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Synthesis Of New Asymmetrical Pyromellitdiimides Derived From Pyromellitic Dianhydride

This work involves the synthesis and characterization of asymmetrical pyromellitdiimide
derivatives [IV]a-f
by four sequence steps selective reaction . One mole of pyromellitic dianhydride
was reacted with one mole of various primary aromatic amines [ 4-nitro aniline , 4-chloro aniline , 4-toludine and 4-anisidine] in excess of dry acetone to produce six compounds (N-substituted-pyromellitamic monoacid) [I]a-f . These new compounds [I]a-d were converted to the corresponding
N- substituted- pyromellitmonoimide [II]a-d via their heating at (80-90)
0
C in sodium acetate-acetic
anhydride mixture .
The compounds [II]a-f
were allowed to react with one mole of another primary amines in
excess of dry acetone to give new derivatives of amic acid [II]a-d followed by intramolecular
cyclization reaction of these compounds [IV]a-f in sodium acetate-acetic anhydride system to yield the
desired asymmetrical pyromellitdiimide derivatives [IV]a-f
, the above reactions can be summarized in
Scheme 1.
All the synthesized compounds have been studied and charachterized by their melting points
, FTIR , and
1
HNMR spectroscopy (for some of them)

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Publication Date
Sun Apr 24 2022
Journal Name
Journal Of The Faculty Of Medicine Baghdad
use of dietary supplement in Iraq

Background: Dietary supplementation is a common strategy to achieve a specific health status or performance benefit. The aim of this study was to describe the use of dietary supplement in Iraqi genders.

Patients and Methods:  several questions on dietary supplement use were asked as a part of single performed on 112 female and 247 women aged 35–74 years in 2021 .n = 359) ,reported the frequency and prevalence of supplement use by sex and type of supplement .

Results: the mean percentage of dietary supplement use varied among female and men. Use was higher in women than in men. Vitamins, minerals were the predominant types of supplements reported, but the

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Publication Date
Wed Feb 20 2019
Journal Name
Political Sciences Journal
Policies governing the mechanisms of referees

The importance of research stems from the prominent role of leaders in the political, administrative, economic and societal spheres in general, which requires highlighting this angle. Research Hypothesis Modern policies work with mechanisms that limit the clear role of governors and transform the ruler into an executive man. It can be assumed that the type of public policy of the state is the only criterion that transfers the ruler from a ruler to an executive.

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Publication Date
Fri Aug 28 2020
Journal Name
Iraqi Journal Of Science
Maximal Ideal Graph of Commutative Rings

In this paper, we introduce and study the notion of the maximal ideal graph of a commutative ring with identity. Let R be a commutative ring with identity. The maximal ideal graph of R, denoted by MG(R), is the undirected graph with vertex set, the set of non-trivial ideals of R, where two vertices I1 and I2 are adjacent if I1 I2 and I1+I2 is a maximal ideal of R. We explore some of the properties and characterizations of the graph.

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Publication Date
Sun Apr 01 2007
Journal Name
Journal Of The Faculty Of Medicine Baghdad
Causes of Vomiting in Hospitalized Children

Background: vomiting is a very common symptom of disease in childhood, it occurs both in gastrointestinal and non-gastrointestinal diseases.
Objectives: Our aim of the study was to find out the causes of vomiting in different age group, the improper management of vomiting in daily practice and to emphasis on the usefulness of imaging study in the diagnosis.
Methods: A prospective study was carried out on patients presented with vomiting admitted to Children Welfare Teaching Hospital from the first of Dec. 2001 to the end of April 2002 .The age ranged between early neonatal periods to 12 years of age.
Reults: A total of 100 child were included in this study,(65) male (35) female male to female ratio 

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Publication Date
Tue Mar 28 2017
Journal Name
Iraqi Journal Of Pharmaceutical Sciences ( P-issn 1683 - 3597 E-issn 2521 - 3512)
Antimicrobial Activity of Hydroxymatairesinol (HMR) Lignan

Lignans are natural products widely distributed in the plant kingdom. They are composed of two β-β-linked phenylpropane (shikimate-derived biogenetic subunits). Although the backbone of lignans is composed of phenylpropane units, there is enormous diversity in the structure of lignans leading to different classes of lignans, such as γ-butyrolactone derivatives, eg. Hymatairesinol, bicyclooctadiene derivatives, e.g. pinoresinol, tetrahydrofuran derivatives e.g.lariciresinol, di-arylbutandiol derivatives, e.g. secoisolariciresinol. Introduction of a further carbon –carbon linkage leads to a class of lignans collectively known as cyclolignans such as tetrahydro-naphthalene derivatives, for example podophyllotoxin. Lignans ha

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Publication Date
Tue Dec 01 2020
Journal Name
Baghdad Science Journal
A Generalization of t-Practical Numbers

This paper generalizes and improves the results of Margenstren, by proving that the number of -practical numbers  which is defined by   has a lower bound in terms of . This bound is more sharper than Mangenstern bound when  Further general results are given for the existence of -practical numbers, by proving that the interval contains a -practical for all

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Publication Date
Wed Jun 01 2022
Journal Name
Political Sciences Journal
The political thought of Robert Nozick

  Robert Nozick is an American thinker who formulated his political theory in his book (Anarchy, State, Utopia) in 1974, which included his most important main ideas represented in the emergence of (The Minimal State) as well as (Entitlement Theory), through which he expressed his rejection of stereotypical distributive justice theories such as equality In Marxism and social liberalism, his ideas were characterized by a very extreme individualist tendency, and his ideas contributed to supporting the neo-liberal trend.     

 

             

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Publication Date
Mon Jun 17 2019
Journal Name
Ibn Al-haitham Journal For Pure And Applied Sciences
Consolidation Behaviour of SiC Ceramic Composites

Three composite grinding wheel series were prepared using three different ceramic binders . Two of the three series behaved in typical ceramic — type manner in their consolidation behaviour , while the third deviated strongly . The measured mechanical properties behaved in a similar manner . The main reason was found tobe the way the binder material interacts with the SiC — particles . The results are discussed in terms of the rol played by the binder in shaping the final mechanical properties of the composites .

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Publication Date
Thu Mar 16 2017
Journal Name
Ibn Al-haitham Journal For Pure And Applied Sciences
Optical Properties of PVA/K2CrO4 Composite

     The change in the optical properties for samples of pure PVA and PVA /K2CrO4composite have been studied .The samples were prepared with different percentage (1,3,5,and 7)%wt of K2CrO4 by casting method technique .In this work ,we are study the absorption ,reflectance spectra ,absorption  coefficient, energy gap ,extinction coefficient ,and transmittance spectra as a function of wavelength range (200-800)nm ,Also  real and imaginary part of dielectric constant have been studied in the range of wave length .The results exhibit the optical properties change by the increase of K2CrO4 concentration, and the values of energy gap for indirect transitions decrease by the increase of the concentration of  K2CrO4

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Publication Date
Wed Jun 29 2022
Journal Name
Journal Of The College Of Education For Women
Cognitive Motive of the Kindergarten Child

Encouraging children towards the cognitive motivation through the discovery and knowledge of the environment around them is essential. Thus, during the two researchers’ supervision of the practical lessons that involved the female students’ application of their experience in the Applied Kindergarten Laboratory, it has been noticed that there was a difference in the cognitive motivation of kindergarten children. In order to reinforce the research problem, the two researchers sent an open questionnaire to a sample of randomly selected kindergarten teachers from Al-Karkh and Al-Rasafa sides. The responses collected accentuated the researchers’ sense of the existing problem. To achieve the aim of the study represented by examining the

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