The (E)-4-chloro-N-(2-(dimethylamino)ethyl)-5-((8-hydroxy quinolin-5-yl)diazenyl)-2-methoxybenzamide azo ligand (L) has been synthesized through the reaction of diazonium salt for 5-amino-4-chloro-N-(2-(dimethylamino) ethyl)-2-methoxybenzamide with 8-hydroxyquinoline and identified azo ligand (L) using spectroscopic studies (FTIR, UV-Vis, 1H and 13CNMR, mass), and micro-elemental analysis (C.H.N). Metal chelates of Co(II), Ni(II), Cu(II), as well as Zn(II) have been completed as well as characterized using mass spectra, flame atomic absorption, elemental analysis (C.H.N), infrared, UV-Vis spectroscopy, as well as conductivity, magnetic measurements. The metal-to-ligand ratio in all complexes, as determined by analytical data, was 1:2 and ex
... Show MoreThe present article discusses the synthesis of tetradentate Schiff base complexes formed by the condensation reaction of 2-hydroxy benzaldehyde and phthalohydrazide. The ligand (LH2) was detected using FT-IR spectra, 1H, 13C-NMR, UV-Vis spectroscopy, elemental microanalysis CHN, and mass spectrometry. The obtained solid complexes have been assessed using physicochemical and spectroscopic techniques, including UV-Vis, FT-IR, nuclear magnetic resonance (1H-NMR, 13C-NMR), mass spectrometry, thermal gravimetric analysis (TGA), and atomic absorption, in addition to complex conductivity and magnetic moment measurements. The infrared results demonstrated that ligands functioning as tetradentate ligands are chelated to metal ions via the ph
... Show MoreSYNTHESIS AND CHARACTERISATION OF NEWCo(II), Zn(II) AND Cd(II) COMPLEXES DERIVED FROM OXADIAZOLE LIGAND AND 1,10-PHENANTHROLINE AS Co-LIGAND
In this work, prepared new ligand namely 5-(2,4-dichloro-phenyl)-1,3,4-oxadiazole-2-(3H)-thion, was obtained from the 2,4-dichlorobenzoyl chloride with hydrazine, after that reaxtion with CS2/KOH in methanol.
يهدف البحث الى بيان اثر تقييم المشاريع الاستثمارية في تطوير واعداد الموازنات الاستثمارية المعدة من قبل الوحدات الاقتصادية حيث ان المشاريع الاستثمارية تعد ذات طابع مهم وحيوي للوحدات الاقتصادية وذلك لما تتضمن هذه المشاريع من طول الفترة الزمنية للاعدادها وتنفيذها ولما يرافق هذه الفترة من مخاطر وعدم تأكد وكذلك احتياجها الى اموال كثيرة لأنجاز المشروع, فأن عملية تقييم المشاريع المنفذة والتي تم اعداد موازنة
... Show MoreThe method of powder technology has been utilized in fabrication of machinable
ceramics by the approach of glass-ceramic principles. The crystalline ceramic phases
partially dissolved by host glass while the undissolved part remain responsible for the
machinability by the usual cutting tools. Thus avoiding the unnecessary use of special
dies to cast fully melted composition and initiate recrystallization process. Two types of
machinable ceramics have been successfully prepared, the first with high silica content
and the other with high alumina content. A comparison of their properties and discussed.
Still Financial institutions, including banks, a key target for money launderers to transfer illicit funds to the legitimate funds and by weaknesses in the internal audit procedures applied in the banks or through a lack of legal structure to combat this phenomenon in addition to the procedures by other regulations
T
... Show Moreيتناول هذا الموضوع تحليلًا لظاهرة وفيات الأمهات في الوطن العربي خلال الفترة من 1990 إلى 2023، مع التركيز على الأسباب الرئيسية لهذه الوفيات، والعوامل الاجتماعية والاقتصادية والصحية التي تسهم في تفاقمها. يهدف الموضوع إلى تسليط الضوء على التحديات التي تواجهها الدول العربية في تحسين صحة الأمهات، وتقييم التقدم المحرز نحو تحقيق أهداف التنمية المستدامة المتعلقة بخفض معدلات وفيات الأمهات.. تم استخدام المنهج الوصفي و
... Show More
