تعد التجارب المختبرية من أهم الوسائل التي تمكن من فهم خصائص المواد الكيميائية وسلوكها، كما إنها الوسيلة الوحيدة لتحضير المركبات الكيميائية المختلفة. وقد أدى تطور التكنولوجيا في الوقت الحاضر إلى إستخدام أدوات وأجهزة قياس في المختبر مكنت من زيادة دقة نتائج التجارب وسرعة الحصول عليها. أن تفعيل المختبر وإجراء الأنشطة العملية يمكن أن تحقق عدة أمور منها : 1- تُنمي في الطالب مهارات التفكير العلمي ( الملاحظة ، وتحديد المشكلة، وفرض الفروض، وإختبار الفروض، وإختيار الفرض الصحيح ، الإستنتاج والتعميم ) 2- تنمية القدرة على حل المشكلات والتفكير الإبداعي . 3- تمكن الطالب من تكوين المفاهيم بدلاً من المعرفة المجردة . 4- تساعد الطالب على تكوين الميول والإتجاهات العلمية ونوع الإختصاص في المستقبل . 5- تساعد على ترسيخ المعلومة وبقاء أثر التعلم فترة أطول . 6- تكسب الطالب طرق التعامل مع الأدوات المختبرية والمواد الكيميائية والتعرف على مخاطرها عن قرب وفهم قوانين وقواعد السلامة في المختبر وتطبيقها والمحافظة على سيرالعمل والآلات والأجهزة الموجودة في المختبر. 7- بث روح التعاون بين الطلاب بين المجاميع المختبرية . ويغطي هذا الكتاب مما يحويه من المعلومات الضرورية الوافية لمساقين في الكيمياء اللاعضوية وخاصة في التعرف على الجدول الدوري للعناصر وكل مايحتاجه الطالب في الالمام بالمعلومات التي تفيده من خلال التعرف على المختبرات العملية والتي تخص المرحلة الثانية . ويتميز هذا الكتاب بشموله بالتجارب العملية لثلاثين تجربة والتي تخص حول مركبات عناصر في الجدول الدوري. ويعتبر هذا الكتاب كمدخل في توضيح العلاقة بين المنهج النظري والمنهج العملي بشكل مترابط المفاهيم من خلال تعرف الطالب على التجارب العملية لما لها من مجالات تطبيقية في بيئته. وإشتمل الكتاب على عشرة فصول : الفصل الأول: توجيهات مختبرية وتعليمات عامة - نموذج كتابة التقريرعن التجربة - التعرف على الأدوات والأجهزة المستخدمة في مختبر الكيمياء ، توضيح الطريقة الصحيحة للتعامل مع الأجهزة ، مبادئ السلامة الأمنية ، مخاطر المواد الكيميائية ، بطاقات التعريف ، قواعد السلامة في تخزين وتداول المواد الكيميائية ،الاشارة الى الإسستعمالات الخاطئة والصحيحة بشكل مخططات او صور او رسوم توضيحية وبعض الإسعافات الأولية . الفصل الثاني: معلومات حول الجدول الدوري للعناصر . الفصل الثالث :الهيدروجين وتجربة (1) وتخص الحوامض والقواعد والأملاح . الفصل الرابع- الفصل العاشر : التجارب من (2-30 ) تخص معلومات عن العناصر بزمر مختلفة مع ذكر المخاطر الكيميائية للمواد الكيميائية التي يتم التعامل معها في المختبر. الملاحق (Appendix ) : وتتضمن بعض الأجوبة النموذجية لبعض تجارب الكيمياء اللأعضوية الواردة في الكتاب مع أسماء جميع عناصرالجدول الدوري وبعض خواصها . الإشارات التحذيرية– إشارات المنع - الإشارات الإجبارية --الإشارات الإستدلالية .
Abstract:
Witness the current business environment changes rapidly reflected on the performance of the facility wishing to stay , which is no longer style reaction enough to handle installations with their environment , and quickly began to lose its luster with the emergence of a message and the vision of contemporary business environment from a set of parts interacting with each other and the concept of behavioral includes all dimensions of performance, it is imperative to adopt a system installations influence variables and positive interaction through the development of strategic plans and the use of implementation and follow-up strategies to ensure the effectiveness of the method for meas
... Show MoreThe purpose of this study was to find out the connection between the water parameters that were examined in the laboratory and the water index acquired from the examination of the satellite image of the study area. This was accomplished by analysing the Landsat-8 satellite picture results as well as the geographic information system (GIS). The primary goal of this study is to develop a model for the chemical and physical characteristics of the Al-Abbasia River in Al-Najaf Al-Ashraf Governorate. The water parameters employed in this investigation are as follows: (PH, EC, TDS, TSS, Na, Mg, K, SO4, Cl, and NO3). To collect the samples, ten sampling locations were identified, and the satellite image was obtained on the
... Show MoreThe research involved a rapid, automated and highly accurate developed CFIA/MZ technique for estimation of phenylephrine hydrochloride (PHE) in pure, dosage forms and biological sample. This method is based on oxidative coupling reaction of 2,4-dinitrophenylhydrazine (DNPH) with PHE in existence of sodium periodate as oxidizing agent in alkaline medium to form a red colored product at ʎmax )520 nm (. A flow rate of 4.3 mL.min-1 using distilled water as a carrier, the method of FIA proved to be as a sensitive and economic analytical tool for estimation of PHE.
Within the concentration range of 5-300 μg.mL-1, a calibration curve was rectilinear, where the detection limit was 3.252 μg.mL
The research seeks to identify the contemporary events that face the use of electronic payment methods to localize the salaries of state employees and its impact in enhancing the mental image of customers, and to achieve this purpose from the fact that a questionnaire was designed and distributed to an optional sample of (31) individual customers (employees) dealing With the researched private banks, it has been analyzed and reached a number of conclusions and recommendations, the most prominent of which is the lack of modernity of electronic payment methods by customers, which is reflected in the mental image of customers and the achievement of their satisfaction, in the Emiratization project for salaries needs an advanced leade
... Show MoreCertainly there is a negative impact on development due to corruption in its corruption forms It is administrative and financial as well as direct impact on all sectors Including the health sector, which has seen in Iraq a marked setback in performance and services , The research aims at the possibility of demonstrating the negative effects of financial and administrative corruption on health institutions and Inability to meet health needs The extent to which Regulatory institutions and institutions manage to reduce financial and administrative corruption and ways of dealing with it The phenomenon of financial and administrative corruption is the most serious phenomenon because of its impact on economic growth, which in turn impedes the
... Show MoreIn the cuurent article, the photophysical properties of 3,6-bis(5-bromothiophen-2-yl)-2,5-bis(2-ethylhexyl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione were investigated. The visible absorption bands at 527, 558 and 362 nm in propylene carbonate and the compound was found to be fluorescent in solution and in the plastic film with emission wavelengths between 550- 750 nm. The Stokes Shift of P.C., acetonitrile, diethyl ether, Tetrahydrofuran THF, cyclohexane, dibutyl ether, and dichloromethane DCM are 734, 836, 668, 601, 601, 719, and 804 cm-1 in respectively. The Stokes Shift Δ was less in THF and cyclohexane, than the solvents, which indicates that the energy loss is less between the excitation and fluorescence states. The
... Show MoreThe article analyzes the neologisms that arose in the Iraqi dialect after the 2003 US-British invasion and the fall of Saddam Hussein's regime, according to the theory I advocate: "The Basic Outline of Reference," a developed theory of Arab legacy and cognitive theory, which came out in 1987 in America, so we have used the terminology of cognitive grammar. In this theory it is stated that the reference is the interaction between four components: perception, imagination, imaginative comprehension and the linguistic sign or symbolization (the neological word in this article), which are closely related, so that none of them can be lacking, because they constitute a holistic whole that belongs to a deeper level. Let us
... Show MoreJean-Paul Sartre and Badr Shakir al-Sayyabe are among the most prominent writers that critiqued the destructive role of capitalism and the patriarchal power system in the period of the Post-World War II crisis. Divided into three chapters, the present study examines two of the most eminent literary works in the history of the Western and Eastern societies in the fifties of the last decade: Jean Paul Sartre’s play : The Respectful Prostitute and Badr Shaker al-Sayyabe’s poem: The Blind Prostitute.
Chapter one discusses the position of the prostitute in a patriarchal societies. Chapter two linguistically analy
... Show MoreOur research comes to shed light on Iraqi literature as literature that arose in special circumstances alongside foreign literature. Using comparative research methods, we chose to highlight two distinguished writers, who have their mark in the world of literature. The first is the Iraqi writer Maysaloun Hadi, who is considered an icon of Iraqi feminist literature, and the second is the French writer Le Clézieu, who won the Nobel in 2008. We will see through the research how the two authors expressed their views of modernity and urbanism. And how each of them separately portrayed the psychological and moral projections that formed the essence of man today.
Résumé
Notre recherche abord un des points inc
... Show MoreIt is very known how great is the role of the Jewish writers in the system of the Zionist movement. The movement relied on writers and writers to carry out their programs, especially those pertaining to the creation of a "national homeland" for Jews. Most Jewish writers sang of Palestine even though they were not born there.
On such a basis, we have followed closely the writings of writers, critics and others by the end of the nineteenth century and the beginning of the twentieth century. We found that these writings are based on one common question: What is the fate of the Jewish people?
Most of these writings were accompanied by Theodor Herzl's proj
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