يهدف البحث إلى تحضير سلسلة جديدة من معقدات العناصر الانتقالية ثنائية التكافؤ (الكوبلت, النيكل, النحاس, الخارصين ,الكادميوم والزئبق) مع المركبات الحلقية غير المتجانسة (L1) و(L2) والمشتقة من تفاعل 2,1- فينيلين ثنائي امين وسايكلوهكسان -2,1-ثنائي امين مع المركب الوسطي (Pr) على التوالي. شخصت المعقدات ذات الصيغة العامة :- [M(L1or L2)Cl2] بواسطة طيف الرنين النووي المغناطيسي البروتوني والكربوني وقياسات الأشعة تحت الحمراء والطيف الإلكتروني ودرجات الانصهار و التوصيلية المولارية و التحليل الدقيق للعناصر C.H.N.والنسبة المئوية للفلز %M والحساسية المغناطيسية. استنادا إلى النتائج المعطاه للدراسات المذكورة فقد تم اقتراح الشكل ثماني سطوح للمعقدات المحضرة من خلال ارتباط ذرات النتروجين الاربعة لمجموعة (NH) في المركبات الحلقية غير متجانسة (L1) و(L2) مع الأيونات الفلزية اضافة الى ايوني الكلور. ثم تم تحضير معقد النحاس النانويAuNPs −[CuL1Cl2] من خلط محلول معقد النحاس مع محلول الذهب النانوي(AuNPs) ، وتم إجراء التشخيص باستخدام طرق مختلفة ، بما في ذلك FTIR و UV-Vis و FESEM. تم اختبار قدرة التثبيط للمركبات المحضرة بما في ذلك معقد النحاس النانوي، ضد نوعين من البكتيريا المختارة (Escherichia coli) والموجبة (Staphylococcus aurous) بتقنية الانتشار ، حيث أظهرت النتائج أن قدرة المركب النانوي على تثبيط كلا النوعين من البكتيريا كانت أكبر من المركبات الحلقية غير المتجانسة(الليكاندات) ومعقد النحاس الحر, كما تم اختبار معقد النحاس الحر ومعقد النحاس النانوي على خط خلايا سرطان الرئة (A456) وخط الخلايا الطبيعي (REF) والمقارنة بين المعقدين حيث اظهر معقد النحاس النانوي نتائج ممتازة في امكانية اختباره مستقبلا كعلاج لسرطان الرئة
In this paper we will explain ,how use Bayesian procedure in analysis multiple linear regression model with missing data in variables X's as the new method suggest , and explain some of missing Patterns under missing mechanism , missing complete at random MCAR and compare Bayesian estimator with complete case estimator by use simulation procedure .
Praise to Allah, Lord of the Worlds. Thank you very much. Blessed. As his face should be majestic and great. His authority, and may peace and blessings be upon our master Muhammad, a perpetual blessing until the Day of Judgment
And upon the God of purity, His righteous companions, and those who follow them in righteousness until the Day of Judgment. But after:-
Anyone who looks into the history of nations, peoples, and the conditions of human beings will see that naturalization as a person’s affiliation to a particular state is something that happened only in recent centuries. In ancient times, a person’s loyalty was to the tribe to which the person belonged, and he was integrated into it and attributed to it, and in
... Show Moreافرض ان (X1, X2, …. , Xn) هي عينة عشوائية من توزيع له دالة احتمالية الكثافة . المثال المعتاد في مثل هكذا تقدير للامكان الاعظم (MLE) هو ليس وحيد باخذ ليكون كثافة منتظمة عليه، مثل .
انظر [Bicked and Doksum (1977, P111)] او [Hogg and Craig (1978, P(207)] بالاضافة الى احضار بعض الامور غير الطبيعية.
... Show MoreThis paper deals with the modeling of a preventive maintenance strategy applied to a single-unit system subject to random failures.
According to this policy, the system is subjected to imperfect periodic preventive maintenance restoring it to ‘as good as new’ with probability
p and leaving it at state ‘as bad as old’ with probability q. Imperfect repairs are performed following failures occurring between consecutive
preventive maintenance actions, i.e the times between failures follow a decreasing quasi-renewal process with parameter a. Considering the
average durations of the preventive and corrective maintenance actions a
... Show MoreThis study was carrid out to produce animal gelatin from chicken skin. Gelatin was prepared by the chemical method using HCl 2% and extraction at the temperature degree 70, 80, 90 c° and at the period of time 4, 6, 8 hours, calculated the yield, functional and sensory characteristics were measured at. The result also demonstrated that the produced gelatin have good functional properties in solubility, viscosity, gelling capacity, water absorpation, lipid binding, emulsification. viscosity was higher in gelatin prepared at 70 c° and period of extraction 8 hours and reached 1.0846 cp. Gelatin prepared were featured by highe gelling capacity at 1% for all extraction time periods. The produced gelatin was characterized by good sensory qual
... Show MoreThis study aims to identify the impact of social support on breast cancer patients’ psychological rigidity using a sample in Ramallah and al-Bireh. A descriptive correlative approach was adopted to fulfill the goals of the study and a questionnaire consisted of two criteria: social support and psychological rigidity, which was adopted as a tool for data collection for the study. In order to achieve the goals of the study, the researcher selected a convenient sample that consisted of 123 female breast cancer patients in Ramallah and al-Bireh. This sample represented 50% of the original patient population. The study showed that the average estimated percentage of social support and psychological rigidity for women with breast cancer, in
... Show MoreThis paper proposes a new method Object Detection in Skin Cancer Image, the minimum
spanning tree Detection descriptor (MST). This ObjectDetection descriptor builds on the
structure of the minimum spanning tree constructed on the targettraining set of Skin Cancer
Images only. The Skin Cancer Image Detection of test objects relies on their distances to the
closest edge of thattree. Our experimentsshow that the Minimum Spanning Tree (MST) performs
especially well in case of Fogginessimage problems and in highNoisespaces for Skin Cancer
Image.
The proposed method of Object Detection Skin Cancer Image wasimplemented and tested on
different Skin Cancer Images. We obtained very good results . The experiment showed that
The study aims to determine the responsibility of nursing staff for medical errors that accompany the surgery at the hospital , which is one of the important issues that the importance of determining the responsibility of landlords nursing medical errors in the hospital was the rationale in choosing the subject. Since study included cases of errors nursing staff of (22) case. While the checklist distributed to a sample of nursing Angel Group in Sadr Teaching Hospital 's (100) nurs According to the problem, the study in determining the responsibility of nursing staff for medical errors that are not important for the hospitals. Has shown results of the study agreement members of the study sample that the clarity of the power posses
... Show MoreMetal enhanced fluorescence (MEF) is an unequaled phenomenon of metal nanoparticle surface plasmons, when light interacts with the metal nanostructures (silver nanoparticles) which result electromagnetic fields to promote the sensitivity of fluorescence. This work endeavor to study the influence of silver nanoparticles on fluorescence intensity of Fluoreseina dye by employment mixture solution with different mixing ratio. Silver nanoparticles had been manufactured by the chemical reduction method so that Ag NP layer coating had been done by hot rotation liquid method. The optical properties of the prepared samples (mixture solution of Fluoreseina dye solutions and colloidal solution with 5 minutes prepared of Ag NPs) tested by using UV-V
... Show MoreLocal food samples investigated for the presence of pathogenic bacteria. Hash meat sample was used to isolate Escherichia coli and chicken meat (poultry) was used to isolate Salmonella typhi. Biochemical tests and API20E system used in order to identify these isolates. Two natural vinegar samples (dates & apple cider) were used in order to study its antibacterial activity against the two tested bacteria. Disc diffusion method was used, the results showed that two vinegar samples have antibacterial activity against the two tested bacteria. Date vinegar showed inhibition zone 19mm against E. coli & 9mm against S. typhi, while Apple cider vinegar showed diameter of inhibi
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