4-Aminoantipyrine
P-ChloroBenzoyl isothiocyanate
complexes
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A new ligand [4-chloro-N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-
dihydro-1H-pyrazol-4-ylcarb amothioyl) benzamide] (CAP) was
synthesized by reaction of P-ChloroBenzoyl isothio cyanate with 4-
aminoantipyrine,The ligand was characterized by micro elemental analysis
C.H.N.S.,FT-IR,UV-Vis and1H13CNMR spectra, some transition metals
complex of this ligand were prepared and characterized by FT-IR, UV-Vis
spectra, conductivity measurements, magnetic susceptibility and atomic
absorption. From the obtained results the molecular formula of all prepared
complexes were [M(CAP)2(H2O)2]Cl2(M+2 =Mn, Co, Ni, Cu, Zn, Cd and
Hg),the proposed geometrical structure for all complexes were octahedral