Copper electrodeposition by electrorefining process in acidic sulfate media contains 40 g/l of cupric ions and 160 g/l of sulfuric acid was achieved to study the influence of the operating parameters on cathode purity, surface morphology, deposition rate, current efficiency and power consumption. These operating parameters and there ranges are: current density 200, 300 and 400 A/m2, electrolyte temperature 35, 50 and 65 oC, electrodes spacing 15, 30 and 45 mm and electrolyte residence time 6, 4 and 2 h were utilized. XRF, SEM and EDX analyses were attained to clarify the properties of the produced cathode.
Abstract
The research aims to diagnose the reality of applying the eighth requirement (operation) of the business continuity management system according to the international standard (ISO 22301: 2019), in the General Tax Authority, which is related to planning, implementing and controlling specific processes and procedures to address risks and opportunities, and the research adopted the checklist of the standard ( ISO 22301: 2019), in obtaining information, to measure the extent of application and documentation, the percentages and the weighted arithmetic mean were relied upon, and the research reached a set of result
... Show MoreThis paper reports test results and describes a numerical investigation of the effectiveness of using carbon fibre reinforced polymer (CFRP) fabrics for strengthening concrete cylinders that have been undamaged and damaged due to heating under preload. The purpose of this research was to investigate whether there is any difference in the performance of CFRP-wrapped cylinders if the wrapping is done under preload, and those for which neither heating, cooling nor wrapping was done under preload. The cylinders were exposed to 30% of maximum load at ambient temperature during heating and cooling before being wrapped under preload. Of 18 Ø 100 × 200 mm identical cylinders, 6 were left as control samples without heating, 12 were exposed t
... Show MoreIn addition to the primary treatment, biological treatment is used to reduce inorganic and organic components in the wastewater. The separation of biomass from treated wastewater is usually important to meet the effluent disposal requirements, so the MBBR system has been one of the most important modern technologies that use plastic tankers to transport biomass with wastewater, which works in pure biofilm, at low concentrations of suspended solids. However, biological treatment has been developed using the active sludge mixing process with MBBR. Turbo4bio was established as a sustainable and cost-effective solution for wastewater treatment plants in the early 1990s and ran on minimal sludge, and is easy to maintain. This
... Show MoreIn this paper, suggested formula as well a conventional method for estimating the twoparameters (shape and scale) of the Generalized Rayleigh Distribution was proposed. For different sample sizes (small, medium, and large) and assumed several contrasts for the two parameters a percentile estimator was been used. Mean Square Error was implemented as an indicator of performance and comparisons of the performance have been carried out through data analysis and computer simulation between the suggested formulas versus the studied formula according to the applied indicator. It was observed from the results that the suggested method which was performed for the first time (as far as we know), had highly advantage than t
... Show MoreDens itiad ns vcovadoay fnre Dec2isco0D,ia asrn2trcds4 fenve ns 6ocfo ts ida%n2notd, rasr sedno6t(a asrn2trcd fnre sc2a 2cynwnvtrnco co nrs wcd2 /nt sedno6t(a fan(er wtvrcd ﯿ)ﺔ mh Dens r,ia cw asrn2trcds et/a laao vcosnyaday wcd asrn2trno( rea itdt2arads ﻘ cw sn2i%a %noatd da(dassnco 2cya%4 feao t idncd asrn2tra cw rea itdt2arad /t%ua )ﻘm ns t/tn%tl%a4 st, ﻘxh Dens ﻘx ets laao dawadday no srtrnsrnvt% %nradtrudas ts (uass icnor tlcur rea itdt2arad ﻘh Dea aMidassncos wcd Snts4 Oato -9utday 8ddcd )O-8m toy .a%trn/a 8wwnvnaov, cw rea idcicsay asrn2trcds tda clrtnoayh 1u2adnvt% dasu%rs tda idc/nyay feao rea
... Show MoreAn experimental investigation has been carried out for zinc-nickel (Zn-Ni) electro-deposition using the constant applied current technique. Weight difference approach method was used to determine the cathode current efficiency and deposit thickness. Also, the influence effect of current density on the deposition process, solderability, and porosity of the plating layer in microelectronic applications were examined. The bath temperature effect on nickel composition and the form of the contract was studied using Scanning Electron Microscope (SEM). Moreover, elemental nature of the deposition was analyzed by Energy Dispersive X-Ray (EDX).
It has been found that the best bath temperature
... Show MoreA novel azo dye ligand namely (2-(pyridin-3-yldiazenyl)naphthalen-1-ol (HPYNA), was synthesized by the coupling reaction of diazonium salt of 3-aminopyridine with naphthol. The palladium(II) complex for HPYNA ligand was prepared by reacting palladium(II) ions with the HPYNA ligand. These synthesized compounds were characterized using different techniques, including mass, 1H-NMR, infrared, and UV-Vis spectroscopy. The infrared results show that the azo ligand reacts as a bidentate via the oxygen atom of phenol and nitrogen atom of the azo group. The palladium(II) complex is square-planer with diamagnetic properties depending on the results of electronic transitions and magnetic sensitivity. The HPYNA ligand and palladium complex show
... Show More