Preferred Language
Articles
/
bsj-2012
Optimum conditions for ascorbic acid determination in three Iraqi citrus using HPLC technique
...Show More Authors

A high-performance liquid chromatography method was employed for the quantitative determination of ascorbic acid (AA) which called vitamin C in three types of Iraqi citrus (orange mandarin and aurantium ) and to establish this goal , evaluation of ascorbic acid degradation is so important due to its significant criticality when exposure to ordinary atmospheric conditions. The chromatographic analysis of AA was carried out after their sequential elution with KH2PO4 ( as mobile phase) by reverse-phase HPLC technique with C8 column and UV detection at 214 nm. .Bad resolutions was appeared clearly for C8 column , so another alternative condition were carried out to improve the resolution by replacement of C8 by C18 column .Statistical treatments were used to calculate relative standard deviation (RSD%) for the results to gain acceptable confidence to the present work , so the linearity of calibration curve, accuracy, and repeatability of this method are all satisfactory.

Crossref
View Publication Preview PDF
Quick Preview PDF
Publication Date
Mon Sep 16 2019
Journal Name
Ibn Al-haitham Journal For Pure And Applied Sciences
Determination of Ibuprofen in Pharmaceutical Formulations Using Differential Pulse Polarography
...Show More Authors

     A reliable differential pulse polarographic (DPP) method has been developed and applied for the determination of ibuprofen IBU in dosage form with dropping mercury electrode (DME) versus Ag/AgCl. The best peak was found at cathodic peak of -1.18 V in phosphate buffer at pH=4 and 0.025M of KNO3 as supporting electrolyte. In order to obtaine the highest sensitivity, instrumental and experimental parameters were examined including the type and concentration of supporting electrolyte, pH of buffer solution, pulse amplitude and voltage step time. Diffusion current showed a direct linear relationship to ibuprofen concentration in the range of (5 – 30) μg. mL-1 (2.43× 10-5

... Show More
View Publication Preview PDF
Crossref (2)
Crossref
Publication Date
Sun Jun 02 2024
Journal Name
Methods And Objects Of Chemical Analysis
Simultaneous Spectrophotometric Determination of Piroxicam, Naproxen, Diclofenac Sodium and Mefenamic Acid in Pharmaceutical Formulations by Partial Least Squares Method
...Show More Authors

A chemometric method, partial least squares regression (PLS) was applied for the simultaneous determination of piroxicam (PIR), naproxen (NAP), diclofenac sodium (DIC), and mefenamic acid (MEF) in synthetic mixtures and commercial formulations. The proposed method is based on the use of spectrophotometric data coupled with PLS multivariate calibration. The Spectra of drugs were recorded at concentrations in the linear range of 1.0 - 10 μg mL-1 for NAP and from 1.0 - 20 μg mL-1 for PIR, DIC, and MEF. 34 sets of mixtures were used for calibration and 10 sets of mixtures were used for validation in the wavelength range of 200 to 400 nm with the wavelength interval λ = 1 nm in methanol. This method has been used successfully to quant

... Show More
View Publication
Scopus Clarivate Crossref
Publication Date
Fri Aug 30 2024
Journal Name
Iraqi Journal Of Science
The Dissipation of the Kinetic Energy for 2D Bounded Flow by Using Moment-Based Boundary Conditions with Burnett Order Stress for LBM
...Show More Authors

     In this article, the lattice Boltzmann method with two relaxation time  (TRT)  for the  D2Q9 model is used to investigate numerical results for 2D flow. The problem is performed to show the dissipation of the kinetic energy rate and its relationship with the enstrophy growth for 2D dipole wall collision. The investigation is carried out for normal collision and oblique incidents at an angle of . We prove the accuracy of moment -based boundary conditions with slip and Navier-Maxwell slip conditions to simulate this flow. These conditions are under the effect of Burnett-order stress conditions that are consistent with the discrete Boltzmann equation. Stable results are found by using this kind of boundary condition where d

... Show More
Scopus Crossref
Publication Date
Tue Feb 13 2024
Journal Name
Iraqi Journal Of Science
Suggested method of Estimation for the Two Parameters of Weibull Distribution Using Simulation Technique
...Show More Authors

In this paper, suggested method as well as the conventional methods (probability
plot-(p.p.) for estimations of the two-parameters (shape and scale) of the Weibull
distribution had proposed and the estimators had been implemented for different
sample sizes small, medium, and large of size 20, 50, and 100 respectively by
simulation technique. The comparisons were carried out between different methods
and sample sizes. It was observed from the results that suggested method which
were performed for the first time (as far as we know), by using MSE indicator, the
comparisons between the studied and suggested methods can be summarized
through extremely asymptotic for indicator (MSE) results by generating random
error

... Show More
View Publication Preview PDF
Publication Date
Tue Nov 02 2021
Journal Name
Iraqi Journal Of Science
Mapping Land Cover/Land Use for Change Derivation Using Remote Sensing and GIS Technique
...Show More Authors

    Deriving land cover information from satellite data is one of the most common applications employed to monitor, evaluate, and manage the environment. This study aims to detect the land cover/land use changes and calculate the areas of different land cover types in Baghdad, Iraq, for the period from 2015 to 2020, using Landsat 8 images. The supervised Maximum Likelihood Classification (MLC) method was applied to classify the images. Four land cover types were obtained, namely urban, vegetation, water, and barren soil.  Changes in the four land cover classes during the study period were observed. The extent of the urban, vegetation, and water areas was increased by about 7.5%, 9.5%, and 1.5%, respectively, whereas t

... Show More
View Publication Preview PDF
Scopus (1)
Crossref (1)
Scopus Crossref
Publication Date
Thu Mar 09 2017
Journal Name
Ibn Al-haitham Journal For Pure And Applied Sciences
Corrosion Inhibition of Aluminium in Acidic Medium using Amino Acid (Methionine)
...Show More Authors

  Corrosion behavior of aluminium in 0.6 mol. dm-3 NaCl solution in acidic medium 0.7 was investigated in the absence and presence of different concentrations of amino acid, methionine, as environmentally – friendly corrosion inhibitor over temperature range (293-308)K. The investigation involved electrochemical polarization method using potentiostatic technique and optical microscopy, the inhibition efficiency increased with an increase in inhibitor concentration but decreased with increase in temperature. Results showed that the inhibition occurs through adsorption of the inhibitor molecules on the metal surface and it was found to obey Langmuir adsorption isotherm. Some thermodynamic parameters ∆. and activation ener

... Show More
View Publication Preview PDF
Publication Date
Wed Jan 01 2020
Journal Name
Journal Of King Saud University - Science
Three iterative methods for solving second order nonlinear ODEs arising in physics
...Show More Authors

View Publication
Crossref (12)
Crossref
Publication Date
Sun Jul 30 2023
Journal Name
Iraqi Journal Of Science
Production of Lactic Acid by lactobacilli using Legume Flours
...Show More Authors

       Due to their high nutritional value, richness in carbohydrates and good source of protein, legumes are considered essential for human diet. Legumes flours were used as fermentable material for lactic acid production. Hence, previously isolated lactobacilli strains were used in this study. The strains showed strong microbial growth and their survival in glucose-containing MRS medium and were described using a modified Gompertz equation. Lactobacilli exhibited the shortest latency phase in MRS-glucose medium. While the highest lactic acid produced was 15.40g/l by Lpb. pentosus U1 isolate after 48hours. Furthermore, these strains were evaluated in flours samples for acidification capacity. The results showed a decrease

... Show More
View Publication Preview PDF
Scopus Crossref
Publication Date
Wed Jun 11 2003
Journal Name
Iraqi Journal Of Laser
Microdrop Size Measurement in a Mixing Unit Using Laser Technique
...Show More Authors

One of the troublesome duties in chemical industrial units is determining the instantaneous drop size distribution, which is created between two immiscible liquids within such units. In this work a complete system for measuring instantaneous droplet size is constructed. It consists of laser detection system (1mW He-Ne laser), drop generation system (turbine mixer unit), and microphotography system. Two immiscible liquids, water and kerosene were mixed together with different low volume fractions (0.0025, 0.02) of kerosene (as a dispersed phase) in water (as a continuous phase). The experiments were carried out at different rotational speed (1180- 2090 r.p.m) of the turbine mixer. The Sauter mean diameter of the drops was determined by la

... Show More
View Publication Preview PDF
Publication Date
Thu Mar 30 2023
Journal Name
Iraqi Journal Of Science
Spatiotemporal Drought Monitoring Using Remote Sensing Technique in Babel-Iraq
...Show More Authors

       Drought is one of the most natural hazards that may harm human life and property under different weather and environmental conditions. This study used remote sensing data to monitor agricultural and meteorological drought in Babel Governorate. Drought maps were drawn using Landsat 8 images based on Normalized Difference Vegetation Index (NDVI) for 2015, 2018, and 2021. The meteorological drought was assessed using a standardized precipitation index (SPI 12) for the same years. The results showed that the SPI-12 indicated near-normal drought types in 2015 and 2018, whereas SPI values showed a lower value in 2021. Two drought categories were identified which were moderate drought and severe drought. The NDVI results showed tha

... Show More
View Publication Preview PDF
Scopus Crossref