Synthesis, characterization and bioactivity Study from azo – ligand derived frommethyl-2-amino benzoatewith some metal ions

Israa H. Ibraheem; Noora Saad Mubder; Mays Mohammed Abdullah; Haider Al-Neshmi

doi:10.21123/bsj.2022.6584

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Publication Date

Wed Feb 01 2023

Journal Name

Baghdad Science Journal

Volume

20

Issue Number

1

DOI

10.21123/bsj.2022.6584

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Synthesis, characterization and bioactivity Study from azo – ligand derived frommethyl-2-amino benzoatewith some metal ions

Bioactivity

complexes

ethanol

Molar conductivity

Transition Metals

Israa H. Ibraheem

Noora Saad Mubder

Mays Mohammed Abdullah

Haider Al-Neshmi

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A Ligand (ECA) methyl 2-((1-cyano-2-ethoxy-2-oxoethyl)diazenyl)benzoate with metals of (Co²⁺, Ni²⁺, Cu²⁺) were prepared and characterization using H-NMR, atomic absorption spectroscopy, ultra violet (UV) visible, magnetic moments measurements, bioactivity, and Molar conductivity measurements in soluble ethanol. Complexes have been prepared using a general formula which was suggested as [M (ECA)₂] Cl₂, where M = (Cobalt(II), Nickel(II) and Copper(II), the geometry shape of the complexes is octahedral.

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Publication Date

Sun Mar 07 2010

Journal Name

Baghdad Science Journal

Safety method, Spectrophotometric Determination of Sulfamethaxazole drug in bulk and Pharmaceutical Preparations

"Spectrophotometric

Sulfamethaxazole

pharmaceutical formulations"

Saadiyah A.

Amira .H.

Maha K.

Rafah K

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A simple, cheap, fast, accurate, Safety and sensitive spectrophotometric method for the determination of sulfamethaxazole (SFMx), in pure form and pharmaceutical dosage forms. has been described The Method is based on the diazotization of the drug by sodium nitrite in acidic medium at 5Cº followed by coupling with salbutamol sulphate (SBS) drug to form orange color the product was stabilized and measured at 452 nm Beer’s law is obeyed in the concentration range of 2.5-87.5 ?g ml-1 with molar absorptivity of 2.5x104 L mole-1 cm-1. All variables including the reagent concentration, reaction time, color stability period, and sulfamethaxazole /salbutamol ratio were studied in order to optimize the reaction conditions. No interferences were

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Publication Date

Fri Feb 01 2019

Journal Name

Journal Of Physics: Conference Series

Spectroscopic and structural properties of Zinc-Phthalocyanine prepared by pulsed laser deposition

Mohammed T.

Mohammed Jawad H.

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Fri Oct 01 2010

Journal Name

Saudi Pharmaceutical Journal

Comparative clinical evaluation of ketotifen and montelukast sodium in asthmatic Iraqi patients

Fadyia Y.

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Publication Date

Wed Feb 03 2016

Journal Name

Nanoscience And Nanotechnology

Fabrication of Functionalize Reduce Graphene Oxide and Its Application in Ampicillin Detection

Sundus

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Graphene oxide (GO) was prepared from graphite (GT) with Hammer method, the GO was reduced with hydrazine hydrate to produce a reduced graphene oxide (RGO). The RGO was reacted with thiocarbohydrazide (TCH) to functionalize the RGO with 4-amino-3-symbol-1h-1, 2, 4-triazol-5 (4H) –thion group and to obtain (RGOT). All the prepared nanomaterial and the product of the functionalization RGOT were characterized with Fourier transformer infrared (FT-IR) spectroscopy, X-ray diffraction (XRD) analysis. RGOT mixed with ultrasonic device at different pH values of phosphate buffer solution (PBS), the mixture used to modifying a screen printed carbon electrodes SPCE and with cyclic voltammetry the sensitivity of selectivity of the new modifying elect

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Publication Date

Sat Dec 01 2018

Journal Name

Journal Of South Asian Federation Of Obstetrics And Gynaecology

Effect of Leptin Level in Pregnancy Complicated by Preeclampsia and Pregnancy Outcome

Bushra

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Publication Date

Mon May 04 2020

Journal Name

Offshore Technology Conference

Hydrate Equilibrium Model for Gas Mixtures Containing Methane, Nitrogen and Carbon Dioxide

gas hydrate

cavity

equilibrium condition

flow assurance

modeling & simulation

hydrate equilibrium condition

upstream oil & gas

cage occupancy

hydrate

gas mixture

Dhifaf Jaafar

Omar

Stefan

Maxim

Callum

Ahmed

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Abstract<p>Gas hydrate formation is considered one of the major problems facing the oil and gas industry as it poses a significant threat to the production, transportation and processing of natural gas. These solid structures can nucleate and agglomerate gradually so that a large cluster of hydrate is formed, which can clog flow lines, chokes, valves, and other production facilities. Thus, an accurate predictive model is necessary for designing natural gas production systems at safe operating conditions and mitigating the issues induced by the formation of hydrates. In this context, a thermodynamic model for gas hydrate equilibrium conditions and cage occupancies of N2 + CH4 and N2 + CO4 gas mix</p> ... Show More

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Publication Date

Fri Mar 14 2014

Journal Name

Arabian Journal Of Geosciences

Wetting and drying collapse behaviour of collapsible gypseous soils treated by grouting

Mohammad Y.

Mahmoud T.A.

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Sat May 01 2021

Journal Name

Iop Conference Series: Earth And Environmental Science

Evaluation Yield of Okra with Associated Traits Using Analysis Correlation and Path

Ayad Waleed Abdulla

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Abstract<p>The study was conducted at the fields of the Department of Horticulture and Landscape Gardening, College of Agriculture Engineering Sciences, University of Baghdad. During the spring 2017. All the recommended practices were followed during experimentation. The experimental material consisted four Genotype it is Batraa, Btera, Mosulle, and local selection. The experiment was applied in Randomized Complete Block Design (RCBD). The objectives of Study were to estimate the some genetic parameters and path coefficient for some traits Okra, The results of statistical analysis for these genotypes were highly significant differences for all traits except the traits number of leaves, the numbe</p> ... Show More

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(3)

Publication Date

Sat Jan 13 2018

Journal Name

Journal Of Engineering

Statistical Analysis of Mortality and Morbidity Due to Traffic Accidents in Iraq

Roaa

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Undoubtedly, Road Traffic Accidents (RTAs) are a major dilemma in term of mortality and morbidity facing the road users as well as the traffic and road authorities. Since 2002, the population in Iraq has increased by 49 percent and the number of vehicles by three folds. Consequently, these increases were unfortunately combined with rising the RTAs number, mortality and morbidity. Alongside the humanitarian tragedies, every year, there are considerable economic losses in Iraq lost due to the epidemic of RTAs. Given the necessity of understanding the contributory factors related to RTAs for the implementation by traffic and road authorities to improve the road safety, the necessity have been a rise for this research which focuses into

Publication Date

Sun Dec 15 2019

Journal Name

Journal Of Baghdad College Of Dentistry

The priorities and emergency treatments of multisystem injuries associated with maxillofacial traumas

Ahmed O.

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Background: The purpose of this study is to evaluate the care of multiple trauma victims with maxillofacial injuries in terms of epidemiological distributions, types of injuries, the related different modalities of surgical treatments delivered, and their complications. Materials and Methods: This prospective study was performed on 50 patients with multiple traumas including maxillofacial injuries, caused by different etiological factors, who were brought first to the surgical emergencies department of the Medical City then referred to the Maxillofacial unit in the Specialized Surgeries Hospital, Baghdad, Iraq, during the period from April 2007 to April 2008. Information was documented prospectively from the time of the emergency call to

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