Worldwide attention is being focused on nanocrystalline zeolites and they are replacing conventional ones due to their pronounced potential in many fields. In this study, NaY zeolite has been prepared hydrothermally using sol –gel method and modified to the proton type by ion –exchange process. Characterization is made using X-ray diffraction (XRD), thermogravimetric analysis (TGA), Fourier transform infrared spectroscopy (FTIR), Atomic force microscopy (AFM), Brunauer –Emmet- Teller (BET) nitrogen adsorption method, Ammonia Temperature programmed desorption (NH3-TPD) and Scanning electron microscopy( SEM). The effect of aging time, silica to alumina ratio is studied and the results show well defined crystalline structure with nano particle size (70 and 81nm) with surface area of 499m2/gm.
Bodas de sangre es una tragedia en verso del escritor Federico García Lorca escrita en 1932, y estrenada el 8 de marzo de 1933 en el teatro Beatriz de Madrid con gran éxito tanto en España como en Hispanoamérica. Fue llevada al cine por Carlos Saura en 1981. Es una producción poética y teatral que se centra en el análisis de un sentimiento trágico. Desde la vida y la muerte, a lo antiguo y lo moderno, en la manera de ver la tragedia. Todo ello enmarcado en un paisaje andaluz trágico y universal.
El tema principal que se trata en este drama es la vida y la muerte. Pero de un modo arcano y ancestral, en la que figuran mitos, leyendas y paisajes que introducen al lector en un mundo de
... Show MoreLa vorágine es una novela insigne de la literatura colombiana e hispanoamericana que trata de manera singular el tema de la violencia. Este artículo propone una reflexión filosófica novedosa para abordar la violencia como objeto de conocimiento. Se plantea, en primer lugar, un nuevo enfoque a partir de la teoría literaria,enseguida se consideran aspectos del relato, tales como: la doble naturaleza del mundo, el absurdo y la dinámica autoproductiva de la violencia y con ayuda de varios autores, constatamos cómo estos mismos aspectos admiten nuevas aproximaciones. Este artículo nos lleva a pensar nuevas formas de ser y de actuar en el mundo a partir del modo como nos relacionamos con lo otro.
This research involves the synthesis of some sulphanyl benzimidazole derivatives (Ia-c), which were prepared from reaction of 2-mercaptobenzimidazole substituted benzyl halide, and structures were identified by spectral methods[FTIR, 1H-NMR and 13C-NMR].These compounds were investigated as corrosion inhibitors for carbon steel in 1M H2SO4 solution using weight loss, potentiostatic polarization methods; obtained results showed that the sulphanyl benzimidazole derivatives retard both cathodic and anodic reactions in acidic media, by virtue of adsorption on the carbon steel surface. This adsorption obeyed Langmuir’s adsorption isotherm. The inhibition efficiency of (Ia-c) ranging between (65-92) %. By using different Ib derivative conc
... Show MoreIn this research investigation, a total of eighteen diverse tetra- and penta-lateral cyclic compounds were synthesized. These included 1,3,4-thiadiazole, thiazolidin-4-one (via an alternative method), 1,2,4-triazole, carbothioamide, thiazole-4-one, azetidin-2-one, and oxazole. The synthesis procedure entailed a sequence of reactions. The thiazolidine-4-one 1 was obtained by reaction p-aminobenzoic acid with thiosemicarbazide, followed by treatment with p-tolualdehyde to produce Schiff base 2. Reaction Schiff base 2 with mercaptoacetic acid in dry benzene was carried out to produce thiazolidine-4-one 3. In another synthesis pathway, the esterification of p-nitro benzoic acid with ethanol in the presence of sulfuric acid was
... Show MoreStable new derivative (L) Bis[O,O-2,3;O,O-5,6(carboxylic methyliden)]L-ascorbic acid was synthesized in good yield by the reaction of L-ascorbic acid with dichloroacetic acid with ratio (1:2) in presence of potassium hydroxide. The new (L) was characterized by 1H,13C-NMR, elemental analysis (C,H) and Fourier Transform Infrared (FTIR). The complexes of the ligand (L) with metal ion, M+2= (Cu, Co, Ni, Cd and Hg) were synthesized and characterized by FTIR, UV-Visible, Molar conductance, Atomic absorption and the Molar ratio. The analysis evidence showed the binding of the metal ions with (L) through bicarboxylato group manner resulting in six-coordinated metal ion.
In this research various of 2,5-disubstituted 1,3,4-oxadiazole (Schiff base, oxo-thiazolidine , and other compounds) were synthesized from 2,5-di(4,4?- amino-1,3,4-oxadiazole ) which use quently synthesized from mixture of 4-amino benzoic acid and hydrazine in the presence of polyphosphorus acid. The synthesized compounds were characterized by using some Spectral data (UV, FT-IR, and 1H-NMR).
Resumen
La literatura española tiene muchísimos de los grandes personajes y las figuras literarias que casi todos desempeñaron de una forma u otra un eficaz e importante papel en el desarrollo de la literatura española en particular y la literatura universal en general, entre otros podemos mencionar el gran escritor de origen argentino Jorge Luis Borges sobre el mismo gira este trabajo de investigación.
Sinceramente, podemos decir que el objetivo principal de ese trabajo de investigación es hacer conocer de una forma tan sencilla, tan simple y tan clara al lector público quién es Jorge Luis Borges quien procedía de una familia de próceres
... Show MoreThe research entitled: (The Constructive Mutation of installation Systems in the Artworks of the artist Ali Al-Najar) has dealt with the concept of Mutation and its systematizations in installation in the artworks of (Ali Al-Najjar).
The research has four chapters: The first Chapter deals with the methodological framework represented by the basic problem of the research, that is concerned with the constructive mutation of installation systems.
The research aims at finding out the constructive mutation of installation systems in the artwork of ( Ali al-Najar). The research is limited by analyzing visual samples of (Ali Al-Najjar) artworks betwen (1967-1991)
The second chapter deals with the theoretical framework, it has five s