يهتم هذا البحث بتحضير وتشخيص ليكاند ثنائي السن -: [4-(5,5-dimethyl-3-oxocyclohex-1-enylamino)-N-(5-methylisoxazol-3-yl)benzene sulfonamide] [H2L] وذلك من صهر السلفاميثوكسازول مع الدايميدون بدرجة ºC)140 (ُ ولمدة نصف ساعة , حظر معقد الكوبالت مѧن تفاعѧل هѧذا الليكاند مع ايون الكوبالѧت الثنѧائي وبطريقѧة التصѧعيد الا ُ رجѧاعي باسѧتعمال الايثѧانول وسѧطا للتفاعѧل . شѧخص الليكانѧد والمعقѧد المحضر باستعمال الطرائق الطيفية التي اثبتت ان المعقد ذات شكل هندسѧي ربѧاعي السѧطوح حѧول الايѧون المركѧزي . كمѧا تѧم ايجاد نسبة أتحاد الفلز بالليكاند المحضر (L:M (باستعمال طريقتي النسبة المولية والتغيرات المستمرة وكانѧت النسѧبة (1:1) . دُرست الظروف المثلى لازالة معقد الكوبالت من خلال الامتزاز على سѧطح البنتونايѧت وكѧذلك دراسѧة المتغيѧرات المѧؤثرة فѧي عملية الامتزاز وهي زمن الاتزان ودرجة الحرارة وقѧيم pH ووزن المѧادة المѧازة وحجѧم دقѧائق المѧادة المѧـازة . وقѧد أظهѧـرت النـتائـج ان الزمـن اللازم للوصـول الى اتـزان التـركيز هو min) 60 (. بينما النمط العام لايزوثيرمات الامتزاز هو مـن نѧوع (1L (وفق تصنيف جيلز . وقد حسبت قيم الدوال الثرموديناميكية (ΔG , ΔH ,ΔS (وفسرت النتائج في ضوئها .
This research aims to measure the discrepancy between the accounting income which is prepared according to generally accepted accounting principles and the tax income that is being prepared according to the rules and tax laws, and find out the most important differences that arise between incomes.The research found the most important to the following conclusions:1.Faces determining the tax base for companies subject to income challenges related to the weakness of the efficiency and the possibility of technical angel tax and its ability to examine the financial statements submitted to the tax administration tax.2.That the tax system in Iraq does not comply with accepted accounting principles generally accepted.The research recommends the
... Show MoreThe Legend between reality and its future Treatment in threatre analytics study
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هدفت الدراسة الى معرفة:
- الاسباب النفسية والاجتماعية لفرط النشاط الحركي لدى تلاميذ المرحلة الابتدائية.
- الاسباب الاكثر حدة وتكراراً من وجهة نظر افراد العينة. اقتصر البحث على معلمي ومعلمات المرحلة الابتدائية لمحافظة بغداد للعام الدراسي 2004/2005.
تم بناء استبيانين
أ- استبيان خاص بالاسباب النفسية.
ب- استبيان
... Show MoreIn this paper, the researcher suggested using the Genetic algorithm method to estimate the parameters of the Wiener degradation process, where it is based on the Wiener process in order to estimate the reliability of high-efficiency products, due to the difficulty of estimating the reliability of them using traditional techniques that depend only on the failure times of products. Monte Carlo simulation has been applied for the purpose of proving the efficiency of the proposed method in estimating parameters; it was compared with the method of the maximum likelihood estimation. The results were that the Genetic algorithm method is the best based on the AMSE comparison criterion, then the reliab
... Show MoreAbstract :
The research aims to study the basic concepts of banking productivity and discuss different approaches to study what ends to identify the most important possible standards applied to measured within the Iraqi banking environment as well as research into the causes of low and high Iraqi banking productivity and identify possible treatments to curb those reasons as to ensure the rise. And in line with the research problem, which states what is the level of productivity and what are the causes of decline and the rise in private banking research sample individually. And what the Iraqi private banks and what is the relationship between performance and the impact of productivity change in the perform
... Show MoreThe problem of research is that the colleges of education in general and the College of Education in particular continue to follow traditional administrative patterns and that there is a complaint that the educational outputs do not match the aspirations of the society and its future directions. The aim of the research is to identify the reality of quality assurance standards in the college and to create a future vision for these standards to apply them. The researcher has designed a questionnaire based on the responses of the research sample which consisted of a group of university teachers to identify the quality assurance standards. The findings revealed that it is necessary to find a clear approach to apply the standards of quality i
... Show MoreThe aim of the research to show the direction of kindergarten‘s
headmasters with students and know the educational technique used by
the teachers with students inside kindergarten , also to know the
differences of headmasters directions towards these technique
according to changing of social state (married , unmarried ) and age
state (30-38) (39-47) (48-56) .
Also shows the sign among the direction of head masters and
educational technique used by teachers with student, where as the
importance of this research shows the importance of the kindergarten
stage and the importance of management .
The role of headmaster and teacher consider the relationship between
them and the mother so that this origin direc
Abstract The success of the system of government in any country needs to have a handle on the amount of power efficiency , capacity , capability and wisdom, Iraq has gone through since its inception through several stages of time, namely: The first stage: which ran from August 23, 1921 until July 14, 1958 and was ruling monarchy (rule of the royal family) and punishing power of political elites both of them and works access to power without taking into consideration the laws and principles of the Constitution, and as a result of the inability of civilian powers and political parties access to power to grant that army officers regulatory and disciplinary specifications as well as possessing arms and overthrow the rule of the minority coup
... Show MoreA political perusal of Initiations in Declaring Middle East a District vacant of mass Destruction weapons