New substituted coumarins derivatives were synthesized by using nitration reaction to produce different nitro coumarin isomers which were separated from these isomers by using different solvent, and the reduction of nitro compounds was done to give corresponding amino coumarins. Temperature and reaction time of reaction were very important factors in determining the most productive nitro isotopes. A low temperature for three hours was sufficient to give a high product of a compound 6-nitro coumarin while increasing the temperature for a period of twenty-four hours that gave a high product of 8-nitro-coumarin. The synthesized compounds were confirmed by FT-IR,1 H-NMR, and13 C-NMR spectroscopy and all final compounds were tested for their ant

The  purpose  of  the  paper  is  to  tind  the  degree  of  the approximation of a functions  f be bounded , measurable and defined

in  interval   [a,h]by  Bernstein  polynomial  in  LP    space  1 $ p < oo by

using Ditzian-Totik modulus  of smootlmess  and  k 1n  average modvlus of smoothness.

A procedure, depending on the derivatization and determination of aniline was depicted andvalidated in this study. 8-hydroxyquinoline (8-HQ) was used as the derivatizing agent for thedetermination of aniline. An optimization study was performed for the derivatization reaction, i.e.,the diazonium coupling reaction, the optimum parameters were as follows: 22 mM of hydrochloricacid, 54mM of sodium hydroxide, and 1.8mM of sodium nitrate. The optimization study of themethod of cloud point extraction (CPE) revealed that the extraction solvent was 0.5 ml of Triton X-100, the optimum temperature was 90 °C, and the incubation time was 25 min. The linearity,correlation coefficients, molar absorptivities, and limits of detection were improved using t

Esterification reaction is most important reaction in biodiesel production. In this study, oleic acid was used as a suggested feedstock to study and simulate production of biodiesel. Batch esterification of oleic acid was carried out at operating conditions; temperature from 40 to 70 °C, ethanol to oleic acid molar ratio from 1/1 to 6/1, H2SO4 as the catalyst 1 and 5% wt of oleic acid, reaction time up to 180 min. The optimum conditions for the esterification reaction were molar ratio of ethanol/oleic acid 6/1, 5%wt H2SO4 relative to oleic acid, 70 °C, 90 min and conversion of oleic 0.92. The activation energy for the suggested model was 26625 J/mole for forward reaction and 42189 J/mole for equilibrium constant. The obtained results s

        A newly developed analytical method was conducted for the determination of Ketotifen fumarate (KTF) in pharmaceuticals drugs via quenching of continuous fluorescence of 9(10H)-Acridone (ACD). The method was applied using flow injection system of a new homemade ISNAG fluorimeter with fluorescence measurements at ± 90◦ via 2×4 solar cell. The calibration graph was linear in the range of 1-45 mmol/L, with correlation coefficient r = 0.9762 and the limit of detection 29.785 µg/sample from the stepwise dilution for the minimum concentration in the linear dynamic ranged of the calibration graph. The method was successfully applied to the determination of Ketotifen fumarate in two different pharma

The repeated measurement design is called a complete randomized block design for repeated measurement when the subject is given the all different treatments , in this case the subject is considered as a block . Many of nonparametric methods were considered like Friedman test (1937) and Koch test(1969) and Kepner&Robinson test(1988) when the assumption of normal distribution of the data is not satisfied .as well as F test  when the assumptions of the analysis of variance is satisfied ,where the observations within blocks are assumed to be equally correlated . The purpose of this paper is to summarize the result of the simulation study for comparing these methods as well as present the suggested

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:يمتاز مرض قصور الدرقية بإنخفاض مستوى هرمونات T3و T4الضرورية لعمليات إنتاج الطاقة و حيوية الجسم ؛ لذلك ترافق هذه الحالة إضطرابات في عمليات الأيض المختلفة في الجسم . أجريت الدراسة في المركز التخصصي للغدد الصم و السكري في بغداد ، و شملت 70ًاضيرممن مرضى قصور الدرقية ، تم تشخيص الحالة لديهم عن طريق قياس مستويات الهرمونات (TSH,T4,T3). كما شملت 60اوريتخأًاصخشبشكل عشوائي من غير مرضى الغدة ، و قد تم التأكد من سلامة الغدة وعدم

ان ايجاد وسائل و طرائق تدريبية وتمارين مستحدثة بالاعتماد على مختلف العلوم وانعكاس ذلك على الافكار الجديدة ولعل واحدة من هذه التمارين اسلوب التمرينات الساكيو  (S.A.Q) وتمرينات الساكيو من التمرينات الحديثة المستخدمة في المجال الرياضي كونها تحسن من كفاءة الأداء اما مشكلة البحث لاحظت الباحثتان هناك هبوط في انجاز100م حواجز, وهذا يتطلب التقصي والبحث عن أسباب هذا الهبوط والوقوف على نقاط الضعف الواضحة في مراحل الع

إن الأبحاث العلمية كانت و لا تزال تحضا باهتمام الكثير من العلماء و المختصين في مجال التربية الرياضية بشكل عام و الجمناستك بشكل خاص لإيجاد أحدث الوسائل و الأدوات التي تساعد على سهولة توصيل المعلومات إلى المتعلمين و بدرجة عالية من الكفاءة, إذ يمكن للمتعلم الاستعانة بوسائل تعليمية عديدة منها القراءات المختلفة و المواد المبرمجة أو الأفلام و الوسائل السمعية و البصرية و ما إلى ذلك, فالمعلم الذي يستخدم هذه الوسائل