يهدف البحث إلى تحضير سلسلة من معقدات العناصر الانتقالية ثنائية التكافؤ(المنغنيز, الكوبلت, النيكل, الخارصين والكادميوم) مع المركب الجديد(KL) والمشتق من تفاعل ثنائي كبريتيد الكاربون و المركب الوسطي (HD). شخصت المعقدات ذات الصيغة العامة[M(L)2] بواسطة طيف الرنين النووي المغناطيسي البروتوني والكربوني للمركب الجديد وقياسات الأشعة تحت الحمراء والطيف الإلكتروني ودرجات الانصهار و التوصيلية المولارية و تحليل العناصر .C. H .N S والنسبة المئوية للفلز M في المعقدات والحساسية المغناطيسية والدراسة الحرارية للمركب (KL) وبعض المعقدات. استنادا إلى النتائج المعطاه للدراسات المذكورة فقد تم اقتراح الشكل رباعي السطوح للمعقدات المحضرة من خلال ارتباط ذرات الكبريت لمجموعة الثايول في المركب (KL) مع الأيونات الفلزية وكذلك تمت دراسة الفاعلية الحيوية للمركب المشتق ومعقداته ضد نوعين من البكتريا السالبة (Escherichia coli) والموجبة (Staphylococcus aurous) بتقنية الانتشار كما تم استخدام المركب المحضر (KL) كمثبط لتأكل سبيكة الفا-براص في محلول ملحي لكلورید الصودیوم بتركیز 0.6 مول. دسم-3 لثلاث قيم من الدوال الحامضية (2،4, 7) في ثلاث درجات حرارية مختلفة تراوحت (288-308) مطلقة وبتركيز مقداره 3-10مول.دسم3- لمركب (KL) باستعمال تقنية المجھاد الساكن وتم التعبير عن النتائج من خلال تسجيل قیم تيار التآكل (icorr) حيث اوضحت النتائج ان المركب قام بعمل التثبيط لتأكل سبيكة الفا- براص عند قيمتي الدالة الحامضية 7,4 وكما تم حساب كفاءة التأكل P% اضافة الى الثوابت الثرموديناميكية لعملية التثبيط
Aleppo bentonite was investigated to remove ciprofloxacin hydrochloride from aqueous solution. Batch adsorption experiments were conducted to study the several factors affecting the removal process, including contact time, pH of solution, bentonite dosage, ion strength, and temperature. The optimum contact time, pH of solution and bentonite dosage were determined to be 60 minutes, 6 and 0.15 g/50 ml, respectively. The bentonite efficiency in removing CIP decreased from 89.9% to 53.21% with increasing Ionic strength from 0 to 500mM, and it increased from 89% to 96.9% when the temperature increased from 298 to 318 K. Kinetic studies showed that the pseudo second-order model was the best in describing the adsorption sys
... Show MorePolymer additives binder system provides many properties useful in thermal energy storage (TES) then developed the efficient energy storage materials and green strength bodies system.
This paper studies the thermal energy storage property for polyvinyl alcohol (PVOH) / paraffin wax (WPw) blends. To enhance paraffin wax thermal conductivity, PVOH as a material which high conductivity was employed. A fixed weight of Paraffin wax was dispersed with PVOH heterogeneously at different additive weights ratios of PVOH/Pw (50/50, 67/33, 75/25, and 80/20) wt. ratio respectively. The composite material was prepared using wetted pressing method.
Both base materials (polyvinyl alcohol and paraffin wax) were scanned using differential
... Show MoreThe field of Optical Character Recognition (OCR) is the process of converting an image of text into a machine-readable text format. The classification of Arabic manuscripts in general is part of this field. In recent years, the processing of Arabian image databases by deep learning architectures has experienced a remarkable development. However, this remains insufficient to satisfy the enormous wealth of Arabic manuscripts. In this research, a deep learning architecture is used to address the issue of classifying Arabic letters written by hand. The method based on a convolutional neural network (CNN) architecture as a self-extractor and classifier. Considering the nature of the dataset images (binary images), the contours of the alphabet
... Show MoreIn this research, the effect of adding two different types of reinforcing particles was investigated, which included: nano-zirconia (nano-ZrO2) particles and micro-lignin particles that were added with different volume fractions of 0.5%, 1%, 1.5% and 2% on the mechanical properties of polymer composite materials. They were prepared in this research, as a complete prosthesis and partial denture base materials was prepared, by using cold cure poly methyl methacrylate (PMMA) resin matrix. The composite specimens in this research consist of two groups according to the types of reinforced particles, were prepared by using casting methods, type (Hand Lay-Up) method. The first group consists of PMMA resin reinforced by (nano-ZrO
... Show MoreThis study aimed to discover the reality of the teacher's maintainced of order and classroom management from the perspective of teachers themselves.
A social survey with an introduce sample that consist (180) male and female teachers from the provinces of Ajloun and Jerash in 2008-2009. To achieve the objective of the study was developed for this purpose and the results have shown the existence of statistically significant differences in marinating order and the management of class and in favor of females, the results also showed Statistically significant differences regarding the academic qualification and for the benefit of holders of master degrees and more compared to those with bachelor's degree.
... Show MoreThe caliphs of Tukalti Able III (Tiglath-pileser) sustained their extension and enclosure strategy whom they were highly talented with outstanding potentialities. They performed their political plan of extinguishingthe ambitions of the upper class and the internal uprisings. The Assyrian Kingdom, in the eighth century BC reached to the highest degree of expansion that no other ancient Iraqi kingdom had reached It dominated the whole near eastbut it did not have absolute command due to the subsequent uprisings that out bursted in the regions attached to the kingdom near the borders.
The aim of this research is to study the surface alteration characteristics and surface morphology of the superhydrophobic/hydrophobic nanocomposite coatings prepared by an electrospinning method to coat various materials such as glass and metal. This is considered as a low cost method of fabrication for polymer solutions of Polystyrene (PS), Polymethylmethacrylate (PMMA) and Silicone Rubber (RTV). Si were prepared in various wt% of composition for each solutions. Contact angle measurement, surface tension, viscosity, roughness tests were calculated for all specimens. SEM showed the morphology of the surfaces after coated. PS and PMMA showed superhydrophobic properties for metal substrate, while Si showed hydroph
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The research deals with the statement of the importance of unanimous in Islamic Sharia in terms of being the third source of Islamic legislation after the Holy Qur’an and the Sunnah of the Prophet, and the extent of interest of the scholars of interpretation in it, and those who took great interest in mentioning what was agreed upon in every site that necessitated mentioning its issues within, or mentioning an event that has encountered an unanimous, and in various sciences, to extract and extrapolate Sharia rules when these rules are lost in the texts, because it is based on them and derived from them. Among these distinguished scholars is Muhammad bin Jarir al-Tabari. Besides, the research discusses in
... Show MoreSamuel Beckett’s Happy Days (1961) clearly portrays a lack of communication among the characters of the play which refers to the condition of modern man. This failure of communication led Samuel Beckett to use a lot of pauses and silences in all plays written instead of using words. To express the bewilderment of the modern man during the 20th century, Beckett adopts the use of no language strategy in the dramatic works. After World War II, people were without hope, religion, food, jobs, homes, or even countries. Beckett gave them a voice. He used a dramatic language out of everyday things, in which silence was part of the syntax as a poetic repetition. Language is no more important to the modern man; instead, he us
... Show MoreAccording to the importance of the subject of research, and the importance of the surveyed organization as a dynamic sector of the country in general , The research attempts to suggest to service organizations in general reconsidering the currently adopted mechanisms in the redesign of its functions , and in the services provided industry . The data was collected from (98) Director Mangers , head of department and head of division . The research tool is the questionnaire , which included (50) items . The results show Significant Effect & Correlation relationship between the two variables due to their dimensions . These lead to he application of job enrichment technology will increase the organization's ability to possess efficient hu
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