Cr2O3:TiO2 Nanostructure Thin Film Prepared by Pulsed Laser Deposition Technique as NO2 Gas Sensor

Saadoon M. Kareem et al.

doi:10.21123/bsj.2020.17.1(Suppl.).0329

Details

Publication Date

Wed Mar 18 2020

Journal Name

Baghdad Science Journal

Volume

17

Issue Number

1(Suppl.)

DOI

10.21123/bsj.2020.17.1(Suppl.).0329

Choose Citation Style

Statistics

View publication

4

View pdf

1

Abstract Views

279

Galley Views

188

Statistics

(5)

(7)

Cr2O3:TiO2 Nanostructure Thin Film Prepared by Pulsed Laser Deposition Technique as NO2 Gas Sensor

Cr2O3:TiO2 Nanostructure

Optical properties

PLD technique

Structural properties

Sensitivity

Saadoon M. Kareem et al.

...Show More Authors

Pulsed laser deposition (PLD) technique was applied to prepared Chromium oxide (Cr₂O₃) nanostructure doped with Titanium oxide (TiO₂) thin films at different concentration ratios 3,5,7 and 9 wt % of TiO₂. The effect of TiO₂ dopant on the average size of crystallite of the synthesized nanostructures was examined by X-ray diffraction. The morphological properties were discussed using atomic force microscopy(AFM). Observed optical band gap value ranged from 2.68 eV to 2.55 eV by ultraviolet visible(UV-Vis.) absorption spectroscopy with longer wave length shifted in comparison with that of the bulk Cr₂O₃ ~3eV. This indicated that the synthesized samples are attributed to the enhancement of the quantum conﬁnement effect. Gas response sensitivity, and recovery times of the sensor in the presence of NO₂ gas were studied and discussed. In this work it is found that, the sensitivity increases when doping ratio increases from 3wt% to 5wt% of TiO₂and return to decrease over that. The optimum concentrations ratio for NO₂ gas sensitivity is 5wt% of TiO₂ and sensitivity is 168.75% at 200^oC.

View Publication Preview PDF

Quick Preview PDF

Publication Date

Sun Dec 07 2014

Journal Name

Baghdad Science Journal

Synthesis, Characterization and Stability Study of V(IV), Zr(IV), Rh(III), Pd(II), Cd(II) and Hg(II) Complexes with Pyrazol Derivative

In this work lactone (1) was prepared from the reaction of p-nitro phenyl hydrazine with ethylacetoacetate

which upon treatment with benzoyl chloride afforded the lactame (2). The reaction of (2) with 2-amino phenol produced a new Schiff base (L) in good yield. Complexes of V(IV)

Zr(IV)

Rh(III)

Pd(II)

Cd(II) and Hg(II) with the new Schiff base (L) have been prepared. The compounds (1

2) were characterized by FT-IR and UV spectroscopy

as well as characterizing ligand (L) by the same techniques with elemental analysis (C.H.N) and (1H-NMR). The prepared complexes were identified and their structural geometries were suggested by using elemental analysis (C.H.N)

flame atomic absorption technique

FT-IR and UV-Vis spectroscopy

in addition to magnetic susceptibility and conductivity measurements. Metal to ligand [M:L] ratio was obtained for all complexes in ethanol using molar ratio method

which gave comparable results with those obtained for the solid complexes. As well as the appa

Sinan M.

Enaam M.

Maysoon A

Sarab M

...Show More Authors

In this work lactone (1) was prepared from the reaction of p-nitro phenyl hydrazine with ethylacetoacetate, which upon treatment with benzoyl chloride afforded the lactame (2). The reaction of (2) with 2-amino phenol produced a new Schiff base (L) in good yield. Complexes of V(IV), Zr(IV), Rh(III), Pd(II), Cd(II) and Hg(II) with the new Schiff base (L) have been prepared. The compounds (1, 2) were characterized by FT-IR and UV spectroscopy, as well as characterizing ligand (L) by the same techniques with elemental analysis (C.H.N) and (1H-NMR). The prepared complexes were identified and their structural geometries were suggested by using elemental analysis (C.H.N), flame atomic absorption technique, FT-IR and UV-Vis spectroscopy, in additio

View Publication Preview PDF

Publication Date

Wed Jan 01 2020

Journal Name

Technologies And Materials For Renewable Energy, Environment And Sustainability: Tmrees20

Change detection of the land cover for three decades using remote sensing data and geographic information system

The changes in the land cover using geographical information systems and remote sensing techniques for the period (1990 - 2019) for part of the Baghdad governorate in central Iraq are detected and monitored. In this research

four satellite scenes with different sensors were used the TM

ETM+

and OLI

which were obtained by Landsat-5

Landsat-7 and Landsat-8 satellites

respectively. Maximum likelihood method supervised classification is adopted as the main classifier to distinguish different land cover types in the study region. The results showed that there are ten different classes in the values of their reflectance. This study proved that any landcover of the earth’s surface can be studied and determined by its spectral characteristics. The change for each class of the land cover for the study area was determined within the study period. The results of the study confirmed the possibility of identifying the types of land cover and finding the percentage of changes that occur in it and detecting it with high efficiency using the remote sensing technique.

Muna Aref

Amal Jabbar

...Show More Authors

View Publication

(3)

Publication Date

Tue Mar 01 2022

Journal Name

Iraqi Journal Of Agricultural Sciences

CORRELATION OF TMPRSS2-ERG GENE FUSION STATUS WITH CLINICOPATHOLOGICAL CHARACTERISTICS IN PROSTATE CANCER OF IRAQI PATIENTS

The aim of this study was to establish the existence and interaction of TMPRSS2 – ERG gene fusion status with clinicopathological features of prostate cancer patients. This research consisted of 123 embedded formalin-fixed tissues obtained from the prostate tumor patients. The above gene fusion is detected through the technique of fluorescent in situ hybridization (FISH) by means of a triple color probe. Seven samples have not been scored due to technical difficulties and 46 patients have fusion (39.6%)

while the remaining (70) have not been seen with fusion. Of the 46 fusion-positive

17 (36%) were caused by ERG-translocation

of the other 29 (63%) were caused by the interstitial segment deletion between the two genes due to their sequential position. In order to find a substantial correlation between 116 patients (fusion took place in 46 and non-fusion in 70) with clinicopathological features

the following findings were calculated: Our findings recorded non-significant correlation at age

BMI and tumor size at which (P-value >0.05).While results showed significant association with: pathological T stage (P value = 0.011)

Gleason score (P value = 0.002)

perineural invasion (P value = 0.047) and PSA (P value = 0.033). The clinicopathological features which had a considerable correlation with fusion status are very important as they aid the doctors in prognosis and treatment of such tumor.

Ammar

Maha

...Show More Authors

1 2 3 4 ... 558 559 560 561