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Publication Date
Sun Dec 04 2016
Journal Name
Baghdad Science Journal
Volume
13
Issue Number
4
DOI
10.21123/bsj.2016.13.4.0762
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12
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Articles
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bsj-2318
Synthesis and Characterization of some New 1,3,4-Oxadiazole derivatives based on 4-amino benzoic acid
"Oxadiazole
Schiff base
?- Lactam"
Shatha F. Al-Zobaydi
Bushra K. Hamed
Ban D. Ismael
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Various of 2,5- disubstituted 1,3,4-oxadiazole (Schiff base, ?- lactam and azo) were synthesized from 2,5-di (4,4?-amino-1,3,4-oxadiazole which usequently synth-esized from mixture of 4- amino benzoic acid and hydrazine arch of polyphosphorus acid. The synthesized compounds were cherecterized by using some spectral data (UV, FT-IR , and 1H-NMR)

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A series of new coumarin and N-amino-2-quinolone derivatives have been synthesized. The reaction of coumarin (1) with excess of  Hydrazine hydrate 98% yielded 1-amino-2-quinolone (2), Compound (2) was reacted with different Sulfonyl chloride to yield Sulfonamides [ N-(2-oxoquinolin-1(2H)-yl) methane sulfonamide (3), N-(2-oxoquinolin-1(2H)-yl) Benzene sulfonamide (4) and 4-methyl-N-(2-oxoquinolin-1(2H)-yl) benzene sulfonamide (5) ], while  reaction of  2-(4-methyl-2-oxo-2H-chromen-7-yloxy) acetic acid (8) with different amines yielded compounds [  2-(4-methyl-2-oxo-2H-chromen-7-yloxy)-N-(2-oxoquinolin-1(2H)-yl) acetamide (9) and N-(5-methyl-1,3,4-thiadiazol-2-yl)-2-(4-methyl-2-oxo-2H-chromen-7-yloxy)acetamide (10) ] th

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                          In this research work, synthesis, antimicrobial and antioxidant bioactivity of a chain of compounds having unsaturated ketones bond and isoxazoline moiety have been described. New chalcone derivatives containing isoxazoline moiety have been synthesized. Generally, Chalcones are unsaturated ketones bearing (-CO-CH=CH-) as reactive ketoethylenic group that give the bright yellow colored compounds due to this chromophore group.  Firstly, chalcones (IIa-d) have been prepared by cyclocondensation (Claisen-Schmidt condensation) of triphenyl aminobenzaldehyde with different substituted acetophenone in ethyl alcohol to produce a series of chalcones compounds with bright yellow colored as a

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Preparation and Identification of some new Pyrazolopyrin derivatives and their Polymerizations study
Synthesis
Fused Pyrazoles
1-(3
6-dimethyl-4-oxo-1
4-dihydro-5H-pyrazolo [4
3-C] pyridin-5-yl)-1H-pyrrole-2
5-Dione S1
1-[2-(3
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4-dihydro-5H-pyrazolo[4
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5-DioneS2 and 1-(3
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4-dihydro-5H-pyrazolo[4
3-C]pyridin-5-yl)-1H-pyrrole-2
5-Dione S3
reactivity ratios
copolymer composition
Mean Sequence lengths.
Redha I. H.
Mahmoud A
Zaynab H. Fadel
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Preparation and Identification of some new Pyrazolopyrin derivatives and their Polymerizations study

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Synthesis And Characterization Of Some New Metal Complexes Of Ethyl Cyano (2-Methyl Carboxylate Phenyl Azo Acetate)
Ethyl cyano (2-methyl carboxylate) phenyl azo acetate
complexes
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Complexes of (Co2+, Ni2+, Cu2+, Zn2+, Cd2+ and Hg2+) with the ligand Ethyl cyano (2-methyl carboxylate phenyl azo acetate) (ECA) have been prepared and characterized by FTIR, (UV-Visible), Atomic absorption spectroscopy, Molar conductivity measurements and magnetic moments measurements. The following general formula has been suggested for the prepared complexes [M(ECA)2]Cl2 where M = (Co2+, Ni2+, Cu2+ ,Zn2+, Cd2+, Hg2+) and the geometry is octahedral.

Publication Date
Mon Apr 01 2019
Journal Name
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synthesis new hetrocyiclic compound derived from fouroic acid
wissam khalifa jasim
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