Background: the aim of this study was to evaluate the effect of different surface acids treatments (37%phospjoric acid, 5%hydrofluoric acid, 1.23 acidulated phosphate fluoride) of feldspathic ceramic VITA 3D MASTER , and the effect of thermocycling on shear bond strength using a ceramic repair kit (ivoclar/vivadent). Material and Methods: sixty Nickel-Chromium metal base plates were prepared(9mm diameter,3mm depth) using lost wax technique, 2mm thick layer of ceramic(VITA 3D MASTER) fused to metal plates, all specimens were embedded in acrylic resin blocks except their examined surfaces and divided into 3 main groups 20 specimens each, Grp A: treatment with 37%phosphoric acid for 2 mins, Grp B: etching with 5% hydrofluoric acid for 2mins, Grp C: etching with 1.23% acidulated phosphate fluoride for 10 mins; monobond-plus, heliobond, resin composite(Tetric EvoCeram) were applied to each specimen according to manufacturer's instruction using transparent split mold(5mm diameter, 4 mm height); specimens were stored in 37OC distilled water for 12 weeks, 10 specimens of each group were subjected to thermocycling between 5 oC and 55 o C for 800 cycles with 30s dwell time; shear bond strength was determined by a universal testing machine (instron 1122) at a cross head speed 0.5mm/min; One way ANOVA test, LSD test and student-t test were used to analyze shear bond strength. Results: Mean shear bond strength values for the tested groups were: A1= 11.65±0.68 Mpa, A2=10.88±0.58 Mpa, B1=17.93±0.41 Mpa, B2=17.42±0.35 Mpa, C1=15.17±0.61 Mpa, C2=14.51±0.48 Mpa ; one way ANOVA test showed highly significant difference among groups; LSD test revealed that the use of 5% HF for ceramic surface treatment(GB) was highly significant than the treatment with 37%PA(GA) or 1.23%APF(GC) respectively and the use of 1.23%APF(GC) was highly significant than the use of 37%PA(GA); Student t- test showed a significant difference between subgroups of the same group with and without thermocycling. Conclusion: ceramic surface treated with 5% HF acid for 2 mins recorded the highest shear bond strength, followed by surface treatment with 1.23% APF for 10 mins, most specimens treated with 5%HF showed cohesive failure with in ceramic while specimens treated with 1.23%AFP showed more (adhesive/cohesive) failure than adhesive or cohesive alone, and specimens treated with 37% PA showed nearly 50:50 adhesive and combination failure, thermocycling reduced the bond strength of each group significantly
In this research a study of the effect of quality, sequential and directional layers for three types of fibers are:(Kevlar fibers-49 woven roving and E- glass fiber woven roving and random) on the fatigue property using epoxy as matrix. The test specimens were prepared by hand lay-up method the epoxy resin used as a matrix type (Quick mast 105) in prepared material composit . Sinusoidal wave which is formed of variable stress amplitudes at 15 Hz cycles was employed in the fatigue test ( 10 mm )and (15mm) value 0f deflection arrival to numbers of cycle failure limit, by rotary bending method by ( S-N) curves this curves has been determined ( life , limit and fa
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The petroleum industry faces a significant problem in enhanced oil recovery (EOR) from carbonate reservoirs because of their mostly oil-wet character, which restricts hydrocarbon extraction. To better understand how surfactant-polymer techniques can enhance oil recovery, this study investigates the effectiveness of polyvinyl alcohol (PVA) as a stand-alone agent and the function of ionically modified smart water on carbonate properties. The study focuses on its effect on critical parameters essential for effective oil displacement and recovery, such as wettability alteration, interfacial tension, and surface tension (ST) using different brines (smart water). The ability of the polymer PVA to lower interfacial and surface tensi
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Background: Poly propylene fibers with and without silane treatment have been used to reinforce heat cure denture base acrylic but, some mechanical properties like transverse strength, impact strength, tensile strength, hardness, wear resistance and wettability. Which are related to the clinical use of the prosthesis are not evaluated yet. The aim of the study is to identify the influence of incorporation of treated and untreated fibers on these properties Materials and methods: Eighty four heat cure acrylic specimens were constructed by conventional flasking technique. They were divided into six groups according to the tests and each group was subdivided into two subgroups control and experimental groups (seven samples for each subgroup
... Show MoreThe effect of different doping ratio (0.3, 0.5, and 0.7) with thickness in the range 300nmand annealed at different temp.(Ta=RT, 473, 573, 673) K on the electrical conductivity and hall effect measurements of AgInTe2thin film have and been investigated AgAlxIn(1-x) Te2 (AAIT) at RT, using thermal evaporation technique all the films were prepared on glass substrates from the alloy of the compound. Electrical conductivity (σ), the activation energies (Ea1, Ea2), Hall mobility and the carrier concentration are investigated as a function of doping. All films consist of two types of transport mechanisms for free carriers. The activation energy (Ea) decreased whereas electrical conductivity increases with increased doping. Results of Hall Effect
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This study deals with the estimation of critical load of unidirectional polymer matrix composite plates by using experimental and finite element techniques at different fiber angles and fiber volume fraction of the composite plate.
Buckling analysis illustrated that the critical load decreases in nonlinear relationship with the increase of the fiber angle and that it increases with the increase of the fiber volume fraction.
The results show that the maximum value of the critical load is (629.54 N/m) at (q = 0°) and (Vf = 40 %) for the finite element method, while the minimum val
... Show MoreThe use of composite materials has vastly increased in recent years. Great interest is therefore developed in the damage detection of composites using non- destructive test methods. Several approaches have been applied to obtain information about the existence and location of the faults. This paper used the vibration response of a composite plate to detect and localize delamination defect based on the modal analysis. Experiments are conducted to validate the developed model. A two-dimensional finite element model for multi-layered composites with internal delamination is established. FEM program are built for plates under different boundary conditions. Natural frequencies and modal displacements of the intact and damaged
... Show MoreIn this paper, the static analysis for finding the best location of boxes inside the composite wing-box structure has been performed. A software ANSYS (ver.11) was used to analyses the Aluminum wing to find the maximum stresses reached in. These results are used as a base for the composite wingbox to find the numbers of layers and location of the box beam and its dimensions so that the composite wingbox may carry the same loading conditions in the Aluminum wing. Analysis showed that a composite wingbox having two boxes is better than the single or triple boxes wing based on stress to weight ratio. Mass saving of (40%) had been achieved when composite wing-box is used instead of Aluminum wing.
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