γ-Al2O3–NPs were synthesized by a green synthesis process based on Boswellia carterii resin extract and aluminum sulphate in an alkaline medium. Boswellia carterii resin extract is a significant reducing and stabilizing agent for synthesizing γ-Al2O3–NPs.Several techniques, including Fourier–transform infrared (FT-IR), UV–visible spectroscopy, x-ray diffraction, electron microscopy (XRD), energy dispersive x-ray (EDX), scanning electron microscopy (SEM), Transmission electron microscopy (TEM), and atomic force microscopy (AFM), were utilized to investigate the final product. XRD and SEM confirmed a plate-like crystalline structure with an average size of 17.5 nm. FT-IR analysis identified aluminum oxide stretching vibrations (655, 451) cm-1, U.V.-visible spectroscopy exhibits an absorption band at 252 nm, and the energy gap, Eg, of 4.91 eV. EDX confirmed the presence of Al, and O TEM and AFM showed agglomerated spherical plates. Antimicrobial assay revealed the highest inhibition at 0.25mg/mL with a decrease in concentration from 2mg/mL to 0.25mg/mL for Staphylococcus aureus, Escherichia coli, and Candida albicans fungi. Adsorption studies by U.V-visible spectroscopy demonstrated high metal ion (II) removal efficiencies: Co (89.18 %), Ni (87.33 %), and Cu (90.42 %).
Polycystic ovary syndrome (PCOS) is a common endocrine disorder affecting women of reproductive age, characterized by anovulatory, infertility and metabolic disturbances. This study aimed to assess the diagnostic accuracy of Leucine-rich alpha-2-glycoprotein-1 (LRG1) and xanthine oxidase (XO) activity as novel biomarkers for PCOS, as well as to explore the relationship between LRG1 and XO activity across different groups. A total of 150 married women, aged 18-46 years were enrolled and divided into three groups: 50 with PCOS under treatment, 50 PCOS without treatment conditions shared by women with polycystic ovary conditions, and 50 healthy women. Serum samples were analysed to measure LRG1, xanthine oxidase (XO) activity,
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