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Publication Date
Fri Jul 28 2023
Journal Name
Journal Of Advanced Pharmaceutical Technology & Research
Volume
14
Issue Number
3
DOI
10.4103/japtr.japtr_285_23
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Development of a spectrophotometric analytical approach for the measurement of cefdinir in various pharmaceuticals
Cefdinir
colorimetric
derivatization
sodium anthraquinone‑2‑sulfonate
spectrophotometry
Ali khalil mahmood
Takleef Dheyab Sallal
Khalid Waleed S Al-Janabi
Hasan Mohammed Luaibi
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Publication Date
Sun Sep 01 2013
Journal Name
Baghdad Science Journal
Six-coordinate oxime-imine cobalt(III) complexes with amino acid co-ligands; synthesis and characterisation
Schiff-base imine-oxime ligands
diaminoethane-N
N`-bis(2-butylidine-3-onedioxime) H2L1 and o-pheneyenediamine-N.N-bis(2-butylidine-3-onedioxime) H2L2
Six coordinate Co(III)-complexes
Structural study.
Mohamad J.
Hasan A.
Alaa M.
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In this publication, several six coordinate Co(III)-complexes are reported. The reaction of 2,3-butanedione monoxime with ethylenediamine or o-phenylenediamine in mole ratios of 2:1 gave the tetradentate imine-oxime ligands diaminoethane-N,N`-bis(2-butylidine-3-onedioxime) H2L1 and o-phenylenediamine-N,N`-bis(2-butylidine-3-onedioxime), respectively. The reaction of H2L1 and H2L2 with Co(NO3)2, and the amino acid co-ligands (glycine or serine) resulted in the formation of the required complexes. Upon complex formation, the ligands behave as a neutral tetradantate species, while the amino acid co-ligand acts as a monobasic species. The mode of bonding and overall geometry of the complexes were determined through physico-chemical and spectro

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