An investigation into the implications of partial substitution of selenium with lead on the thermal properties for S60Se40-XPbX Chalcogenide Compound

doi:10.1088/1742-6596/2857/1/012007

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Publication Date

Tue Oct 01 2024

Journal Name

Journal Of Physics: Conference Series

Volume

2857

Issue Number

1

DOI

10.1088/1742-6596/2857/1/012007

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An investigation into the implications of partial substitution of selenium with lead on the thermal properties for S60Se40-XPbX Chalcogenide Compound

Engineering controlled terms Electric arc furnaces

Glass manufacture

Lead alloys

Melting point

Selenium compounds Engineering uncontrolled terms 950° C

Chalcogenide compound

Melting point method

Partial substitution

Property

Quartz ampoule

Quartz tubes

Rapid cooling

Thermal

Weight ratios Engineering main heading Heat flux

Kareem A.Jasim

Mohamed Muthana

...Show More Authors

AbstractThis study includes the manufacture of four ternary alloys represented S60Se40-XPbX with weight ratios x = 0, 10, 20, and 30 by the melting point method. The components of each alloy were mixed separately, then placed in quartz ampoules and vacuumed out with a vacuum of roger that 10−4 Torr. The ampule was heated in two stages to avoid sudden dissipation and precipitation of selenium on the inner mass of the quartz tube. The ampoule was gradually heated and kept at 450°C for approximately 4 hours followed by 950°C for 10 hours.at a rate of 10 degrees Celsius, the temperature of the electric furnace was increased, and then the ampoule was subjected to rapid cooling with cold water to reach a state of solidity glass-like. The research aims to investigate the effect of adding lead to selenium on the properties of thermal conductivity and heat flux density. It has been noted that the partial replacement of selenium with lead affected these properties significantly.

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Publication Date

Mon Jul 01 2019

Journal Name

Journal Of Physics: Conference Series

Effect of Nickel Substitution On Structural and Electrical Properties of Hg0.5Pb0.5Ba2Ca2Cu3-yNiyO8+δ Superconductor Composite

Laheeb A.

Kareem A.

...Show More Authors

Abstractsix specimens of the Hg0.5Pb0.5Ba2Ca2Cu3-y <italic>Niy </italic>O8+δ (y=0.2,0.4,0.6,0.8,1.0) superconducting compound were prepared by solid state reaction method, with sintering temperature equal to 1123K for 24 hours. The electrical resistivity was examined by the four probe technique, It was found that all the specimens have metallic behavior and increasing the critical temperature with increasing nickel concentration. The optimum critical temperature Tc was found equal ... Show More

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(3)

Publication Date

Tue May 01 2018

Journal Name

Journal Of Physics: Conference Series

Partial substitution of Zn Effects on the Structural and Electrical Properties of High Temperature Hg0.95Ag0.05Ba2Ca2Cu3O8+δ Superconductors

Noor S.

Sabah J.

Kareem A.

Shatha

...Show More Authors

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(10)

(7)

Publication Date

Sun Nov 01 2020

Journal Name

Iop Conference Series: Materials Science And Engineering

Investigation effect of ZnO content on the structural and electrical properties of pulsed laser deposited (NiO)1-x (ZnO)x thin films

NiO

ZnO

PLD

thin films (NiO )1-x(ZnO)x

Ameer J.

Mohmmed Ebd

Bushra A.

...Show More Authors

AbstractThis research is devoted to the effect of investigation of the ZnO content on the structural and electrical properties of (NiO)1-x (ZnO)x films prepared by pulsed laser precipitation on the glass substrate at room temperature. Thin-film (NiO)1-x (ZnO)x sediments were deposited with different composition ratios where x = 0, 0.2, 0.4, 0.6 and 1.0 with a thickness of n150nm. The diffraction pattern for X-ray analysis reveals that the structure of the prepared thin films is identical with the cubic phase and hexadecimal stage of x = 0 and 0.1, respectively while the structure is mixed with the remaining x ... Show More

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(1)

Publication Date

Tue Oct 01 2024

Journal Name

Journal Of Physics: Conference Series

An Effect of Al on the Properties of ZnIn2Se4 Thin Film

Husham Kamil

Bushra H.

...Show More Authors

AbstractZinc-indium-selenide ZnIn2Se4 (ZIS) ternary chalcopyrite thin film on glass with a 500 nm thickness was fabricated by using the thermal evaporation system with a pressure of approximately 2.5×10−5 mbar and a deposition rate of 12 Å/s. The effect of aluminum (Al) doping with 0.02 and 0.04 ratios on the structural and optical properties of film was examined. The utilization of X-ray diffraction (XRD) was employed to showcase the influence of aluminum doping on structural properties. XRD shows that thin ZIS-pure, Al-doped films at RT are polycrystalline with tetragonal structure and preferred (112) orientation. Where the ... Show More

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(2)

Publication Date

Mon Jul 01 2019

Journal Name

Journal Of Physics: Conference Series

Effect of aluminum content on the structural, morphology, and electrical properties of Al1-xSbxthin films

Bushra A

Duaa A

...Show More Authors

AbstractBulk AlxSb1-x samples were prepared with different x ratios (0.1, 0.3, 0.5, 0.7 and 0.9) by quenching technique. This was done throughout mixing the aluminum and antimony elements according to the proper atomic weight and put them in an evacuated quartz ampoule which then sealed and heated at 1273 K for five hours and left to cool in air. Thin films of AlxSb1-xwere prepared by using thermal evaporation under vacuum of 10-5 mbar on glass substrates at room temperature with deposition rate (10-15nm/min) at thickness of ∼ 500nm. The structures of AlxSb1-x bulk and thin films have been studied by X–ray diffraction technique. The results showed that all alloys have polycrystalline structures and the p ... Show More

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Publication Date

Mon Sep 20 2021

Journal Name

Key Engineering Materials

Fabrication of Ge30Te 70-xSbx Glasses Alloys and Studying the Effect of Partial Substitution on D.C Electrical Energy Parameters

Riyadh Kamil

Sarab Saadi

Kassim Mahdi

Kareem Ali

Auday H.

...Show More Authors

The non-linear components has been emphasized for its multiple applications in rewritable recording and data storage devices. Chalcogenide glasses materials are promising due to their high refractive index. In this paper, alloys for Ge₃₀Te_70-xSb_xglasses semiconductor (where x =0.0, 5, 10, 15 and 20) will be fabricated by melt quenching method. The effect of partial substitution on DC electric power parameters, and its knowledge of electrical conduction mechanisms, were investigated to determine the effect of Antimony on the density of extended states, local states, and in Fermi energy states. The electrical measurements revealed the existence of three conduction mechanis

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(36)

(30)

Publication Date

Mon Sep 20 2021

Journal Name

Key Engineering Materials

Effect of Partial Substitution of Sr by Ba on the Structural Properties of Tl0.8Ni0.2Sr2-xBrxCa2Cu3O9-δ System

Mohammed Abdul Nebi

Rihab Nassr

Shatha

Kareem Ali

Auday H.

...Show More Authors

In this manuscript, the effect of substituting strontium with barium on the structural properties of Tl_0.8Ni_0.2Sr_2-xBr_xCa₂Cu₃O_9-δcompound with x= 0, 0.2, 0.4, have been studied. Samples were prepared using solid state reaction technique, suitable oxides alternatives of Pb₂O₃, CaO, BaO and CuO with 99.99% purity as raw materials and then mixed. They were prepared in the form of discs with a diameter of 1.5 cm and a thickness of (0.2-0.3) cm under pressures 7 tons / cm², and the samples were sintered at a constant temperature o

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(4)

(1)

Publication Date

Mon Mar 01 2021

Journal Name

Journal Of Physics: Conference Series

Investigating the Effect of ZnO on the Structural and Optical Properties of (MgO)1-x(ZnO)x via Pulsed Laser Deposition

PLD

(MgO)1-x(ZnO)x

XRD.

Bushra A

...Show More Authors

AbstractThis work concerned with effect of zinc oxide concentrating on the structural and optical properties of (MgO)1-x(ZnO)x thin films. (MgO)1-x(ZnO)x compounds were produced by mixing the two oxides powders accordance to the atomic ratios and compressed as pellets, these pellets were sintered in an oven at temperature1273K for five hours. Thin films from (MgO)1-x(ZnO)x compounds were obtained using pulsed laser deposition technique using Nd:YAG laser . The results of x-ray diffraction as well as UV-Visible- spectrophotometer measurements transmittance of (MgO)<jats></jats> ... Show More

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(2)

Publication Date

Sun Mar 01 2020

Journal Name

Iop Conference Series: Materials Science And Engineering

The Influence of x ratio and Annealing Temperatures on Structural and Optical Properties for (CuO)x(ZnO)1-x Composite Thin Films Prepared by PLD

E M

M F A

A N

...Show More Authors

AbstractThin films of (CuO)x(ZnO)1-x composite were prepared by pulsed laser deposition technique and x ratio of 0≤ x ≤ 0.8 on clean corning glass substrate at room temperatures (RT) and annealed at 373 and 473K. The X-ray diffraction (XRD) analysis indicated that all prepared films have polycrystalline nature and the phase change from ZnO hexagonal wurtzite to CuO monoclinic structure with increasing x ratio. The deposited films were optically characterized by UV-VIS spectroscopy. The optical measurements showed that (CuO)x(ZnO)1-x films have direct energy gap. The energy band gaps of prepared thin films ... Show More

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(5)

Publication Date

Sat May 01 2021

Journal Name

Journal Of Physics: Conference Series

The effect of the Doping with Cobalt Transition Metal on the Dielectric and Structural Properties of Fe0.5CoxMg0.95-xO Nanoparticles Synthesized by Sol-Gel Assisted Auto-Combustion

Tagreed M.

Omar A.

Imad H.

T.A.

...Show More Authors

AbstractThe compound Fe0.5CoxMg0.95-xO where (x= 0.025, 0.05, 0.075, 0.1) was prepared via the sol-gel technique. The crystalline nature of magnesium oxide was studied by X-ray powder diffraction (XRD) analysis, and the size of the sample crystals, ranging between (16.91-19.62nm), increased, while the lattice constant within the band (0.5337-0.4738 nm) decreased with increasing the cobalt concentration. The morphology of the specimens was studied by scanning electron microscopy (SEM) which shows images forming spherical granules in addition to the presence of interconnected chips. The presence of the elements involved in the super ... Show More

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