 2-hydrazinyl-1-[(2-nitrobenzylidene)amino]- 1H-imidazol-5(4H)-one, andreation of compound(2) with aromatic aldehydes to give 5arylidene -3-({2-nitro benzylidene}amino)2-thioxo-3,5-dihydro-4H-imidazole-4-one(5a,5b), which was reacted with ethyl aceto acetate to give 4-aryl-1-[2-nitrobenzylidene, amino -6oxo-2-thioxo octa hydro-1H-benzo[d]imidazole-5-carboxylate and followed synthesis of βlactamederivtives(9a,9b) by treatment derivatives(

   This paper concerns is the preparation and characterization of a bidentate ligand [4-(5,5dimethyl-3-oxocyclohex-1-enylamino)-N-(5-methylisoxazol-3-yl) benzene sulfonamide].  The ligand was prepared from fusing of sulfamethoxazole and dimedone at (140) ºC for half hour.              The complex was prepared by refluxing the ligand with a bivalent cobalt ion using ethanol as a solvent. The prepared ligand and complex were identified using Spectroscopic methods. The proposed tetrahedral geometry around the metal ions studied were concluded from these measurements. Both molar ratio and continuous variation method were studied to determine metal to ligand ratio (M:L). The M to L ratio wa

Mn(II), Co(II), Ni(II), Cu(II), and Cr(III) metal complexes with the ligand (L) [3-(2nitro benzylidene) amino-2-thioxoimidazolidin-4-one] have been prepared and characterized in their solid state using the elemental micro analysis (C.H.N.S), flame atomic absorption, UV-Vis spectroscopy, FT-IR, magnetic susceptibility measurements, and electrical molar conductivity. The ratio of metal to ligand [M:L] was got for all complexes in the ethanol by using the molar ratio method, which produced comparable results with those results obtained for the solid complexes. From the data of all techniques, octahedral geometry was proposed for Cr(III), Mn(II), and Co(II) complexes, while tetrahedral structure was proposed for Ni(II), Cu(II) complexes.

The results indicated that the biofilm formed by each Staphylococcus haemolyticus isolate was inhibited by 52%–82%. The highest value of biofilm formation (before treatment) was seen in the case of isolate A39, followed by A49 with absorption values of (1.382 and 1.116), respectively. Bacterial cells are capable of catalyzing the biosynthesis process by producing reductive enzymes. These green synthesized inorganic nanoparticles have been frequently investigated as possible bactericidal agents. Our findings revealed that at sub-Minimum Inhibitory Concentration (Sub-MIC), Copper oxide nanoparticles and Vancomycin combinations showed remarkable biofilm inhibitory outcomes in wild-type strains of Staphylococcus haemolyticus <

There is a desperate need for extended versions of the classical distributions. There have been attempts to find novel families of probability distributions that widen existing families and provide great flexibility in data modeling in a number of application areas, including lifetime analysis, finance, and insurance. In this paper, we introduce a new family of distributions based on [0,1] Truncated and propose a new extension for the exponential distribution. The new distribution is called Truncated Nadarajah-Haghighi Distribution, symbolized with {[0,1]TNHE}. This study aims to derive some statistical properties for the new distribution, such as the quantile function, the mixture representation for the probability density function, the

Irisin is a myokine that controls energy metabolism by making adipose tissue brown. The present goal in doing this research was to determine how irisin concentration relates to other biochemical markers of disease. Hemodialysis (HD) for chronic kidney failure. The study included 30 individuals with end-stage renal disease on HD and 30 healthy subjects as the control group. The ages of all patients and the control group ranged from (25 to 60) years. The excluded criteria included patients with viral hepatitis and diabetes. Serum irisin concentration and the level of fasting serum glucose (FSG), urea, creatinine (Cr), total protein (TP), albumin (Alb), albumin to creatinine ratio (ACR), total cholesterol (TC), alanine aminotransferase (ALT

Polycystic ovary syndrome (PCOS) is a significant cause of infertility due to ovulation dysfunction in women of childbearing age. Although the pathogenesis of PCOS is still not clear, many studies have shown that many factors within the ovary promote infection. With this syndrome, the disruption of the natural monthly ovulation process causes an imbalance in the body's hormones, and the high level of insulin in the body and the blood sugar imbalance leads to the occurrence of hyperandrogenism, which is the main factor for the occurrence of pathogens, in addition to genetic factors, if any. This study aims to identify this disease and its most important causes, symptoms, and modern treatments to prevent and get rid of it. Polycystic ovari

New complexes were synthesized from a newly prepared Schiff base ligand (L₂) derived from malonic acid dihydrizde and 2- pyridine carboxaldehyde. The ¹H-NMR and ¹³C-NMR spectra demonstrated all the needed peaks to prove the chemical structure of the synthesized ligand (L₂). Utilizing mass spectroscopy, the molecular ion peak was found at m/e 310, confirming the formula weight for L₂, which matches the estimated m+ value (310.12). Accordingly, its Mn (II) and Co (II) complexes were trainedusing glacial acetic acid as a catalyst. These compounds were characterized by FT-IR, UV-Vis, C.H.N., chloride-containing, molar conductance, magnetic susceptibility, and atomic absorption. The chara

Due to high blood sugar over long periods, the incidence and prevalence of type 2 diabetes are increasing throughout the world. Diabetic complications include microvascular and macrovascular complications that target the kidneys, nerves, eyes, and heart. Hence, the current study aimed to investigate the levels of (CTGF) and (TGF-β1) for both men and women and to demonstrate the effect of sex on it. In addition, some related biochemical factors in patients with diabetes and diabetic nephropathy are compared with those in healthy controls. The study included 120 males and females with an age range of (30-65) years old. Ninety patients with type 2 diabetes were subdivided into three groups on the basis of ACR criteria. All the individuals

Depending on the needs and requirements of keeping up with the scientific procession, researchers tend to find new recurrence schemes or develop previous recurrence schemes that will help researchers reach the fixed point and solution of variational inequality. This article aims to provide novel approaches to finding a common fixed point of different types of important mappings and the set of zeros of maximal monotone operators. Also, we studied the weak and strong convergence of the proposed iterative method under some suitable conditions. To achieve this goal, we will introduce a new technical method of resolvent operators and metric projection using different types of function sequences, including sequence of maximal monotone operator

Diazotization reaction between 1-(2,4,6-trihydroxy-phenyl)-ethanone and diazonium salts produced the ligand 4-(3-Acetyl-2,4,6-trihydroxy-phenylazo)-N-(5-methyl-isoxazol-3-yl)-benzenesulfonamide, which in turn reacted with the metal ions (Ni²⁺, Zn²⁺, Pd²⁺ and Pt⁴⁺) forming stable complexes with Octahedral geometry suggest of (Ni²⁺ and Pt⁴⁺), Zn²⁺ complex Tetrahedral and Pd²⁺ complex Square planer. The creation of such complexes was detected by employing spectroscopic means involving ultraviolet-visible, which proved the obtained geometries; FT-IR confirmed the formation of the azo group and the coordination with metal ions through it. Thermogravimetric

  The current study aimed to identify the histological structure of the lung in Iraqi weasels, Herpestes javanicus. The present study was conducted on 5 samples of weasel animals weighing between 288 and 564 g. The results of the study displayed that the trachea in Herpestes javanicus branches into two branches of the primary bronchi, which are similar in tissue structure to the trachea, and the results also showed that the primary bronchus branch out to be the secondary and tertiary intrapulmonary bronchus, as the cartilaginous rings turn into finger-shaped plates of hyaline cartilage and these cartilaginous plates disappear in the bronchioles, which in turn branch into the terminal bronchioles, which give a branch to

The set of all (n×n) non-singular matrices over the field F this set forms a group under the operation of matrix multiplication. This group is called the general linear group of dimension n over the field F, denoted by GL(n,F). The determinant of these matrices is a homomorphism from GL(n,F) into F* and the kernel of this homomorphism was the special linear group and denoted by SL(n,F). Thus SL(n,F) is the subgroup of GL(n,F) which contains all matrices of determinant one.
The rational valued characters of the rational representations written as a linear combination of the induced characters for the groups SL(2,17^2 ) discuss in this work and find the Artin indicator for this group after study the rational valued characters of the

 The present study aimed to investigate the morphological description and histological  structure of  thyroid gland in Herpestes javanicus . The results revealed that thyroid gland in adult Herpestes javanicus is located in the neck region just below the larynx and attached to the trachea . Histological study revealed that thyroid gland  in H. javanicus surrounded by a capsule of losse connective tissue and the thyroid gland mainly formed from follicles within different sizes. The results showed that the follicle consists of three compenets represented by follicular lining cells, basal parafollicular cells and the colloid. Microscopical examination revealed that the follicular lining  tissue is either to be simpl

 This article talks about a model of fractional differential equations to describe how COVID-19 is spread in the world in general and Iraq in particular. The model contains five fractional differential equations. Moreover, we have proven the existence and uniqueness of the solution of the model, found the equilibrium points of the model and checked its stability. Then we solved it using a fractional linear multi-step method. When we compare the results with the data documented by the World Health Organisation (WHO), we find that the total number of active cases in the world are equal to 584498294 on 3/8/2022, and it is similar to what was done with the system. The number of those who have recovered and died from the disease ha

This study aimed to explain the effect of the flavonoid extract of Cappairs Spinosa on the body weight, lipid profile, glucose, and kidney functions of male rats. We extracted the plant material using methanol at 85% in the Soxhlet apparatus for 8 hours and fractionated it with  ethyl acetate. Twenty adult male rats were used in this study, which was divided into four groups (5 rats/group); the first group (T1) received 10 mg/kg. The second group (T2) received 20 mg \kg.  The third group (T3) received 40 mg\kg orally for 30 days, and the 4^th group (control) received orally distal water. At the end of the experiment, we collected blood samples by cardiac puncture to measure blood sugar level, lipid profile, and kidney functi

Kidney stone disease is a highly significant clinical issue that poses a serious threat to both global health and the economy. For the sustainability of good health and well-being of kidney stone patients, this study aimed to elucidate the role of the enzyme glyoxylate reductase and hydroxypyruvate reductase (GRHPR) in the formation of the kidney stones and their development. There are many different types of kidney stones, but calcium oxalate kidney stones are the most prevalent in Iraq. In this study, 50 Iraqi patients with calcium oxalate stones (25 males and 25 females) were compared to 30 healthy control groups (17 males and 13 females). The biochemical tests for kidney function, such as serum urea, creatinine, and uric acid, were d

The study was conducted to identify the immunomodulatory effect of beta-glucan and to compare its immunomodulatory properties with S.boulardii yeast. In this study, S.boulardii yeast was used to extract beta-glucan. The yeast was activated using a YPD medium, its purity was examined, and the following operations were performed on it: The biomass of S.boulardii yeast was grown in a vibrating incubator. The biomass was isolated, collected, washed, and dried. Extracting beta-glucan using the acid-base method for S.boulardii yeast is considered the best  extraction method. Beta-glucan was partially purified using 4% phosphoric acid. Chemical tests were conducted on it and its functional properties (abilit

     The research is demonstrating the use of an X-ray diffraction pattern obtained experimentally from barium oxide powder. The X-ray diffraction pattern of the barium oxide nanoparticle sample was analyzed through the program to obtain the mean intensity width values and use these values to extract the particle size for all diffraction pattern lines using the Scherrer method. The nanoparticle size was calculated for each barium oxide line. Then the dislocation density was calculated through two mathematical equations, one of which depended on the particle size and the other depended on the integral breadth, a comparison was made between the results of the two dislocation densities and the particle size, where it was found

Mesoporous silica was developed to transport metoprolol tartrate (MPT). The data obtained from the kinetic experiments of adsorption of 15 ppm of MPT drug at 293 K was fitted in the pseudo-first-order, pseudo-second-order, and intraparticle diffusion models. The results show that the adsorption process obeys the pseudo-first-order equation and the rate-controlling step, not just the intraparticle diffusion step. The MPT drug load onto mesoporous silica was 15.13 mg/g. The release profile shows that the MPT drug was about 55% released after 40 min when released in water, while in phosphate-buffered saline (PBS) media, the release reached 90% after 60 min at body temperature (37°C). Three kinetic release versions, including first-order, K

This paper presents two important contributions to the field of numerical analysis for third-order ordinary differential equations (ODEs). First, a new class of direct implicit Runge-Kutta (RK) processes, called RKTDIO, is introduced as solutions to third-order ODEs. Secondly, it develops the ERKTDIO method, which is an embedded pairwise diagonal implicit RK method. The study begins by introducing the theory of relevant-colored trees and B-series as fundamental concepts. By utilizing the order constraints, two RKTDIO methods are derived: a fifth-order method with three stages and a sixth-order method with four stages. In addition, an embedded method called ERKTDIO6(5) is derived, which has orders six and five. The derivation of the embed

In the current study, 100 different clinical samples were collected in Baghdad hospitals, including Teaching Laboratories Hospital, Medical City, Baghdad Teaching Hospital, and Martyr Ghazi Hariri Hospital, for a period from May 2022 to September 2022. After diagnosis, we obtained 19 isolates of Pseudomonas aeruginosa from different clinical sources, including burns, wounds, urinary tract infections, otitis media, and blood. Cultured all samples on MacConkey, cetrimide agar. Then it underwent several microscopic and biochemical tests. Included are: Oxidase, Citrate utilization, Triple sugar-iron (TSI), catalase, Gelatinase, Motility and Ornithine decarboxylation tests. Pseudomonas aeruginosa susceptibility to 11 antibio

While transmitting data across a network, it is important to keep in mind that some fields may contain sensitive information. One of the most pressing concerns, then, is the protection of private information. The confidentiality and integrity of an online video are the primary concerns of the suggested approach in this work. Video compression using Moving Picture Experts Group (MPEG), video encryption, and video decryption are the three components that make up the proposed study. The data is encrypted using one of the most used block cipher algorithms, the Advanced Encryption Standard (AES) technique. The real-time needs of frame decoding can be satisfied by a software implementation. Our research leads us to believe that this has the po

This scientific study aims to introduce a new type of topological space, called "Grill v-space", with the aim of contributing to scientific knowledge in this field. New generalizations were developed for both the local function and the Kuratowski closure function in order to generalize their concepts. Subsequently, these generalizations were used to define a new topology based on the concepts associated with the grill and the v -space. The set of v -open in v -space is defined as the sum of the set of v -open forms in v -space when the grill consists of the subsets of P(X) except the

The current study focuses on the surface modification of an air dielectric barrier discharge (DBD) at atmospheric pressure on a polymer (epoxy). Atomic force microscopy (AFM), Hardness and Thermo-gravimetric analysis (TGA), and Differential Scanning Calorimetry (DSC) were used to characterize the material. Plasma was used to expose the epoxy sample for (0, 10, 20, and 30 min). The AFM study shows an increase in the time of plasma treatment and an increase in the parameter of roughening, in which the surface of the material is roughened by the plasma treatment. This plasma-induced morphological modification of the epoxy surface will also contribute to enhancing the wettability. In the DSC test, the stability of the glass transition temper

Rheumatoid arthritis (RA) is a chronic inflammatory disease that primarily affects the synovial joints and produces recurring inflammation of the synovial membrane, which ultimately causes joint degeneration, deformity, and disability. The current study included 110 blood samples collected from patients infected with rheumatoid arthritis (60) and 50 blood samples from controls. The results showed that investigation of some hematological tests revealed a high significant erythrocyte sedimentation rate (ESR) for the patient group compared to the control group (28.25 ± 2.72, 16.24 ± 1.83), respectively. But it is non-significant for patients for (WBC, RBC, and PLT) was (7.34 ± 0.25, 4.71 ± 0.08, and 248.26 ± 9.18), while the control gr

Fifty isolates of Staphylococcus aureus were obtained out of 220 samples collected from clinical sources after a diagnosis of the bacteria, and then a sensitivity test was performed for the isolates, and the minimum inhibitor concentration of 15 antibiotics in the bacterial isolates under study was determined using the Vitek -2 Compact System device. All isolates showed 100% resistance to Benzylpenicillin at (>=0.5-0.12) and the resistance to Oxacillin was 76% at (>= 1-4), Ciprofloxacin and Moxifloxacin was 42, 40% at (>=2-8), Gentamycin (20%) at >=16, Erythromycin by (78%) at >=8, Clindamycin (by 74%) at (>=8-16), Tetracycline by 40% at (>=2-16), Fusidic Acid by (14%) at (>=8-32), and Rifampicin by (6% )

The Tigris River is the primary source of water for human consumption in Iraq and is the ultimate sink for wastewater generated by activities. This research was conducted between November 2021 and September 2022 using 15 physio-chemical parameters (pH, air and water temperature, EC, salinity, DO, BOD, TH, Ca+, Mg+, SO4, TDS, TSS, turbidity, and Chloride), two heavy metal parameters (Cr, and Al), and biological pollutants to analyze temporal and spatial variation and the effects of pollutants sources on the water quality of the Tigris River from the north to the south of Baghdad city. The results show that some values of the tested parameters were higher than Iraqi and WHO standards for the water river, which call for attention to be paid

Proteus mirabilis is considered the third most common cause of catheter-associated urinary tract infections. With urease production, the potency of the catheter’s blockage due to the formation of biofilm is significantly enhanced. This study was aimed at exploring whether green synthesized ZnO-CuO nanoparticles (ZnO-CuO NPs) can function as an anti-biofilm agent produced by P.Mirabilis. The characterization of biosynthesized nanoparticles was carried out to determine the chemical and physical properties of the product using AFM, TEM, FESEM, XRD, and UV visible spectrometry. The hexagonal structure was confirmed by XRD, the size range was marked at 96.00nm by TEM, and FESEM was used to confirm the surface morphology. A

A theoretical study of electronic characteristics based on charge transfer using quantum model N719 dye-sensitized contact with TiO2 in solar cells. The current density expression used to calculate the photovoltaic characteristics is assumed to be a continuum level of the N719 dye and TiO2 semiconductor in the heterojunction N719-TiO2 devices using the MATLAB program. The transition energy, current, fill factor, and efficiency of N719-TiO2 DSSCs are calculated based on quantum transition theory. The performance of DSSCs photovoltaic was estimated based on the I-V characteristics of the N719-TiO2 device using concentrations  at (100 mW/cm²) irradiation. The N719-TiO2 device with Butanol solvent at a concentrati