في تعزيز بيئة الانتاج الرشيق استخدام اسلوب S -5
دأبت الأسطورة تفسر للإنسان أصل النشوء والتطور، والقص الأسطوري لنتاج أبراهام ركلسون في قصة "عمود النوارس" من المجموعة القصصية "بيت البريق" يفسر ضمنا أصول يهودية للسكان الأصليين في الولايات المتحدة، سردها ركلسون بأسلوب توراتي نحوا ومعنى لمقاربة النص الأدبي من النص في كتاب المورمون والتوراة. إن النص محاولة تعويضية لليهود المهاجرين للشعور بالألفة في المكان. وظف ركلسون أحداث تاريخية ذكرت في كتاب المورمون ل
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البحث يحدد القيم التي تم التركيز عليها والإهتمام بها في كتاب القراءة الكوردية للصف الثاني في المرحلة الاساسية المقرر, وكذلك القيم التي لم يتم التركيز عليها أو الإهتمام بها و التي تم تجاهلها بصورة كاملة في نفس الكتاب. وتحديد عدد الصفحات التي تم تخصيصها مقارنة مع مساحات الصور التوضيحية والفنون الأدبية في الكتاب المقرر
عرفت لغة الصحافة بأنها الجامعة لصحة الفصحى وسلامتها ووضوح العامية وبساطتها ؟ وتشكل عقبات الفهم في الكتابة الاخبارية محور البحث الى سوء الفهم لدى المتلقي حيث وضع الباحث تساؤلا رئيساً يغطي على كل الجوانب مشكلة البحث وسيتلزم الاجابة عنه. ماعقبات الفهم في الكتابة الاخبارية الاستنتاجات التي توصل إليها الباحث: 1. ركزت الصحيفة على المصطلحات السياسية بااعتبارها صحفية سياسية يوميه 2. استخدمت الصحيفة المصطلحات الت
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لا شك أن البلاغة تمثل الركن الأساس في إعجاز القرآن الكريم وبها تسمى معجزة (الإذعان) إذ عجز أفصح العرب عن معارضته أو حتى مجاراته أو حتى كتابة سورة من سوره الرصينة والبليغة المعجزة , لذلك شغل العلماء : (مفسرون , بلاغيون , نحويون , ...) بهذا العلم , فأخذ كل منهم يدرسه بطريقة مختلفة ومنهاج مغاير ليزيد من هذا البحر المديد, ولأجل الكشف عن المزيد من لآلئ القرآن الكامنة وال
... Show More4-(((4-hydroxy-3,5-dimethoxybenzyl)oxy)methyl)benzoic acid was synthesized from multisteps and converted to their corresponding hydrazide. The corresponding hydrazide was cyclized to their corresponding 5-amino-1,3,4-oxadizole. Newly Schiff bases (7a-7e) were synthesized from reaction the 5-amino-1,3,4-oxadizole with several substituted of 4-hydroxybenzylaldehyde. The resulting compounds were characterized based on their IR, 1H-NMR, 13C-NMR, and HRMS data. 2,2-Diphenyl-1-picrylhydrazide (DPPH) and ferric reducing antioxidant power (FRAP) assays were used to test the antioxidant properties of the synthesized compounds. Compound 7d and 7e exhibited significant free-radical scavenging ability in both assays.
Pathogenic microorganisms are becoming more and more resistant to antimicrobial agents. So the synthesis of new antimicrobial agents is very important. In this work, new 5-fluoroisatin-chalcone conjugates 5(a–g) were synthesized based on previous research that showed the modifications of the isatin moiety led to the synthesis of many derivatives that have antimicrobial activity. 4-aminoacetophenone reacts with 5-fluoroisatin to form Schiff base (3), which in turn reacts with two different groups of aromatic (carbocyclic and heterocyclic) aldehydes 4(a–g) separately to form the final compounds 5(a–g). Proton-nuclear magnetic resonance (¹H-NMR) and Fourier-transform infrared (FT-IR) spectroscopy were used to confirm the chemic
... Show MoreThe aim of the present work is the synthesis of new carbohydrate derivatives containing 1,2,4-triazole from D-fructose . To obtain these derivatives, the diacetone fructose (1 ) was chosen as the starting material, which was obtained from the reaction of anhydrous fructose with dry acetone in presence of anhydrous ferric chloride. Oxidation of ( 1) with potassium permanganate in potassium hydroxide solution gave the acid ( 2). Esterification of the acid with dimethyl sulphate gave the methyl ester (3 ). Treatment of the methyl ester (3 ) with hydrazine hydrate gave the hydrazide (4 ), which is the desired Chiron. The hydrazide (4 ) was used for the preparation of 1,2,4-triazole-5-one (6 ) derivative. These compounds was synthesized by the i
... Show MoreNanocrystalline micro-mesoporous ZSM/MCM-41 composite was synthesized using alkaline treatment method and two step of crystallization in poly tetraflouroethylene (PTFE) lined autoclave. The synthesized zeolites was characterized by X-Ray diffraction (XRD), Scanning electron microscopy (SEM), Transmission electron microscopy (TEM), Atomic force microscopy (AFM), Fourier transport infrared (FTIR), and N2 adsorption-desorption (BET). It was approved that the best results for alkaline leaching can be got with 1.5M NaOH solution. High surface (BET) area of 630 m2/g with pore volume of 0.55 cm3/g has been got. AFM reports showed a nano-level size for average particle size of 50nm.
Nitrogen heterocycles are of a special interest because they constitute an important class of natural and non natural products, many of which exhibit useful biological activities.Among these nitrogen heterocycles are 1, 3, 4-thiadiazole containing compounds. The therapeutic effects of these derivatives have been well studied for a number of pathological conditions including inflammation, pain, or hypertension. Moreover, synthesis of thiadiazoles has attracted wide-spread attention due to their diverse applications as antibacterial, anticancer, antifungal anti-inflammatory and antidepressant agents.According to this information’s new derivatives of 1, 3, 4-thiadiazole were designed and synthesized and in the hope of having some act
... Show MoreAniline and its derivatives are common contaminants in various wastewaters and represent a serious worry for societies health and a challenge to ecologists due to their dangers effects on to the human health.
ZSM-5 zeolite was prepared from locally available materials (kaolin and rice husk) for adsorption of aniline from synthetic wastewater. Characterization of the prepared zsm-5, kinetics and thermodynamic of the adsorption process were investigated.
The characterization results of the prepared zsm-5 zeolite showed that the surface area was 270.1 m2/g and pore volume 0.21828 cm3/g. The silica to alumina ratio (Si/Al) was 166. 47 and the sodium content was 11 wt. %. The atomic force microscope (AFM)
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