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Some azo compounds were prepared by coupling the diazonium salts of amines with 2,4-dimethylphenol The
structure of azo compounds were determined on the basis of elemental analyses, 1HNMR, FT-IR and UV-Vis
spectroscopic techniques. Complexes of nickel(II) and copper(II) have been synthesized and characterized.
The composition of complexes has been established by using flame atomic absorption, (C.H.N) Analysis, FT-IR and
UV-Vis spectroscopic methods as well as conductivity magnetic susceptibility measurements. The nature of the complexes
formed were studied following the mole ratio and continuous variation methods, Beer's law obeyed over a concentration
range (1×10-4 - 3×10-4 M). High molar absorbtivity of the complex solutions were observ
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