A new, simple, accurate, fast and sensitive spectrophotometric method has been
developed for the analysis of Pyrocatechol, Resorcinol, and pyrogallolin pure
commercial samples by continuous flow injection analysis. The method was based on
the oxidation of the organic compounds with Ce(IV)sulfate in acidic medium to
formed a brown colored species which determined using homemade Ayah 3SBGR x3-
3D solar cell flow injection microphotometer. Optimum conditions were obtained
using a high intensity green light emitted diode as an irradiation source
forPyrocatechol, Resorcinol, whileblue light emitted diode as an irradiation source for
pyrogallol. The linear dynamic range for the instrument response versus Pyrocatechol,
Resorcinol, and pyrogallol concentrationswere5-40mmol.L-1 while the L.O.D was of
36.63, 17.17, and 41.61ng / sample respectively. The correlation coefficient (r) was
0.9952, 0.9970, and 0.9960 while percentage linearity (r2%) was 99.05%, 99.41% and
99.22%forPyrocatechol, Resorcinol, and pyrogallol respectively. RSD% for the
repeatability (n=8,7, and 8) was 1.4%, 0.63%, 1.78% for the determination of
Pyrocatechol, Resorcinol,andpyrogallol, respectively at concentration of 30 mmol.L-1.
The method was applied successfully for the determination of three organic
compounds in purecommercial samples. A comparison was made between the newly
developed method and the classical method (UV-Vis spectrophotometry) at wave
length 492, 481, and 438 nm forPyrocatechol, Resorcinol and pyrogallolrespectively
of analysis using the standard additions method via the use of paired t-test. It was
noticed that there is no significant difference between two different methods for
analysis three different organic compounds; in addition to no significant difference in
the contribution of the Pyrocatechol, Resorcinol and pyrogallol to the oxidant reaction
path, at 95% confidence level.
In this work, thin films of undoped and Al-doped CdO with (0.5, 1 and 2) wt.% were prepared by using thermal vacuum evaporation on glass substrate at room temperature. The optical absorption coefficient (α) of the films was determined from transmittance spectra in the range of wavelength (400-1100) nm. The spectral transmission and the optical energy band gap decrease from 75% and 2.24 eV to 20% and 2.1 eV respectively depending upon the Al content in the films, also our studies include the calculation of the optical constants (refractive index, extinction coefficient, real and imaginary part of dielectric constant) as a function of photon energy. It is evaluated that the optical band gap of
... Show MoreThis study deals with seismic structural and stratigraphic interpretation that applied on the East Razzaza (central of Iraq) area, by using 2D seismic data from Oil Exploration Company. Three main seismic reflectors are picked. These reflectors are Zubair, Yamama and Gotnia Formations, which were defined by using petrophysical well logs and synthetic traces that calculated from sonic- logs of the wells East Baghdad-1(Eb-1) and West kifl-1(Wk-1) using Geoframe program, to suggest a stratigraphic model for them. Structural maps of formations are prepared to obtain the location and direction of the sedimentary basin and shoreline. Seismic interpretation of the area approves the presence of some stratigraphic features in the studied formatio
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The reasons for the totality are varied and multiple, some of which are attributed to the methods of the Arabic language as the participant
Verbal and omnipotent differences in the oud of conscience, which are comprehensive reasons for language in all
And some of these reasons are due to the sciences of the Qur'an, such as cessation and initiation
The explanation of the explanation for the multiplicity of words and differences in them, which necessarily led to a dispute jurisprudence
Linked to the origin of disagreement in the interpretation of the totality and its orientation and understanding and to summarize this subject and diverge
Parts and vocabulary did not receive the necessary care and did not absorb the lesson an
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The extraction of Eucalyptus oil from Iraqi Eucalyptus Camadulensis leaves was studded using water distillation methods. The amount of Eucalyptus oil has been determined in a variety of extraction temperature and agitation speed. The effect of water to Eucalyptus leaves (solvent to solid) ratio and particle size of Eucalyptus leaves has been studied in order to evaluate the amount of Eucalyptus oil. The optimum experimental condition for the Eucalyptus oil extraction was established as follows: 100˚C extraction temperature, 200 rpm agitation speed; 0.5 cm leave particle size and 6:1 ml: g amount of water to eucalyptus leaves Ratio.
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Field trial was conducted during the growing season of 2011-2012 at the Research
Field, Department of Biology, College of Science, Baghdad University to test the
performance of wheat cv Rabyaa, Latifiya, Al-Iraq, Tummose 2, Abu-Graib 3, IPA
99 and Sham 6 grown under different soil water deficit stresses. Several agronomic
and physiological traits and yield and yield components of the test cultivars were
determined. The experiment was conducted in split plot design with five replications
for each treatment. The cultivars were kept in the sub plot while water stress
treatment was assigned as main plot. Water stress was applied by irrigated the plots
to the soil field capacity (FC) then withheld next irrigation until
In this research an improvement of the efficiency of vacuum microwave tube type Gl-19B had been done by activation of internal surfaces using two specific procedures which can qualify the tubes to be reused again.
The first method was the reevacuuated and heating treatment.
The second method wa:s the glow discharge method which used ro
clean the electrodes and improve the vacuum to about!o·8 mbar.
In order to study the using of both processes together, Copper
samples heate
... Show MoreIn this study, the potential of adsorption of amoxicillin antibiotic (AMOX) from aqueous solutions using prepared activated carbon (AC) was studied. The used AC was prepared from an inexpensive and available precursor (sunflower seed hulls (SSH)) and activated by potassium hydroxide (KOH). The prepared AC was examined for its ability to remove AMOX from aqueous contaminated solutions and characterized with the aid of N2 -adsorption/desorption isotherm Brunauer–Emmett– Teller, scanning electron microscopy, energy-dispersive X-ray spectroscopy and Fourier-transform infrared. Zeta potential of the prepared activated carbon from sunflower seed hulls (SSHAC) were studied in relation to AMOX adsorption. The physical and chemical propert
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