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The [2-hydroxy -1,2-diphynel-ethanone oxime] was reacted with 1,2- dichloroethan to
give the new ligand [H2L].this ligand was reacted with some metal ions
(Co(II),Ni(II),Cu(II),Zn(II) and Cd(II) in methanol as a solvent to give a series of new
(1:1)complexes of the general formula [ M(HL)]Cl ,( where : M=
Co(II),Ni(II),Cu(II),Zn(II) and Cd(II)) are isolated All compounds have been characterized
by spectroscopic methods [ I.R , U.V -Vis ] atomic absorption . Chloride content along
with conductivity measurements. From the above data the proposed molecular structure
for (Co, Cu, Ni, Zn and Cd) complexes adopting a tetrahedral structure.