Aflatoxin B1 (AFB1) is a mycotoxin produced mainly by fungi Aspergillus flavus in food and animals feed. It is considered as a carcinogenic toxin for human and animals. The current study is designed to investigate the incidence of mycoflora in twenty four samples of local stored maize collected from Iraqi governorates; investigate the presence of aflatoxin B1 on these samples using TLC and ELISA techniques. The fungi recovered from maize samples were Aspergillus flavus (18.57 % ), Fusarium spp. (12.8 % ), A. ocraceus (9.96 % ) , A. terrus (9.07 % ), A. fumigatus (8.46 % ) , Alternaria spp. (6.40 % ) Rhizopus spp. (4.98 % ), A. niger spp., A. oryzae spp. (4.80 % ), Penicillium spp. (4.53 %) A. versicolor spp., Rhizoctonia spp. (4.27 %), A. tamari and Mucor spp. (3.20 %). Aflatoxin B1 was present in twelve samples of stored maize collected from Iraqi governorate and the concentration of toxin ranged between 2.30 to 30 ppb using TLC technique and 270 to 500 ppb using ELISA technique.
The effect of thickness variation on some physical properties of hematite α-Fe2O3 thin films was investigated. An Fe2O3 bulk in the form of pellet was prepared by cold pressing of Fe2O3 powder with subsequent sintering at 800 . Thin films with various thicknesses were obtained on glass substrates by pulsed laser deposition technique. The films properties were characterized by XRD, and FT-IR. The deposited iron oxide thin films showed a single hematite phase with polycrystalline rhombohedral crystal structure .The thickness of films were estimated by using spectrometer to be (185-232) nm. Using Debye Scherrerś formula, the average grain size for the samples was found to be (18-32) nm. Atomic force microscopy indicated that the films had
... Show MoreThe reaction oisolated and characterized by elemental analysis (C,H,N) , 1H-NMR, mass spectra and Fourier transform (Ft-IR). The reaction of the (L-AZD) with: [VO(II), Cr(III), Mn(II), Co(II), Ni(II), Cu(II), Zn(II), Cd(II) and Hg(II)], has been investigated and was isolated as tri nuclear cluster and characterized by: Ft-IR, U. v- Visible, electrical conductivity, magnetic susceptibilities at 25 Co, atomic absorption and molar ratio. Spectroscopic evidence showed that the binding of metal ions were through azide and carbonyl moieties resulting in a six- coordinating metal ions in [Cr (III), Mn (II), Co (II) and Ni (II)]. The Vo (II), Cu (II), Zn (II), Cd (II) and Hg (II) were coordinated through azide group only forming square pyramidal
... Show Moreالمستودع الرقمي العراقي. مركز المعلومات الرقمية التابع لمكتبة العتبة العباسية المقدسة
In this article four samples of HgBa2Ca2Cu2.4Ag0.6O8+δ were prepared and irradiated with different doses of gamma radiation 6, 8 and 10 Mrad. The effects of gamma irradiation on structure of HgBa2Ca2Cu2.4Ag0.6O8+δ samples were characterized using X-ray diffraction. It was concluded that there effect on structure by gamma irradiation. Scherrer, crystallization, and Williamson equations were applied based on the X-ray diffraction diagram and for all gamma doses, to calculate crystal size, strain, and degree of crystallinity. I
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