A newly developed analytical method characterized by its speed and sensitivity for the determination of metformin-HCl via the formation of complex for metformin-HCl-OH--copper(II) ion from the gel bead system by continuous flow injection analysis. The method is based on the imbedded copper(II) ion in the gel bead structure can be used in the reaction for the formation of red –magneta colour complex(λmax. =530nm) formed by direct reaction of the drug with the released copper (II) ion from the gel bead in alkaline medium. Linear dynamic range for the absorbance versus metformin concentration was 0.001-1 mmol.L-1 while C.O.D was (r2% =95.33%) . The L.O.Q was 0.868mmol.L-1.L.O.D (S/N=3)=0.5μmol.L-1 from the step wise dilution for the minimum concentration of lowest concentration in the linear dynamic ranged of the calibration graph with R.S.D% lower than 0.5% for 0.01 mmol.L -1( n=8) concentration of metformin- HCl, throughput 30 sample.hr-1. The method was applied successfully for the determination of metformin in three pharmaceutical drugs. A comparison was made between the newly developed method of analysis with the classical method(Uv-spectrophotometry at wave length = 241nm) of analysis using the standard addition method via the use of paired t-test. It shows that there was no significant difference at α= 0.05 (95% confidence) between the two methods. Therefore the newly developed method(using the Metformin- OH- - Cu(II) entrapped inside gel bead) can be adopted as an alternative method for the analysis of metformin.
Objective: The aim of this study was to evaluate the effect of pumice, burning investment material
and black sand on the surface roughness of heat cure acrylic resin.
Methodology: Sixty specimens were prepared from pink heat cure acrylic resin, the specimens
where grouped into; 20 specimens which polished with pumice and water (control group); 20
specimens which polished with investment material (after burning it) and water; and 20 specimens
which polished with black sand and water. The average surface roughness of specimens after
polishing procedure had been determined by profilometer (surface roughness tester).
Results: Through the application of ANOVA and LSD tests, the result of this study showed that there
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Upper Cretaceous Oceanic Red Beds (CORBs) are pelagic sediment deposits that deposited in the Upper Cretaceous basin, with widespread in part of the world as well as in Iraq. This research investigates the deposition of cyclic marl and marly limestone CORBs of six selected sections at the active southern margin of the Tethys during the Late Campanian - Maastrichtian with petrography, microfacies, and depositional environment.
The measurement of carbonate content (CaCO3 %) in the rocks, 180 samples of all the geological sections were studied twice for each sample and the average readings were taken.
This examination proved the following major oxides wt. % concentrations domination SiO2, CaO, Al2 O3 and Fe2O3 with average values of 3
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The present study investigates the effect of the de-sanding (recycling system) on the bearing capacity of the bored piles. Full-scale models were conducted on two groups of piles, the first group was implemented without using this system, and the second group was implemented using the recycling system. All piles were tested by static load test, considering the time factor for which the piles were implemented. The test results indicated a significant and clear difference in the bearing capacity of the piles when using this system. The use of the recycling system led to a significant increase in the bearing capacity of the piles by 50% or more. Thus it was possible to reduce the pile length by (15 % or more) thus, and implementation c
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In this study we focused on the determination of influence the novel synthesized thiosemicarbazide derivative "2-(2-hydroxy-3-methoxybenzylidene) hydrazinecarbothioamide" (HMHC) influenced the corrosion inhibition of mild steel (MS) in a 1.0 M hydrochloric acid acidic solution.This is in an effort to preserve the metal material by maintaining it from corrosion.The synthesized inhibitor was characterized using elemental analysis, and NMR-spectroscopy. Then the corrosion inhibition capability of (HMHC) was studied on mild steel in an acidic medium by weight loss technique within variables [temperature, inhibitor concentration, and time]. The immersion periods were [1:00, 3:00, 5:00, 10:00, 24:00, and 72:00] hours and the tem
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The research discusses two variables are important, orientation marketing and quality of service, and that the purpose of the research is to see whether the telecom companies applied orientation marketing or not and to what extent is keen to apply it to suit the Iraqi environment as it has been applied research in kork Telecom company and Asia Cell Telecom are sectors service job in the business sector in Iraq, The information was obtained through the design of the questionnaire compatible runway Likert, and distribution (92) questionnaire, which (50) for the company Korek Telecom and (42) of the Asia-Cell, research population sample included a number of staff in the departments and units in the two companies, it has been support
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This study deals with formation models of gypsum barrier, chemical temporal changes, and assessments of the Sawa Lake within the Al- Muthanna province, Southern Iraq, it is a very important issue to find the water quality and water assessments of this lake. Eleven water samples are collected from Sawa Lake. Many scientific concepts are used such as major cations (Ca2+, Mg2+, Na+ and K+), major anions (SO4=,Cl-,HCO3- and CO3=) with minor anions ( PO43-, NO3-) and H2S . Trace elements (Pb, Cd, Zn, As, Ni, Co, Cu, Mn, Fe, As, Sr And B) and bacterial test were analyzed in each sample. Total dissolved solids (TDS), electrical conductivity (EC), pH and temperature (T) were directly measured in the field. The equilibrium state between the conce
... Show MoreThe study has used Geographic Information Systems (GIS) data and Arc GIS software, to produce a new map. This map contains a spatial database of the newly constructed buildings, in the area of water resources engineering college, and using the above tool for updating contains the college in any time, also the map and browse all buildings individually or in clustered, for example, browsing geometric data, statistical data and the plans of drawings, and make any necessary changes to these sectors immediately, or in the future, like the expansion of the study halls by constructed a new floor, or add supplements, prepare any electrical to any building, and anything else. The paper also, updates the old Google Earth image, f
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