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The azo Schiff base [Reaction of 4-aminoanypyrine and P-hydroxy acetophenone] and O-Phenylene
diamine have been prepared. One azo Schiff base chelate of Co(Il), Ni(II), Cu(II) and Zn(II)ion was also
prepared. The chemical frameworks of the azo Schiff base and like elemental analyses (CHN),
determinations of molar conductance,
1 H &13C NMR, IR mass and electronic spectroscopy .The elemental
analyses exhibited the combination of [L: M] 1:1 ratio. Established on the values IR spectral, it is showed
that the azo Schiff base compound acts as neutral hexadentate ligand bonded with the metal ion from two
hydroxyl, two azomethine and two azo groups of the azo Schiff base compound in chelation was
confirmed by IR ,
1Hand 13CNMR spectral outco
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