A simple, rapid and sensitive method for the analysis of Atenolol in pure and pharmaceutical preparation as an alternative analytical procedure were developed by continuous flow injection analysis via turbidimetric (T180o) and scattered light effect at two opposite position (2N90o). The method is based upon the formation of white precipitate for the ion pair compound by phosphomolybidic acid with Atenolol in aqueous medium. The precipitate is measured via the attenuation of incident light and scattering of the incident light in two opposite direction namely +90o and -90o angle were measured. Chemical and physical parameters were investigated. The linearity of Atenolol is ranged from (0.1-11) mmol.L-1, with correlation coefficient r=0.9938, lower limit of detection (LOD) 0.05 mmol.L-1(3SB)(S/N=3) for n=13 and the relative standard deviation for 7 mmol.L-1 Atenolol solution is lower than 3% (n=7). The method was applied successfully for the determination of atenolol in three pharmaceutical drugs. A comparisons were made between the newly developed method of analysis with the classical method ( uv-spectrophotometry at wave length 274nm) of analysis using the standard addition method via the use of t- test. It shows that there was no significant difference at α=0.05(95% confidence) between the two methods. Therefore the newly developed method can be accepted as an alternative method for the analysis of Atenolol, in addition to comparison between the official value and the calculated value for both methods
An electrolytic process for the removal of Zn(II) from aqueous solution using a parallel amalgamated copper screens cathode operated in the flow through mode is proposed. The current-potential curves recorded at a rotating amalgamated copper disc electrode were used to determine diffusion coefficient of Zn(II). The performance of electrolytic reactor was investigated by using different flow rates at initial zinc ion concentration(48 mg/L). Taking into account the residential Zn(II) concentration, the best results were obtained for cathode potential of (-1.35 V vs. SCE) at flow rate (320 L/h). Zinc ion concentration was found to decrease from 48 mg/L to 1 mg/L during 120 min. of electrolysis. The experimental data are well correlate
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Although many technological improvements are occurring in power production worldwide, power plants in third world countries are still using old technologies that are causing thermal pollution to the water bodies. Power facilities that dump hot water into water bodies are damaging aquatic life. In the study, the impact of the Al Dora thermal power plant on a nearby stretch of Tigris River in Baghdad city was assessed by measuring the temperature of the disposed of hot water in various cross-sections of the selected stretch of Tigris River, including measuring the thermal mixing length. The measurements were conducted in winter, spring, and summer. For field measurements, it was found that the impact of recovery distances
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Eruca sativa (jarjeer) is an annual herb (family Brassicaceae), which contains a wide range of chemicals and minerals with nutraceutical and organoleptic characteristics. Jarjeer was generally used as a food and traditionally mainly consumed due to its aphrodisiac properties. This crop known to contain various phytochemicals such as flavonoids, phenolic acids, terpens, carotenoids, tannins, glycosides, saponins, sterols, alkaloids, and other secondary metabolites. In leaves, kaempferol and its derivatives, glucosativin, are the main flavonoids and glucosinolate, respectively, while erucic acid and glucoerucin are the main fatty acid and glucosinolate, respectively. Medicinally, the plant has antibacterial, antidiabetic, antihyperten
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(29)
This research had been conducted to investigate response of two Antirrhinum majus L. varieties, tall and dwarf variety to foliar application of Indole 3-acetic acid and Benzyladenin at (0, 60, 120, 180, 240 ppm), through plant height, fresh weight, dry weight of shoot, length of inflorescence (raceme), number of flowering buds per raceme and chlorophyll content in leaves at complete flowering stage.
Results of treatment of the tall variety with IAA and BA showed that IAA had the highest significant increase in plant height, while BA had the highest significant increase in chlorophyll content .Increasing concentrations of both IAA and BA resulted a significant increase in all growth parameters, this was obvious in floweri
... Show MoreBackground:Â Various fluids in the oral environment can affect the surface roughness of resin composites. This in vitro study was conducted to determine the influence of the mouth rinses on surface roughness of two methacrylate-based resin (nanofilled and packable composite) and siloraine-based resin composites.
Materials and methods: Disc-shaped specimens (12 mm in diameter and 2mm in height) were prepared from three types of composi
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Abstract :In this study, amygdaline in Iraqi plant seeds was extracted and isolated from their seeds matrix using reflux procedure and subsequently identified and determined by high performance liquid chromatography (HPLC) on reversed phase column of LC-18 (150mm x 4.6mm, 5?m )with actonitrile :water ( 50 : 50 ) as mobile phase at flow rate of ( 0.5 mL/min ) and detection at wavelength of 215 nm.The experimental results indicated that the linearity of calibration is in the range of 1.0-30.0 mg L-1amygdaline with the correlation coefficient of 0.9949. The limit of detection (LOD) and limit of quantitation (LOQ) for amygdaline were of 0.88 and 2.93 mg L-1 in standard pure sample. The mean recovery percent is 97.34±0.58 at 95% confidence inte
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(2)
The general objective of surface shape descriptors techniques is to categorize several surface shapes from collection data. Gaussian (K) and Mean (H) curvatures are the most broadly utilized indicators for surface shape characterization in collection image analysis. This paper explains the details of some descriptions (K and H), The discriminating power of 3D descriptors taken away from 3D surfaces (faces) is analyzed and present the experiment results of applying these descriptions on 3D face (with polygon mesh and point cloud representations). The results shows that Gaussian and Mean curvatures are important to discover unique points on the 3d surface (face) and the experiment result shows that these curvatures are very useful for some
... Show MoreThe effects of root exudates of two sunflower cultivars (Shumoose and Sin
Altheeb) were studied on companion weeds during the growing season of 2012.
Results showed the ability of both cultivars to affect weed population and growth
with the superiority of cultivar Shumoose in suppression of weed density at 60 and
120 days after sowing compared to Sin Altheeb. Weed biomass was significantly
reduced up to 90 and 71% by Shumoose and Sin Altheeb cultivars, respectively.
Stair case experiment indicated that root exudates of Shumoose cultivar showed
more suppression to weeds than Sin Altheeb giving additional evidence for the
superiority of Shumoose cultivar in its allelopathic weed suppression. Chemical
analysis by
In this study, lateral groundwater inflow was examined, according to the phenomena of groundwater mixing, groundwater flow and groundwater chemistry. The study region is composed of different aquifer systems; including karst-fracture media (Rattga-Jeed carbonates aquifer), fissure–porous media (Mullusi, Mullusi-Ubaid, Hartha-Rutba, and Digma-Tayarat aquifers) and porous media (Permo-carboniferous clastics rocks of Ga’ra aquifer).The aquifers are vertically super-imposed or of lateral contacts make open hydraulic connection between aquifers system. There is a severe shortage of water resources in the region because of rare precipitation and strong evapotranspiration. These conditions have hampered eco-environm
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