A simple, fast, and sensitive batch and flow injection spectrophotometric
methods have been developed for the determination of clonazepam(CZP) in pure
form and in pharmaceutical preparations. The proposed methods are based on the
oxidative coupling reaction of the reduced clonazepam using Zn powders and conc.
HCl with payrocatechol and in the presence of ferric sulphate. The resulting reddish
colored product had a maximum absorbance at 515 nm. The optimum reaction
conditions and other analytical parameters have been evaluated . The linear ranges
for the batch and FI methods determination of CZP were 0.5-32, 50-400 μg mL-1
and the detection limits were 0.193, 22.60 μg mL-1 for both methods respectively.
Statis

In this paper, turbidimetric and reversed-phase ultra-fast liquid chromatography (UFLC) methods were described for the quantitative determination of ephedrine hydrochloride in pharmaceutical injections form. The first method is based on measuring the turbidimetric values for the formed yellowish white precipitate in suspension status in order to determine the ephedrine hydrochloride concentration. The suspended substance is formed as a result of the reaction of ephedrine hydrochloride with phosphomolybdic acid which was used as a reagent. The physical and chemical characteristics of the complex were investigated. The calibration graphs of ephedrine were established by turbidity method. While the second method (UFLC) was conducted using the

In this study, a new, rapid and sensitive batch and flow injection-merging zones spectrophotometric methods for the determination of hydroquinone in a pure material and in pharmaceutical preparation were proposed. These methods were based on the oxidative-coupling reaction of HQ with 2,4-dinitrophenylhydazine (DNPH) in the presence of sodium periodate and sodium hydroxide to form a dark brown water slouble dye that is stable and has maximum absorption at 530 nm, graphs of absorbance versus concentration show that Beer's low is obeyed over the concentration rang of 1-40 and 3-300 μg.ml-1 of hydroquinone, with detection limits of 0.162 and 0.510 μg.ml-1 of hydroquinone for batch and FIA methods, respectively. The optimized FIA system is

In this research, a study is introduced on the effect of several environmental factors on the performance of an already constructed quality inspection system, which was designed using a transfer learning approach based on convolutional neural networks. The system comprised two sets of layers, transferred layers set from an already trained model (DenseNet121) and a custom classification layers set. It was designed to discriminate between damaged and undamaged helical gears according to the configuration of the gear regardless to its dimensions, and the model showed good performance discriminating between the two products at ideal conditions of high-resolution images.

So, this study aimed at testing the system performance at poor s

In this research, a study is introduced on the effect of several environmental factors on the performance of an already constructed quality inspection system, which was designed using a transfer learning approach based on convolutional neural networks. The system comprised two sets of layers, transferred layers set from an already trained model (DenseNet121) and a custom classification layers set. It was designed to discriminate between damaged and undamaged helical gears according to the configuration of the gear regardless to its dimensions, and the model showed good performance discriminating between the two products at ideal conditions of high-resolution images. So, this study aimed at testing the system performance at poo

       Performance issues could be appearing from anywhere in a computer system, finding the root cause of those issues is a troublesome issue due to the complexity of the modern systems and applications. Microsoft builds multiple mechanisms to make their engineers understand what is happening inside All Windows versions including Windows 10 Home and the behavior of any application working on it whether Microsoft services or even third-party applications, one of those mechanisms is the Event Tracing for Windows (ETW) which is the core of logging and tracing in Windows operating system to trace the internal events of the system and its applications. This study goes deep into internal process activities to investigat

This study aims to evaluate reservoir characteristics of Hartha Formation in Majnoon oil field based on well logs data for three wells (Mj-1, Mj-3 and Mj-11). Log interpretation was carried out by using a full set of logs to calculate main petrophysical properties such as effective porosity and water saturation, as well as to find the volume of shale. The evaluation of the formation included computer processes interpretation (CPI) using Interactive Petrophysics (IP) software.  Based on the results of CPI, Hartha Formation is divided into five reservoir units (A1, A2, A3, B1, B2), deposited in a ramp setting. Facies associations is added to well logs interpretation of Hartha Formation, and was inferred by a microfacies analysis of th

Intrusion detection system is an imperative role in increasing security and decreasing the harm of the computer security system and information system when using of network. It observes different events in a network or system to decide occurring an intrusion or not and it is used to make strategic decision, security purposes and analyzing directions. This paper describes host based intrusion detection system architecture for DDoS attack, which intelligently detects the intrusion periodically and dynamically by evaluating the intruder group respective to the present node with its neighbors. We analyze a dependable dataset named CICIDS 2017 that contains benign and DDoS attack network flows, which meets certifiable criteria and is ope

Carbon monoxide (CO) plays an important indirect greenhouse gases due to its influences on the budgets of hydroxyl radicals (OH) and Ozone (O3). The atmospheric carbon monoxide (CO) observations can only be made on global and continental scales by remote sensing instruments situated in space. One of instrument is the Measurements of Pollution in the Troposphere (MOPITT), which is designed to measure troposphere CO and CH4 by use of a nadir-viewing geometry and was launched aboard the Earth Observing System (EOS) Terra spacecraft on 18 December 1999. Results from the analysis of the retrieved monthly (1ºх1º) spatial grid resolution, from the MOPITT data were utilized to analyze the distribution of CO surface mixing ratio in Iraq for th