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This work includes preparing of some new derivatives of 1,2,4-Triazoles and
oxazoles from the reaction between 3,5-dimethyl phenol and chloroethyl acetate in
the presence of potassium carbonate and dry acetone to obtain the ester ethyl 3,5-
dimethyl phenoxy acetate , then converted this ester to Thiosemicarbazone and
Semicarbazone. Then ,the Triazoles were prepared from the cyclization of these
Thiosemcarbazones and Semicarbazones in alkaline media( potassium hydroxide
solution) . The prepared compounds were characterized by spectral methods FT-IR
,1H-NMR and measurement of some of its physical properties and evaluation of the
biological activity for some of them.