A reliable differential pulse polarographic (DPP) method has been developed and applied for the determination of ibuprofen IBU in dosage form with dropping mercury electrode (DME) versus Ag/AgCl. The best peak was found at cathodic peak of -1.18 V in phosphate buffer at pH=4 and 0.025M of KNO3 as supporting electrolyte. In order to obtaine the highest sensitivity, instrumental and experimental parameters were examined including the type and concentration of supporting electrolyte, pH of buffer solution, pulse amplitude and voltage step time. Diffusion current showed a direct linear relationship to ibuprofen concentration in the range of (5 – 30) μg. mL-1 (2.43× 10-5 – 1.45 × 10-4 mol·L–1) with correlation coefficient r= 0.9999, detection limit (S/N = 3) =3.40 μg. mL-1 (1.65 × 10-5 mol·L–1) and the value of precision in terms of relative standard deviation RSD%, ranged between 0.374-0.5176 %. The established DPP method offers an excellent analytical figure of merits as well as its successful applicability to examine two commercial drug forms (tablet and suspension) for the determination of ibuprofen.
The new sustainable development goals set by the UN include a goal of making cities inclusive, safe, sustainable, and resilient. Cities are growing at huge rates, and conditions of deteriorating QOL̛s are increasing in the form of poor access to services, and slums are remarkable, especially in the cities of the Middle East; hence, the research problem can arise from a lack of knowledge regarding the in determination of a way to assess the resilience of cities to develop mechanisms that will improve the quality of urban life. In this study, a tool called CRF has been applied for the assessment of the city's resilience principles of health and quality of life, economics and social, infrastructure and environmental systems, and the principle
... Show MoreTwo different oxidative desulfurization strategies based on oxidation/adsorption or oxidation/extraction were evaluated for the desulfurization of AL-Ahdab (AHD) sour crude oil (3.9wt% sulfur content). In the oxidation process, a homogenous oxidizing agent comprising of hydrogen peroxide and formic acid was used. Activated carbons were used as sorbent/catalyst in the oxidation/adsorption process while acetonitrile was used as an extraction solvent in the oxidation/extraction process. For the oxidation/adsorption scheme, the experimental results indicated that the oxidation desulfurization efficiency was enhanced on using activated carbon as catalyst/sorbent. The effects of the operating conditions (contact time, temperat
... Show MoreMonthly rainfall data of Baghdad meteorological station were taken to study the time behavior of these data series. Significant fluctuation,very slight increasing trend and significant seasonality were noticed. Several ARIMA models were tested and the best one were checked for the adequacy. It is found that the SEASONAL ARIMA model of the orders SARIMA(2,1,3)x(0,1,1) is the best model where the residual of this model exhibits white noise property, uncorrelateness and they are normally distributed. According to this model, rainfall forecast for four years was also achieved and showing similar trend and extent of the original data.
Abstract
In this study, modified organic solvent (organosolv) method was applied to remove high lignin content in the date palm fronds (type Al-Zahdi) which was taken from the Iraqi gardens. In modified organosolv, lignocellulosic material is fractionated into its constituents (lignin, cellulose and hemicellulose). In this process, solvent (organic)-water is brought into contact with the lignocellulosic biomass at high temperature, using stainless steel reactor (digester). Therefor; most of hemicellulose will remove from the biomass, while the solid residue (mainly cellulose) can be used in various industrial fields. Three variables were studied in this process: temperature, ratio of ethano
... Show MoreCharacteristic evolving is most serious move that deal with image discrimination. It makes the content of images as ideal as possible. Gaussian blur filter used to eliminate noise and add purity to images. Principal component analysis algorithm is a straightforward and active method to evolve feature vector and to minimize the dimensionality of data set, this paper proposed using the Gaussian blur filter to eliminate noise of images and improve the PCA for feature extraction. The traditional PCA result as total average of recall and precision are (93% ,97%) and for the improved PCA average recall and precision are (98% ,100%), this show that the improved PCA is more effective in recall and precision.
The speech recognition system has been widely used by many researchers using different
methods to fulfill a fast and accurate system. Speech signal recognition is a typical
classification problem, which generally includes two main parts: feature extraction and
classification. In this paper, a new approach to achieve speech recognition task is proposed by
using transformation techniques for feature extraction methods; namely, slantlet transform
(SLT), discrete wavelet transforms (DWT) type Daubechies Db1 and Db4. Furthermore, a
modified artificial neural network (ANN) with dynamic time warping (DTW) algorithm is
developed to train a speech recognition system to be used for classification and recognition
purposes. T