Biodiesel production · Esterifcation reaction · Waste cooking oil
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An innovative two-step noncatalytic esterifcation technique was proposed to synthesize alkyl esters from free fatty acids simulated in waste cooking oil, as a pretreatment process for biodiesel production, without adding any catalyst under normal conditions of pressure and temperature. The efect of methanol:oil molar ratio,
reaction time, mixing rate, and reaction temperature were investigated. The results
confrmed that the conversion of the reaction was increased when increasing the
methanol molar ratio and decreased in prolonged reaction temperature. High conversion (94.545%) was successfully achieved at optimized conditions of 115:1, 65:1
methanol:oil molar ratio in the frst step and second step, respectively, other conditions i
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