Sulfamethoxazole (SMX) was added to P-N,N-dimethyl amino benzaldehyde (PDAB) by condensation reaction in acidic medium to form, a yellow colored dye compound which exhibits maximum absorption (λmax) at 450.5 nm. The concentration of (SMX) was determined spectrophotometrically. The optimum reaction conditions and other analytical parameters were evaluated. In addition to classical univariate optimization, design of experiment method has been applied in optimization of the variables affecting the color producing reaction. Beer’s law obeyed in the concentration range of 0.1-10 μg.mL-1 with molar absorptivity of 5.7950×104 L.mol-1.cm-1. The limit of detection and Sandell's sensitivity value were 0.078 μg.mL-1 was 4.3706 μg.cm-2 respectivily. The proposed method could be successfully applied to the determination of (SMX) in synthetic sample and urine.
Spectrophotometric Determination of Sulfamethoxazole with P-N,N-dimethyl amino benzaldehyde as Condensation Reaction
Spectrophotometric determination
Sulfamethoxazole
Condensation reaction
P-N
Ndimethyl amino benzaldehyde
Publication Date
Tue Oct 20 2020
Journal Name
Ibn Al-haitham Journal For Pure And Applied Sciences
Fuzzy Semimaximal Submodules
Let R be a commutative ring with unity and an R-submodule N is called semimaximal if and only if Mâ„(Nis a semisimple R-module ).The main objective of this work is to fuzzify this concept
study the basic properties and we investigate the sufficient conditions of F-submodules to be semimaximal .Also the concepts of (simple
semisimple) F- submodules and quotient F- modules are introduced and given some properties .
Let R be a commutative ring with unity and an R-submodule N is called semimaximal if and only if
the sufficient conditions of F-submodules to be semimaximal .Also the concepts of (simple , semisimple) F- submodules and quotient F- modules are introduced and given some properties .
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