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Experimental Investigation of Nano Alumina and Nano Silica on Strength and Consistency of Oil Well Cement
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In oil and gas well cementing, a strong cement sheath is wanted to insure long-term safety of the wells. Successful completion of cementing job has become more complex, as drilling is being done in highly deviated and high pressure-high temperature wells. Use of nano materials in enhanced oil recovery, drilling fluid, oil well cementing and other applications is being investigated. This study is an attempt to investigate the effect of nano materials on oil well cement properties. Two types of nano materials were investigated, which are Nano silica (>40 nm) and Nano Alumina (80 nm) and high sulfate-resistant glass G cement is used. The investigated properties of oil well cement included compressive strength, thickening time, density, free water and rheological properties. All tests are conducted according to API specification and proceed in Laboratory of Drilling in Petroleum Technology Department in University of Technology and in Missan Oil Company. The experimental results show that NS and NAL behave like accelerators when added to cement and work to increase the compressive strength at 38°C but these increasing in compressive strength changes when the temperature is increased to 60°C. Also, adding NS and NAL lead to increasing in rheological parameter and reduce free water but the change in density is very small. The results show that the effect of NAL on compressive strength and thickening time is greater than the effect of NS but the effect of NS on free water and rheology is greater than the effect of NAL.

 

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Publication Date
Thu Mar 30 2017
Journal Name
Iraqi Journal Of Pharmaceutical Sciences ( P-issn 1683 - 3597 E-issn 2521 - 3512)
Synthesis of New Opioid Analgesic Peptide Analogues to Enkephalin (Leucine- and Methionine-Enkephalin)
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A small number of researches were done in the design and synthesis of enkephalin analogues that are able to resist degradation effect of proteolytic enzymes with good bioavailability and half-lives.Through studying structure activity relationships we tried to incorporate phthalyl group, tryptophan and lysine amino acids in different positions in the basic backbone structure of the naturally occurring opioid Leu5- and Met5- enkephalin, in the hope that such insertion of these amino acids could induce interesting addition in the biological activity of these analogues with enhancement of their bioavailability, in addition to decrease side effects as addiction liability.

These synthesized peptides are:

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    Publication Date
    Tue Dec 01 2020
    Journal Name
    Iraqi Journal Of Physics
    Enhancement of thermal stability and wettability for epoxy/Cu coated carbon fiber composites
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        This research study the effect of surface modification and copper (Cu) plating carbon fiber (CF) surface on the thermal stability and wettability of carbon fiber (CF)/epoxy (EP) composites. The TGA result indicates that the thermal-stability of carbon fiber may be enhanced after Cu coating CF. TGA curve showed that the treatment temperature was enhanced thermal stability of Ep/CF, this is due to the oxidation during heating. The Cu plating increased the thermal conductivity, this increase might be due to reduce in contact resistance at the interface due to chemical modification and copper plating and tunneling resistance.

       The increase of surface polarity after coating cause decreas

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    Publication Date
    Thu Dec 06 2018
    Journal Name
    Iraqi Journal Of Pharmaceutical Sciences ( P-issn 1683 - 3597 E-issn 2521 - 3512)
    Effects of Vitamin E and Q10 Supplementation against Doxorubicin-Induced Neurotoxicity in Rats
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    Publication Date
    Thu Mar 30 2017
    Journal Name
    Iraqi Journal Of Pharmaceutical Sciences ( P-issn 1683 - 3597 E-issn 2521 - 3512)
    Formulation and in vitro Evaluation of In-situ Gelling Liquid Suppositories for Naproxen
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    In-situ gelation is a process of gel formation at the site of application, in which a drug product formulation that exists as a liquid has been transformed into a gel upon contact with body fluids. As a drug delivery agent, the in-situ gel has an advantage of providing sustained release of the drug agent.  In-situ gelling liquid suppositories using poloxamer 188 (26-30% W/W) as a suppository base with 10% W/W naproxen were prepared, the gelation temperature of these preparations were measured and they were all above the physiological temperature. Additives such as polyvinylpyrrolidin "PVP" ,hydroxylpropylmethylcellulose  "HPMC", sodium alginate and sodium chloride were used in concentration ranging from (0.25-1

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    Publication Date
    Sun Feb 24 2019
    Journal Name
    Iraqi Journal Of Physics
    Construction and performance study of a solar - powered hybrid cooling system in Iraq
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    The systems cooling hybrid solar uses solar collector to convert solar energy into the source of heat for roasting Refrigerant outside of the compressor and this process helps in the transformation of Refrigerant from the gas to a liquid state in two-thirds the top of the condenser instead of two-thirds the bottom of the condenser as in Conventional cooling systems and this in turn reduces the energy necessary to lead the process of cooling. The system cooling hybrid use with a capacity of 1 ton and Refrigerant type R22 and the value of current drawn by the system limits (3.9-4.2A), the same value of electric current calculated by the system are  Conventional  within this atmosphere of Iraq, and after taking different readings

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    Publication Date
    Mon Mar 01 2021
    Journal Name
    Iraqi Journal Of Physics
    Antibacterial and morphological properties of polypyrrole/silver nanocomposites synthesized by chemical oxidative polymerization
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    Polypyrrole/silver (PPy/Ag) nanocomposites was synthesized via a chemical oxidative method. The AFM analysis is performed to study the surface roughness, morphology and size distribution of the PPy particles and PPy-ag nanocomposites. The results indicated that as the concentration of Ag in the nanocomposite increases, the roughness also increases. The size of nanoparticles was also evaluated and found in the range of 15 nm to 125 nm. The PPy/Ag nanocomposites exhibited an effectiveness against Gram-negative Escherichia coli showing an inhibition zone of 4mm and displayed poor efficacy against Gram-positive Staphylococcus aureus. Based on given adequate antibacterial characteristics of PPy/Ag nanocomposites, it can be identified as a pro

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    Publication Date
    Thu Oct 01 2009
    Journal Name
    Iraqi Journal Of Physics
    Preparation Cadmium Telluride Compound and Study Structural Properties of thermal evaporation thin films
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    Polycrystalline ingots of cadmium telluride have been synthesized using the direct
    reaction technique, by fusing initial component consisting from pure elements in
    stoichiometric ratio inside quartz ampoule is evacuated 10-6 torr cadmium telluride has
    been grown under temperature at (1070) oC for (16) hr. was used in this study, the phases
    observed in growing CdTe compound depend on the temperature used during the growth
    process. Crystallography studies to CdTe compound was determined by X-ray diffraction
    technique, which it has zinc blend structure and cubic unit cell, which lattice constants is
    a=6.478
    oA

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    Publication Date
    Tue Sep 01 2020
    Journal Name
    Iraqi Journal Of Physics
    Biosynthesis of silver nanoparticles using Thyme Vulgaris leaves extract and its Antibacterial activity
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    In the current research, an eco-biosynthesis method for synthesizing silver nanoparticles (AgNPs) is reported using thymus vulgaris leaves (T. vulgaris) extracts. The optical and structural properties of the nanoparticles is determined using UV-visible, x-ray diffraction (XRD) and field emission scanning electron microscope (FESEM). In addition, the synthesis factors such as the temperature, the molar ratio of silver nitride and thymus vulgaris leaves extract have been investigated. The XRD pattern presented higher intensity for the five characteristic peaks of silver. FESEM images for same samples indicated that the particle size was distributed between 24-56 nm. In addition, it’s observed the formation of some aggregated Ag particles

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    Publication Date
    Mon Dec 30 2013
    Journal Name
    Iraqi Journal Of Chemical And Petroleum Engineering
    Kinetic Study and Simulation of Oleic Acid Esterification over Prepared NaY Zeolite Catalyst
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    Esterification considers the most important reaction in biodiesel production. In this study, oleic acid was used as a suggested feedstock in order to study and simulate production of biodiesel. The batch esterification reaction of oleic acid was carried out at various operating conditions; temperature from 40 to 70 °C, ethanol to oleic acid molar ratio from 3/1 and 6/1 and a reaction time up to 180 min.
    The catalyst used was prepared NaY zeolite, which is added to the reaction mixture as 2, 5 and 10 wt.% of oleic acid.
    The results show that the optimum conditions, gives 0.81 conversion of oleic acid, were 6/1 molar ratio of ethanol/oleic acid, 5 wt.% NaY relative to initial oleic acid, 70°C and 60 minutes. The activation energy o

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    Publication Date
    Thu Jun 01 2023
    Journal Name
    Baghdad Science Journal
    Batch and flow injection spectrophotometric methods for determination of Ceftazidime in pharmaceutical formulations
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    It is generally accepted that there are two spectrophotometric techniques for quantifying ceftazidime (CFT) in bulk medications and pharmaceutical formulations.  The methods  are described as simple, sensitive, selective, accurate and efficient techniques. The first method used an alkaline medium to convert ceftazidime to its diazonium salt, which is then combined with the 1-Naphthol (1-NPT) and 2-Naphthol (2-NPT) reagents. The azo dye that was produced brown  and red in color with absorption intensities of ƛmax 585 and 545nm respectively. Beer's law was followed in terms of concentration ranging from  (3-40) µg .ml-1 For (CFT-1-NPT) and (CFT-2-NPT), the detection limits were 1.0096 and 0.8017 µg.ml-1, respec

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