Some Metal Ions Complexes Derived From Schiff Base Ligand with Anthranillic Acid: Preparation, Spectroscopic and Biological Studies: organic chemistry

lekaa khalid karem

doi:10.21123/bsj.2020.17.1.0099

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Publication Date

Mon Mar 23 2020

Journal Name

Baghdad Science Journal

Volume

17

Issue Number

1

DOI

10.21123/bsj.2020.17.1.0099

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Some Metal Ions Complexes Derived From Schiff Base Ligand with Anthranillic Acid: Preparation, Spectroscopic and Biological Studies: organic chemistry

Anthranillic Acid

Geometrical

Mixed Ligands

Spectroscopy.

lekaa khalid karem

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This search includes the preparation of Schiff base ligand (SB) from condensation primary amine with vanillin. The new ligand was diagnosed by spectroscopic methods as Mass, NMR, CHN and FTIR. Ligand complexes were mixed from new (SB) and Anthranillic acid (A) with five metal (II) chlorides. The preparation and diagnosis were conducted by FTIR, CHN, UV-visible, molar conductivity, atomic absorption and magnetic moment. The octahedral geometrical shape of the complexes was proposed. The ligands and their new complexes were screened with two different types of bacteria.

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Publication Date

Wed Mar 10 2021

Journal Name

Baghdad Science Journal

Synthesis & Characterization of Oxazinan and 5-oxa-7-aza-spiro[2,5] octane from reaction of Dibenzylidene with malonic anhydride and 5-oxa-spiro[2,3] hexane-4,6-dione.

Waleed, F.

Obaid H.

Mohammed A

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Di Benzylidenes were prepared by condensation of 1,2-diamino benzene with o- hydroxy benzaldehyde. These dibenzylidenes when treated with one equivalent of malonic anhydride or 5-oxo-spiro[2,3]hexane-4,6-dione in dry benzene give 6-membered heterocyclic ring system of 3-{2-[(2-Hydroxy-benzylidene)-amino]-phenyl}-2-(2-hydroxy –phenyl)-[1,3]oxazinane-4,6-diones ( 1-3) or 7-{2-[(2-hydroxy-benzylidene)-amino]-phenyl}-6-(2-hydroxy-phenyl)-5-oxa-7-aza-spiro[2.5]octane-4,8-diones ( 7- 9 ) But when two equivalents of malonic anhydride or 5-oxo-spiro[2,3]hexane-4,6-dione were used and under sam conditions compounds (4-6 , 10-12 ) were obtained .

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Publication Date

Tue Sep 01 2015

Journal Name

Nano Science And Nano Technology

Preparation CuInSe2 (CIS) by arrested precipitation method as alight absorption layer of photovoltaic solar-cells

CuInSe2

Nanoink

Arrested precipitation

Selenization

Ar- Atmosphere

Wasan

Omar

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The CuInSe2 (CIS) nanocrystals are synthesized by arrested precipitation from molecular precursors are added to a hot solvent with organic cap- ping ligands to control nanocrystal formation and growth. CIS thin films deposited onto glass substrate by spray - coating, then selenized in Ar- atmosphere to form CIS thin films. PVs were made with power conversion efficiencies of 0.631% as -deposited and 0.846% after selenization, for Mo coated, under AM 1.5 illumination. X-ray diffraction (XRD) and energy dispersive spectroscopy (EDS) analysis it is evident that CIS have the chalcopyrite structure as the major phase with a preferred orientation along (112) direction and the atomic ratio of Cu : In : Se in the nanocrystals is nearly 1 : 1 : 2

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Publication Date

Sun Jan 01 2023

Journal Name

Materials Science In Semiconductor Processing

A dual S-scheme g-C3N4/Fe3O4/Bi2WO6/Bi2S3 heterojunction for improved photocatalytic decomposition of methylene blue: Proposed mechanism, and stability studies

Aya A

Abeer I.

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Publication Date

Tue Aug 01 2023

Journal Name

Baghdad Science Journal

A New Model Design for Combating COVID -19 Pandemic Based on SVM and CNN Approaches

CNN

COVID-19

Machine Learning

Medical Imaging

RNN

SVM

Sura Monther

Hadeel K.

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In the current worldwide health crisis produced by coronavirus disease (COVID-19), researchers and medical specialists began looking for new ways to tackle the epidemic. According to recent studies, Machine Learning (ML) has been effectively deployed in the health sector. Medical imaging sources (radiography and computed tomography) have aided in the development of artificial intelligence(AI) strategies to tackle the coronavirus outbreak. As a result, a classical machine learning approach for coronavirus detection from Computerized Tomography (CT) images was developed. In this study, the convolutional neural network (CNN) model for feature extraction and support vector machine (SVM) for the classification of axial

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Publication Date

Thu Mar 01 2012

Journal Name

Journal Of Economics And Administrative Sciences

Notes on estimation of ARMA model (1.1) And ARMA (0,1)

طريقة العزوم للانموذج ARMA(1

1) و ARMA(0

1)

: ARMA Modeling Method (1.1) And ARMA (0

1)

لميعه باقر

لمياء محمد

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By driven the moment estimator of ARMA (1, 1) and by using the simulation some important notice are founded, From the more notice conclusions that the relation between the sign and moment estimator for ARMA (1, 1) model that is: when the sign is positive means the root gives invertible model and when the sign is negative means the root gives invertible model. An alternative method has been suggested for ARMA (0, 1) model can be suitable when

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Publication Date

Sat Feb 01 2020

Journal Name

Journal Of Economics And Administrative Sciences

Applying some hybrid models for modeling bivariate time series assuming different distributions for random error with a practical application

أنمُوذج

التوزيع الطبيعي القياسي

توزيع

توزع الخطأ العام

سعر الصرف

معدل البطالـة.

: Bivariate time series ARMAX-GARCH

ARMAX-GARCHX

Normal distribution

Student-t distribution

General Error distribution (GED)

Unemployment rate

Exchange rate.

فراس احمد

مؤمن عباس

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Abstract

Bivariate time series modeling and forecasting have become a promising field of applied studies in recent times. For this purpose, the Linear Autoregressive Moving Average with exogenous variable ARMAX model is the most widely used technique over the past few years in modeling and forecasting this type of data. The most important assumptions of this model are linearity and homogenous for random error variance of the appropriate model. In practice, these two assumptions are often violated, so the Generalized Autoregressive Conditional Heteroscedasticity (ARCH) and (GARCH) with exogenous varia

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Publication Date

Tue Jan 01 2019

Journal Name

Plant Archives

Evaluation of water stress effect on some chemical properties of several sunflower varieties callus treated with colocynth fruit extract

Y.I.H.

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The study was carried out in plant tissue culture laboratory, University of Baghdad during the period 2017-2019, as factorial experiment in complete randomized design, to study the effect of PEG at (0, 2, 4, 6 and 8%) on physiological and chemical changes in callus of three sunflower (Ishaqi 1, Aqmar and Al-haga) induced by the cultivation of the young stem in vitro under water stress. The content of callus cells of SOD, POD, CAT and APX enzymes as well as total dissolved carbohydrate were determined as indicators to determine the effect of PEG in callus tissue cells cultivated on medium equipped with the PEG concentrations. The results showed that cultivars were differs significantly, and A-haja variety was superior in increasing SOD to 12

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Publication Date

Tue Mar 31 2015

Journal Name

Al-khwarizmi Engineering Journal

Influence of Coating with Some Natural Based Materials on the Erosion Wear Behavior of Glass Fiber Reinforced Epoxy Resin

Keywords: Composites

Preparation of natural materials

Erosion wear

glass fiber

Coating.

Aseel Basim

Emad Saadi

Reem Alaa

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Abstract

In the present study, composites were prepared by Hand lay-up molding. The composites constituents were epoxy resin as a matrix, 6% volume fractions of glass fibers (G.F) as reinforcement and 3%, 6% volume fractions of preparation natural material (Rice Husk Ash, Carrot Powder, and Sawdust) as filler. Studied the erosion wear behavior and coating by natural wastes (Rice Husk Ash) with epoxy resin after erosion. The results showed the non – reinforced epoxy have lower resistance erosion than natural based material composites and the specimen (Epoxy+6%glass fiber+6%RHA) has higher resistance erosion than composites reinforced with carrot powder and sawdust at 30cm , angle 60

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Publication Date

Sat Nov 22 2025

Journal Name

Journal Of Studies And Researches Of Sport Education

The effect of using the educational bag on the level of learning some offensive skills with the epee weapon

The effect of using the educational bag on the level of learning some offensive skills with the epee weaponDr. Lamia Hassan Al-Diwan

D. Fatima Abdel-Maliki

Dr. Kholoud Laith Abdel Karim2005 Technical and technological development has been increasing day after day and has included all areas of life

including the educational process

which has benefited from technologies such as (computer

video

and pictorial models) in introducing them as tools to aid the learning process. Educational packages have proven their effectiveness in education as they prepare learners with different areas of experience. Sensory audio-visual

through which the learner acquires different educational experiences through interaction

practice

participation

and communication with the data of the surrounding environment through the diversity of knowledge sources that suit his inclinations and needs. The research aimed to prepare an educational bag to teach some offensive skills in the epee weapon. And to find out the effect of using the proposed educational bag on the level of learning some offensive skills in the epee weapon. We hypothesized that the proposed educational package has a positive impact on the level of learning some offensive skills with the epee weapon. There were statistically significant differences in testing the level of learning some offensive skills with the epee weapon between the post-tests of the experimental and control groups

and in favor of the experimental group. The researchers used the experimental method to suit the nature of solving the research problem

and the research sample was chosen intentionally from the girls’ fencing club players (beginners) in the governorate. Basra for the year 2005. The number of players was (16)

which represented the entire study population. The experiment was conducted in the sports hall of the South Oil Sports Club in Basra. We concluded that the educational package has a positive impact on the level of learning some offensive skills in the epee weapon. There were statistically significant differences in the learning level test for some offensive skills in the epee weapon between the experimental group and the control group in the post-tests and in favor of the experimental group. We recommended the necessity of using the proposed educational curriculum to learn some offensive skills in the epee weapon in fencing lessons or in sports clubs. Adopting modern techniques in training

teaching or teaching fencing skills and searching for new methods. Conducting similar studies on other skills or different samples.Keywords: educational bag

offensive skills with an epee weapon

fencing game. Teaching methods. Basra Girl Sports ClubLamya Hassan Aldewan [email protected] of Basra - College of Education and Sports Scienceshttps://orcid.org/0000-0003-0377-6915 Keywords educational bag

offensive skills with an epee weapon

fencing game. Teaching methods. Basra Girl Sports Club

‏Lamyaa

Fatima

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Publication Date

Wed Jan 01 2020

Journal Name

Plant Archives

The effect of adding some essential oils to the physicochemical properties of frozen beef sausage with different storage periods

Al-Zaidi R.M.K.

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