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jih-913
Spectrophotometric Determination of Isoptin (Verapamil Hydrochloride) in Pharmaceutical Preparations
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Verapamil Hydrochloride (VH) has been determined spectrophotometrically by using Methyl Orange (MO).  In our previous researches MO was used for determination of Mexiletine Hydrochloride [1]. The method was based on complexation between (MO and VH).  After shaking and diluting the complex solution with D.W, the pH was adjusted with NaOH and HCl to pH 4. The colored complex formed between VH and the reagents were transferred into separating funnels and extracted using 4.5 ml CH2Cl2 and were shaken for (4 minutes).  The extracted organic layer was used for the preparation of the calibration curves for spectrophotometric measurements of VH at 437nm.  The blanks were carried out in exactly the same way throughout the whole procedure.  Molar absorptivity (ε L.mol-1.cm-1), detection limit, limit of linearity (µg.ml-1) and r2 were, 1.75*105, 0.009253, 0.08 and 0.993 for (VH-MO) respectively. The method was used with reasonable accuracy and precision for the determination of (VH) in synthetic samples of tablets, capsules and ampoules.

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Publication Date
Thu Mar 30 2017
Journal Name
Iraqi Journal Of Pharmaceutical Sciences ( P-issn 1683 - 3597 E-issn 2521 - 3512)
Determination of Cefalexin by Direct (UV- Vis) Spectrophotometer and Indirect(Flame Atomic Absorption) Technique
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         A new method for the determination of the drug cefalexin in some Pharmaceuticals using (UV-Vis) and  indirect Flame Atomic Absorption Spectrophotometer (FAAS) , Fe III should forms a chelating complex with cefalexin (CEX –Fe III) at pH (1-8) and the best pH for the formation of (CEX –Fe III) chelating complex was (2) .The complex extracted with Methanol  and  Dimethy-Sulphoxide .The mole-ratio method has been used to determine the structure of chelate (CEX - Fe III) and found to be 2:1 LM ( Ligand : Metal.) .

Keywords : Cefalexin , chelating complex.

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Publication Date
Mon Jun 05 2023
Journal Name
Al-khwarizmi Engineering Journal
Determination of the Optimum Conditions for Removal of Congo Red Dye by Peroxidase Enzyme Plant
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The pollution producing from textile industries effluents is growing since the years, due to at discharged lots of it in water without treatment. The resulting effluent is colourful, highly toxic, and poses a significant environmental hazard. This problem can be solved by using enzymic biological treatment, where the Congo red dye was used with concentrations (100,200,300,500) mg /L, pH values (3,4,5,6,7,8), and variable temperatures (25,35,45)°C, the best removal of Congo red (CR) dye  under optimum conditions for degradation was at  concentration of 100 mg/L, at (pH 6, 25 °C) with efficiency of 99.85 % using the peroxidase enzyme extracted from red radish plant, while the removal percentage decreased when increase dye concentration

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Publication Date
Wed Jul 29 2020
Journal Name
Iraqi Journal Of Science
Determination of DynamicElastic Properties of Anah Formation, Near Rawa city / Western Iraq Using Ultrasonic Technique
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The aim of the current  study is to determine the elastic properties  of carbonate rocks using ultrasonic method.  Forty rock samples of  Anah formation  were collected at  different depths from  four wells drilled at the study area . The relationship between wave velocities and elastic properties of rocks was defined. Regression analyses to define these relations were applied. The results indicate that the elastic properties of the rocks show a linear relationship with both P- and S-wave velocities. The best relationship was obtained between both Young's modulus and Shear modulus with Vs in the determination of the coefficient ( R2  ), with values of 0.91 and 0.94,  respectively.&n

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Publication Date
Thu Apr 01 2021
Journal Name
Iraqi J Of Agricultural Science
Determination of Beta Lactam Resistance of Klebsiella Pneumoniae Isolated from Clinical Specimens and Water Samples
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Publication Date
Sun Jan 30 2022
Journal Name
Iraqi Journal Of Science
Determination of Active Phytochemical Compounds of Alhagi Maurorum using Gas Chromatography-Mass Spectroscopy (GC-MS)
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Alhagi maurorum (camel thorn) is a grayish, evergreen, deeply rooting plant that has spiny needle -like branches. In our study, the phytochemical contents of the root ethanoloic extract of A. maurorum were determined by using gas chromatography-mass spectroscopy (GC-MS). Thirty two chemical constituents were identified. We revealed the existence of oxalic acid, anti-2 acetoxyacetaldoxime, sulfone, butyl isopropyl, 2,3-pentanedione, 2-butanone, n,n,o triacetylhydroxylamine. di(1,2,5-oxadiazole)[3,4-b;3,4-e]pyrazine, isobutane,3,4-hexanedione,3-hexanone, pentane, 3-pentanone, 3-butene, 2-thiopheneacetic acid, 2-pyrazoline, 4-hepten-3-onemethylphosphonic acid, butane, propanoic acid, methane, azetidine, heptane, butanoic a

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Publication Date
Tue Dec 01 2020
Journal Name
Baghdad Science Journal
Optimization of Voltammetric Determination of Dysprosium (III) Using Plackett-Burman and RSM-CCD Experimental Designs
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This study was aimed to develop an optimized Dy determination method using differential pulse voltammetry (DPV). The Plackett-Burman (PB) experimental design was used to select significant factors that affect the electrical current response, which were further optimized using the response surface method-central composite design (RSM-CCD). The type of electrolyte solution and amplitude modulation were found as two most significant factors, among the nine factors tested, which enhance the current response based on PB design. Further optimization using RSM-CCD shows that the optimum values for the tw

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Publication Date
Mon Oct 01 2018
Journal Name
2018 International Conference On Advanced Science And Engineering (icoase)
Determination of the Influence Forces Affecting the Surface Layers of the Rotating Magnetic Neutron Stars
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Publication Date
Thu Jun 30 2022
Journal Name
Iraqi Journal Of Science
Determination of Differential Cross-Section of (n+89Y) Elastic and Inelastic Scattering using Eikonal Approximation
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     Neutron differential-elastic and inelastic scattering cross-sections of Yttrium-89 isotope were calculated at energies 8,10,12,14, and 17 MeV, at angles distributed between 20o and 180o in the center of mass frame. The obtained results data were interpreted using a spherical optical potential model and Eikonal approximation, to examine the effect of the first-order Eikonal correction on the effective potential. The real and imaginary parts of optical potential were calculated. It was found that the nominal imaginary potential increase monotonically while the effective imaginary one has a pronounced minimum around r = 6fm and then increases. The analysis of the relative energy of the projectile and reaction

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Publication Date
Sun Mar 04 2018
Journal Name
Iraqi Journal Of Science
Determination the Quantity of Extreme Rainfall and calculation of the Climatology Mean for Baghdad City
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Recently heavy rainfall that occurs in last decade for Baghdad city is part of climate changes effect on Iraq in general and Baghdad in particular. Rain is considered the main part in the water cycle as it enters mainly within the water system and water balance; therefore present study put of a special criterion to determine the amount of rainfall and analyzed in order to quantify the amount and the diagnosis of heavy rain. The availability of data by Iraqi Metrological  Organization  and Seismology (IMOS) for time period (1985/1986-2014/2015) held achieve the research objective .There are many statistical methods figure out  the difference to determine the amount of rain, Climatology mean  (C M) is one of them specia

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Publication Date
Sun Oct 22 2023
Journal Name
Iraqi Journal Of Science
Determination of the MESEP Events of 2-9th April 2001 According to ERNE/SOHO Observation
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On 2-9th April 2001 the Energetic and Relativistic Nuclei and Electron (ERNE) instrument on the Solar and Heliospheric Observatory (SOHO) observed three gradual solar energetic particle (SEP) events separated by 9 hour and 7days respectively, in association with three effective solar flares and coronal mass ejections (CMEs).
In this paper, a study of MESEP events was considered. As the definition of this phenomenon suggested there might be many sources for each MESEP event. This event has been examined in order to view the different sources that might relate to suspected accelerator of the SEPs. A careful analysis for the spectra and associated emission with such eruptions was made. Soft X-ray emission was observed by the Geostationar

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